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Nanoindentation studies of TNZ and Ti2448 biomaterials after magnetoelectropolishing

Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
This work presents the nanoindentation results of two newly developed titanium alloy biomaterials, TNZ and Ti2448, after different surface treatments. The investigations were performed on the samples, AR – as received, MP – after abrasive polishing, EP – after a standard electropolshing, and MEP – after magnetoelectropolishing. The electropolishing processes, both EP and MEP, were conducted in the same proprietary electrolyte based on concentrated sulfuric acid. The mechanical properties of the titanium alloys biomaterials demonstrated an evident dependence on the surface treatment method, with MEP samples revealing extremely different behaviour and mechanical properties. Such a different mechanical behaviour may mean completely different composition and thickness of the surface film formed on the studied samples after MEP.
Rocznik
Strony
34--44
Opis fizyczny
Bibliogr. 25 poz., rys., tab., wykr.
Twórcy
  • Koszalin University of Technology, Faculty of Mechanical Engineering, Division of Surface Electrochemistry, Racławicka 15-17, 75-620 Koszalin, Poland
autor
  • Koszalin University of Technology, Faculty of Mechanical Engineering, Division of Surface Electrochemistry, Racławicka 15-17, 75-620 Koszalin, Poland
autor
  • Electrobright, 142 W. Main St, Macungie, PA 18062, USA
  • info@electrobright.com
autor
  • Ecole Nationale Supérieure de Chimie de Paris, France
Bibliografia
  • 1. Hryniewicz T., Rokosz K., Valíček J., Rokicki R., Effect of magnetoelectropolishing on nano-hardness and Young’s modulus of titanium biomaterial, Materials Letters, 83 (2012), 69–72.
  • 2. Hryniewicz T., Konarski P., Rokicki R., Valíček J., SIMS studies of titanium biomaterial hydrogenation after magnetoelectropolishing, Surf. Coat. Technol., 206 (2012), 4027–4031.
  • 3. Rokicki R., Haider W., Hryniewicz T., Influence of sodium hypochlorite treatment of electro-polished and magnetoelectropolished nitinol surfaces on adhesion and proliferation of MC3T3 pre-osteoblast cells, J. Mater. Sci. Mater. Med., 23 (2012), 2127–2139.
  • 4. Rokicki R., The passive oxide film on electropolished titanium, Met. Finish., 88 (1990), 65–66.
  • 5. Kuhn A., The electropolishing of titanium and its alloys, Met. Finish., 102(6) (2004), 80–86.
  • 6. Hryniewicz T., Rokicki R., Rokosz K., Corrosion and Surface characterization of titanium bio-material after magnetoelectropolishing, Surf. Coat. Technol., 203(10-11) (2009), 1508–1515.
  • 7. Simka W., Kaczmarek M., Baron-Wiecheć A., Nawrat G., Marciniak J., Żak J., Electropolishing and passivation of NiTi shape memory alloy, Electrochimica Acta, 55(7), (2010), 2437–2441.
  • 8. Simka W., Mosiałek M., Nawrat G., Nowak P., Żak J., Szade J., Winiarski A., Maciej A., Szyk-Warszyńska L., Electrochemical polishing of Ti–13Nb–13Zr Alloy, Surf. Coat. Technol., 213, (2012), 239–246.
  • 9. Rokicki R., Hryniewicz T., Rokosz K., Modifying metallic implants with magnetoelectropolish-ing, Med. Device & Diagn. Industry, 30(1), (2008), 102–11.
  • 10. Hryniewicz T., Rokicki R., Rokosz K., Magnetoelectropolished titanium biomaterial, Chapter 11, in Biomaterials Science and Engineering, Rosario Pignatello (ed.), ISBN 978-953-308-118-2; InTech, (2011), 227–248.
  • 11. Hryniewicz T., Rokicki R., Rokosz K., Magnetoelectropolishing for metal surface Modification, Trans. Inst. Met. Finish., 85(6) (2007), 325–32.
  • 12. Hryniewicz T., Rokosz K., On the wear inspection and endurance recovery of nitinol endodontic files, PAK (Measurement Automation and Monitoring), 55(4) (2009), 247–250.
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  • 13. Long M, Rack HJ. Titanium alloys in total joint replacement--a materials science perspective. Biomaterials, 19(18) (1998), 1621-1639.
  • 14. Pluta Z., Hryniewicz T., Quantitative determination of material hardness, J. Quantum Inform. Sci., 1(3) (2011), 127–134.
  • 15. Hryniewicz T., Rokicki R., Rokosz K., Magnetoelectropolishing process improves characteristics of finished metal surfaces, Met. Finish., 104(12) (2006), 26–33.
  • 16. Hryniewicz T., Rokosz K., Rokicki R., Surface investigation of NiTi rotary endodonticinstru-ments after magnetoelectropolishing, MRS Proceedings, Biomaterials (XVIII International Mate-rials Research Congress, 9. Biomaterials, Cancun, Mexico, 16–20 August 2009), vol. 1244E978-1-60511-221-3; 2009, 21–32.
  • 17. Rokosz K., Hryniewicz T., Valíček J., Harničárová M., Vyležík M., Nanoindentation measurements of AISI 316L biomaterial samples after annual immersion in Ringer’s solution followed by electrochemical polishing in a magnetic field, PAK (Measurement Automation and Monitoring), 58(5) (2012), 460-463.
  • 18. Shuman D., Computerized Image Analysis Software for Measuring Indents by AFM, Micros-copy-Analysis, P 21, (May 2005)Fischer-Cripps, A.C. Nanoindentation. Springer, New York, 2004.
  • 19. Oliver W.C., and Pharr G.M., Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology, J. Mater. Res., 19 (2004), 3-27.
  • 20. Chuang L.C., Luo C.H., Yang S., The structure and mechanical properties of thick rutile–TiO2 films using different coating treatments, Appl. Surf. Sci., 258 (201), 1297-303.
  • 21. Cheng Y-T., Cheng C-M., Scaling, dimensional analysis, and indentation measurements, Mater. Sci. Eng. R, 44 (2004), 91-149.
  • 22. Rokicki R., US Patent 7632390, 2009.
  • 23. Technical documentation and manual of HYSITRON™. www.hysitron.com
  • 24. Marteleur M., Sun F., Gloriant T., Vermaut P., Jacques P.J., and Prima F., On the design of new β-metastable titanium alloys with improved work hardening rate thanks to simultaneous TRIP and TWIP effects, Scripta Materialia, 66 (2012), 749-752.
  • 25. StatSoft Inc. STATISTICA (data analysis software system), version 10. www.statsoft.com 2011.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-24d5c50e-38f9-4c18-aa5b-1cc8ca2d664b
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