Synthesis and characterization of Zn/ZnO microspheres on indented sites of silicon substrate

Ahmed, N.; Majid, A.; Khan, M. A.; Rashid, M.; Umar, Z. A.; Baig, M. A.

doi:10.2478/msp-2018-0058

Artykuł - szczegóły

Tytuł artykułu

Synthesis and characterization of Zn/ZnO microspheres on indented sites of silicon substrate

Autorzy

Ahmed N. , Majid A. , Khan M. A. , Rashid M. , Umar Z. A. , Baig M. A.

Wybrane pełne teksty z tego czasopisma

Identyfikatory

DOI

10.2478/msp-2018-0058

Warianty tytułu

Języki publikacji

Abstrakty

Self-assembled Zn/ZnO microspheres have been accomplished on selected sites of boron doped P-type silicon substrates using hydrothermal approach. The high density Zn/ZnO microspheres were grown on the Si substrates by chemical treatment in mixed solution of zinc sulfate ZnSO₄·7H₂O and ammonium hydroxide NH₄ (OH) after uniform heating at 95 degrees C for 15 min. The Zn/ZnO microspheres had dimensions in the range of 1 pm to 20 pm and were created only on selected sites of silicon substrate. The crystal structure, chemical composition and morphology of as-prepared samples were studied by using scanning electron microscope SEM, X-ray diffraction XRD, energy dispersive X-ray spectroscopy EDS, Fourier transform infrared spectroscopy FT-IR and UV-Vis diffuse reflectance absorption spectra DRS. The energy band gap E_g of about 3.28 eV was obtained using Tauc plot. In summary, this study suggests that interfacial chemistry is responsible for the crystal growth on indented sites of silicon substrate and the hydrothermal based growth mechanism is proposed as a useful methodology for the formation of highly crystalline three dimensional (3-D) Zn/ZnO microspheres.

Słowa kluczowe

Zn/ZnO hydrothermal synthesis microspheres growth indent

Wydawca

De Gruyter

Czasopismo

Materials Science Poland

Rocznik

2018

Tom

Vol. 36, No. 3

Strony

501--508

Opis fizyczny

Bibliogr. 50 poz., rys., tab.

Twórcy

autor

Ahmed N.

nasar.ahmed@ajku.edu.pk

Department of Physics, University of Azad Jammu and Kashmir, Muzaffarabad-13100, Pakistan

autor

Majid A.

Department of Physics, University of Azad Jammu and Kashmir, Muzaffarabad-13100, Pakistan
Department of Physics, College of Science, Majmaah University, P.O. Box no. 1712, Al-Zulfi 11932, Saudi Arabia

autor

Khan M. A.

Department of Physics, University of Azad Jammu and Kashmir, Muzaffarabad-13100, Pakistan

autor

Rashid M.

Department of Physics, University of Azad Jammu and Kashmir, Muzaffarabad-13100, Pakistan

autor

Umar Z. A.

National Centre for Physics, Quaid-i-Azam University Campus, 45320 Islamabad, Pakistan

autor

Baig M. A.

Department of Physics, University of Azad Jammu and Kashmir, Muzaffarabad-13100, Pakistan
National Centre for Physics, Quaid-i-Azam University Campus, 45320 Islamabad, Pakistan

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Typ dokumentu

Bibliografia

Identyfikator YADDA

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