Effect of Heat Treatment Temperature on Isothermal Oxidation of Ni-based Fe-33Ni-19Cr Alloy

• Autorzy: Zaiton Nurul Athirah Z. , Parimin Noraziana , Hayazi Nur Farhana , Zainal Farah Farhana , Garus Sebastian , Vizureanu Petrica

Identyfikatory

DOI

10.24425/amm.2024.149806

• Języki publikacji: EN

Abstrakty

EN

This project studies the influence of different grain sizes of Ni-based Fe-33Ni-19Cr alloy obtained from heat treatment procedure on high temperature isothermal oxidation. Heat treatment procedure was carried out at two different temperatures, namely 1000℃ and 1200℃ for 3 hours of soaking time, followed by quenching in the water. These samples are denoted as T1000 and T1200. The heat-treated Ni-based Fe-33Ni-19Cr alloy was subjected to an isothermal oxidation test at 950℃ for 150 hours exposure. Oxidized heat-treated alloys were tested in terms of oxidation kinetics, phase analysis and surface morphology of oxidized samples. Oxidation kinetics were determine based on weight change per surface area as a function of exposure time. Phase analysis was determined using the x-ray diffraction (XRD) technique and surface morphology of oxidized samples was characterized using a scanning electron microscope (SEM). As a result, the heat treatment procedure shows varying grain sizes. The higher the heat treatment temperature, shows an increase in grain size with a decrease in hardness value. The oxidation kinetics for both heat-treated samples showed an increment pattern of weight change and followed a parabolic rate law. The oxidized T1000 sample recorded the lowest parabolic rate constant of 3.12×10^-8mg²cm^-4s^-1, indicating a low oxidation rate, thus having good oxidation resistance. Phase analysis from the XRD technique recorded several oxide phases consisting of Cr₂O₃, MnCr₂O₄, and (Ti_0.97Cr_0.03)O₂ oxide phases. In addition, a uniform oxide layer is formed on the oxidized T1000 sample, indicating good oxide scale adhesion, thereby improving the protective oxide behavior.

Słowa kluczowe

EN

Ni-based alloys; Fe-Ni-Cr alloys; Incoloy 800H alloy; high temperature oxidation; oxidation kinetics

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2024
• Tom: Vol. 69, iss. 2
• Strony: 747--752
• Opis fizyczny: Bibliogr. 30 poz., fot., rys., tab.

Twórcy

autor

Zaiton Nurul Athirah Z.

• Universiti Malaysia Perlis (UniMAP), Faculty of Chemical Engineering & Technology, 02600 Arau, Perlis, Malaysia

• https://orcid.org/0009-0005-5636-3710

autor

Parimin Noraziana

• Universiti Malaysia Perlis (UniMAP), Faculty of Chemical Engineering & Technology, 02600 Arau, Perlis, Malaysia
• Universiti Malaysia Perlis (UniMAP), Surface Technology Special Interest Group, Faculty of Chemical Engineering & Technology, 02600 Arau, Perlis, Malaysia

• https://orcid.org/0000-0003-2069-7207

autor

Hayazi Nur Farhana

• Universiti Malaysia Perlis (UniMAP), Faculty of Chemical Engineering & Technology, 02600 Arau, Perlis, Malaysia
• Universiti Malaysia Perlis (UniMAP), Surface Technology Special Interest Group, Faculty of Chemical Engineering & Technology, 02600 Arau, Perlis, Malaysia

• https://orcid.org/0000-0001-8583-5995

autor

Zainal Farah Farhana

• Universiti Malaysia Perlis (UniMAP), Faculty of Chemical Engineering & Technology, 02600 Arau, Perlis, Malaysia
• Universiti Malaysia Perlis (UniMAP), Surface Technology Special Interest Group, Faculty of Chemical Engineering & Technology, 02600 Arau, Perlis, Malaysia

• https://orcid.org/0000-0001-5550-8117

autor

Garus Sebastian

• Czestochowa University of Technology, Faculty of Mechanical Engineering and Computer Science, 42-201 Częstochowa, Poland

• https://orcid.org/0000-0002-6649-5435

autor

Vizureanu Petrica

• Gheorghe Asachi Technical University of Iasi, Faculty of Material Science and Engineering, 41 D. Mangeron St., 700050 Iasi, Romania

• https://orcid.org/0000-0002-3593-9400

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Uwagi

This research was funded by the Ministry of Higher Education Malaysia under the Fundamental Research Grant Scheme (FRGS) FRGS/1/2020/TK0/UNIMA)/02/43