Ultrasound mediated synthesis of CuS nanocrystallites

• Autorzy: Panda B. B. , Sharma B. , Rana R. K.

Identyfikatory

DOI

10.1515/msp-2016-0062

• Języki publikacji: EN

Abstrakty

EN

We present a unique ultrasonication based method for the preparation of copper sulphide nanoparticles in ambient air using a single precursor complex, which acts as a source of both metal and sulphur. The nanoparticles of 3.31 nm have been prepared successfully by the method and characterized using powder X-ray diffractogram (PXRD), dynamic light scattering (DLS) analysis UV-Vis spectroscopy and fluorescence spectroscopy. The results proved that copper sulphide nanoparticles of hexagonal structure (covellite phase) can be prepared by sonochemical method within a very short reaction time of ~5 min. The band gap of the nanomaterial has also been calculated from absorption spectrum and was found to be 2.36 eV.

Słowa kluczowe

EN

copper sulphide nanoparticles; X-ray diffraction; ultrasonication; characterization; band gap

• Wydawca: De Gruyter
• Czasopismo: Materials Science Poland
• Rocznik: 2016
• Tom: Vol. 34, No. 2
• Strony: 446--450
• Opis fizyczny: Bibliogr. 58 poz., rys.

Twórcy

autor

Panda B. B.

• Department of Chemistry, Indira Gandhi Institute of Technology, Sarang, Dhenkanal, Odisha-759146, India

autor

Sharma B.

• Nanomaterials Laboratory, I & PC division, CSIR – Indian Institute of Chemical Technology, Hyderabad-500007, India

autor

Rana R. K.

• Nanomaterials Laboratory, I & PC division, CSIR – Indian Institute of Chemical Technology, Hyderabad-500007, India

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Uwagi

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.