Synthesis and characterization of indium tin oxide nanoparticles via reflux method

• Autorzy: Manafi S. , Tazikeh S. , Joughehdoust S.

Identyfikatory

DOI

10.1515/msp-2018-0008

• Języki publikacji: EN

Abstrakty

EN

Synthesis of indium tin oxide (ITO) nanoparticles by reflux method without chlorine contamination at different pHs, temperatures, solvents and concentrations has been studied. Indium chloride, tin chloride, water, ethanol and Triton X-100 were used as starting materials. Structure, size, surface morphology and transparency of indium tin oxide nanoparticles were studied by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM) and UV-Vis spectrophotometry. XRD patterns showed that 400 °C is the lowest temperature for synthesis of ITO nanoparticles because metal hydroxide does not transform to metal oxide in lower temperature. FT-IR results showed the transformation of hydroxyl groups to oxide. SEM images showed that pH is the most important factor affecting the nanoparticles size. The smallest nanoparticles (40 nm) were obtained at pH = 8.8. The size of crystallites was decreased by lowering of concentration (0.025 M).

Słowa kluczowe

EN

reflux method; indium tin oxide; resistivity; transparency

• Wydawca: De Gruyter
• Czasopismo: Materials Science Poland
• Rocznik: 2017
• Tom: Vol. 35, No. 4
• Strony: 799--805
• Opis fizyczny: Bibliogr. 25 poz., rys., tab.

Twórcy

autor

Manafi S.

• Department of Engineering, Shahrood Branch, Islamic Azad University, Shahrood, Iran

autor

Tazikeh S.

• Department of Engineering, Shahrood Branch, Islamic Azad University, Shahrood, Iran

autor

Joughehdoust S.

• Department of Engineering, Shahrood Branch, Islamic Azad University, Shahrood, Iran

Bibliografia

• [1] GAO Y., ZHAO G., DUAN Z., REN Y., Mater. Sci.- Poland, 32 (2014), 66.
• [2] LIU Y., ŠTEFANIĆ G., RATHOUSKY J., HAYDEN O., BEIN T., FATTAKHOVA-ROHLFING D., Chem. Sci., 3 (2012), 2367.
• [3] DOMARADZKI J., KACZMAREK D., DRABCZYK K., PANEK P., Mater. Sci.-Poland, 33 (2015), 363.
• [4] RAJABI N., HESHMATPOUR F., MALEKFAR R., Mater. Sci.-Poland, 32 (2014), 102.
• [5] SHI J., SHEN L., MENG F., LIU Z., Mater. Lett., 182 (2016), 32.
• [6] POHL A., DUNN B., Thin solid films, 515 (2006), 790.
• [7] SONG S., YANG T., LIU J., XIN Y., LI Y., HAN S., Appl. Surf. Sci., 257 (2011), 7061.
• [8] QIANG X.B., KANG F.R., BIN Y., YONG D., Trans. Nonferrous Met. Soc. China, 20 (2010), 643.
• [9] ZHANG D., TAVAKOLIYARAKI A., WUB Y., VAN SWAAIJ R.A., ZEMAN M., Energy Procedia, 8 (2011), 207.
• [10] ZHANG H., YE F., LIU L., XU H., SUN C., J. Alloys Compd., 504 (2010), 171.
• [11] MEHTA V., COOPER J., J. Power Sources, 114 (2002), 32.
• [12] XU S., SHI Y., Sens. Actuat. B., 143 (2009), 71.
• [13] PATEL N.G., PATEL P.D., VAISHNAV V.S., Sens. Actuat. B., 96 (2003), 180.
• [14] PATEL N.G., MAKHIJA K.K., PANCHAL C.J., Sens. Actuat. B., 21 (1994), 193.
• [15] PATEL N.G., MAKHIJA K.K., PANCHAL C.J., DAVE D.B., VAISHNAV V.S., Sens. Actuat. B., 23 (1995), 49.
• [16] LUO S., OKADA K., KOHIKI S., TSUTSUI F., SHIMOOKA H., SHOJI F., Mater. Lett., 63 (2009), 641.
• [17] DELACY G., LACEY S., ZHANG D., VALDES E., HOANG K., Mater. Lett., 117 (2014), 108.
• [18] KYU-JEON M., KANG M., Mater. Lett., 62 (2008), 676.
• [19] XIE-BIN Z., TAO J., GUAN-ZHOU Q., BAI-YUN H., Trans. Nonferrous Met. Soc. China, 19 (2009), 752
• [20] WOOD S., SAMSON I., Ore. Geol. Rev., 28 (2006), 57.
• [21] JIANG L., SUN G., ZHOU Z., SUN S., WANG Q., YAN S., LI H., TIAN J., GUO J., ZHOU B., XIN Q., J. Phys. Chem. B., 109 (2005), 8774.
• [22] YU D., YU W., WANG D., QIAN Y., Thin solid films, 419 (2002), 166.
• [23] THOMAS HE Y., WANG J., TOKUNAGA T., J. Nanapart. Res., 10 (2008), 321.
• [24] KIM K.Y., PARK S.B., Mater. Chem. Phys., 86 (2004), 210.
• [25] SILVA G.M, FARIA DE E.H., NASSAR E.J., CIUFFI K.J., CALEFI P.S., Quim. Nova., 35 (2012), 473.

Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).