Liquid phase microextraction techniques combined with chromatography analysis: a review

Dugheri, Stefano; Mucci, Nicola; Bonari, Alessandro; Campagna, Marcello; Montalti, Manfredi; Arcangeli, Giulio; Ubiali, Daniela; Marrubini, Giorgio; Cappelli, Giovanni

doi:10.1556/1326.2019.00636

Artykuł - szczegóły

Tytuł artykułu

Liquid phase microextraction techniques combined with chromatography analysis: a review

Autorzy

Dugheri Stefano , Mucci Nicola , Bonari Alessandro , Campagna Marcello , Montalti Manfredi , Arcangeli Giulio , Ubiali Daniela , Marrubini Giorgio , Cappelli Giovanni

Wybrane pełne teksty z tego czasopisma

Identyfikatory

DOI

10.1556/1326.2019.00636

Warianty tytułu

Języki publikacji

Abstrakty

Sample pretreatment is the first and the most important step of an analytical procedure. In routine analysis, liquid–liquid microextraction (LLE) is the most widely used sample pre-treatment technique, whose goal is to isolate the target analytes, provide enrichment, with cleanup to lower the chemical noise, and enhance the signal. The use of extensive volumes of hazardous organic solvents and production of large amounts of waste make LLE procedures unsuitable for modern, highly automated laboratories, expensive, and environmentally unfriendly. In the past two decades, liquid-phase microextraction (LPME) was introduced to overcome these drawbacks. Thanks to the need of only a few microliters of extraction solvent, LPME techniques have been widely adopted by the scientific community. The aim of this review is to report on the state-of-the-art LPME techniques used in gas and liquid chromatography. Attention was paid to the classification of the LPME operating modes, to the historical contextualization of LPME applications, and to the advantages of microextraction in methods respecting the value of green analytical chemistry. Technical aspects such as description of methodology selected in method development for routine use, specific variants of LPME developed for complex matrices, derivatization, and enrichment techniques are also discussed.

Słowa kluczowe

Liquid phase MicroExtraction gas chromatography liquid chromatography derivatization large volume injection

Wydawca

University of Silesia in Katowice
Akademiai Kiado

Czasopismo

Acta Chromatographica

Rocznik

2020

Tom

Vol. 32, no. 2

Strony

69--79

Opis fizyczny

Bibliogr. 162 poz., rys.

Twórcy

autor

Dugheri Stefano

Careggi University Hospital, Florence, Italy

autor

Mucci Nicola

University of Florence, Florence, Italy

autor

Bonari Alessandro

University of Florence, Florence, Italy

autor

Campagna Marcello

University of Cagliari, Cagliari, Italy

autor

Montalti Manfredi

University of Florence, Florence, Italy

autor

Arcangeli Giulio

University of Florence, Florence, Italy

autor

Ubiali Daniela

University of Pavia, Pavia, Italy

autor

Marrubini Giorgio

University of Pavia, Pavia, Italy

autor

Cappelli Giovanni

University of Florence, Florence, Italy

Bibliografia

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Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2020).

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Bibliografia

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