Comparison of different columns in analysis of C1–C5 aliphatic acids mixture in ion exclusion chromatography and vacancy ion exclusion chromatography modes

• Autorzy: Zapała W. , Kostka J , Kaczmarski K.
• Języki publikacji: EN

Abstrakty

EN

Ion exclusion chromatography (IEC) is a chromatographic technique based on the exclusion of dissociated sample molecules. This method has many applications in various analytical separations of weak acids. An alternative technique is the vacancy IEC (v-IEC), where the column is equilibrated with the sample solution flowing as mobile phase through the system, whereas pure water is injected as a sample. In this case, characteristic negative “vacant” peaks are obtained. The aim of this paper is to compare the efficiency of four RP-HPLC columns in the separation of C1–C5 aliphatic acids mixture by use of classical HPLC and very high pressure liquid chromatography. The investigations were conducted in IEC and v-IEC modes.

Słowa kluczowe

EN

ion exclusion chromatography; vacancy ion-exclusion chromatography; aliphatic acids; HPLC; very high pressure liquid chromatography

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2011
• Tom: Vol. 23, no. 3
• Strony: 377--388
• Opis fizyczny: Bibliogr. 31 poz., rys., tab.

Twórcy

autor

Zapała W.

• Rzeszów University of Technology Department of Chemical and Process Engineering, Chemical Faculty Powstańców Warszawy 6 35-959 Rzeszów Poland

autor

Kostka J

• Rzeszów University of Technology Department of Chemical and Process Engineering, Chemical Faculty Powstańców Warszawy 6 35-959 Rzeszów Poland

autor

Kaczmarski K.

• Rzeszów University of Technology Department of Chemical and Process Engineering, Chemical Faculty Powstańców Warszawy 6 35-959 Rzeszów Poland

Bibliografia

• [1] V.T. Turkelson and M. Richards, Anal. Chem., 50, 1420 (1978)
• [2] K. Tanaka and J.S. Fritz, J. Chromatogr., 409, 271 (1987)
• [3] J.S. Fritz, J. Chromatogr., 546, 111 (1991)
• [4] K. Tanaka, K. Ohta, J.S. Fritz, Y.-S. Lee, and S.-B. Shim, J. Chromatogr. A, 706, 385 (1995)
• [5] K. Tanaka, K. Ohta, and J.S. Fritz, J. Chromatogr. A, 770, 211 (1997)
• [6] K.L. Ng, B. Paull, P.R. Haddad, and K. Tanaka, J. Chromatogr. A, 850, 17 (1999)
• [7] K. Ohta, A. Towata, M. Ohashi, J. Chromatogr. A, 997, 95 (2003)
• [8] K. Ohta, A. Towata, M. Ohashi, J. Chromatogr. A, 997, 107 (2003)
• [9] M. Novic and P.R. Haddad, J. Chromatogr. A, 1118, 19 (2006)
• [10] T. Abe, H. Baba, I. Soloshonok, and K. Tanaka, J. Chromatogr. A, 884, 93 (2000)
• [11] T. Abe, H. Baba, E. Itoh, and K. Tanaka, J. Chromatogr. A, 920, 173 (2001)
• [12] K.L. Ng, B.K. Glód, G.W. Dicinoski, and P.R. Haddad, J. Chromatogr. A, 920, 41 (2001)
• [13] K. Tanaka, H. Chikara, W. Hu, and K. Hasebe, J. Chromatogr. A, 850, 187 (1999)
• [14] K. Tanaka, K. Ohta, P.R. Haddad, J.S. Fritz, A. Miyanaga, W. Hu, and K. Hasebe, J. Chromatogr. A, 884, 167 (2000)
• [15] K. Tanaka, K. Ohta, P.R. Haddad, J.S. Fritz, A. Miyanaga, W. Hu, K. Hasebe, K.P. Lee, and C. Sarzanini, J. Chromatogr. A, 920, 239 (2001)
• [16] K. Tanaka, M. Yu Ding, M.I.H. Helaleh, H. Taoda, H. Takahashi, W. Hu, K. Hasebe, P.R. Haddad, J. S. Fritz, and C. Sarzanini, J. Chromatogr. A, 956, 209 (2002)
• [17] K. Tanaka, M. Mori, Q. Xu, M.I.H. Helaleh, M. Ikedo, H. Taoda, W. Hu, K. Hasebe, J. S. Fritz, and P.R. Haddad, J. Chromatogr. A, 997, 127 (2003)
• [18] M.I.H. Helaleh, K. Tanaka, M. Mori, Q. Xu, H. Taoda, M.Yu Ding, W. Hu, K. Hasebe, and P.R. Haddad, J. Chromatogr. A, 997, 133 (2003)
• [19] M.I.H. Helaleh, K. Tanaka, M. Mori, Q. Xu, H. Taoda, M.Yu Ding, W. Hu, K. Hasebe, and P.R. Haddad, J. Chromatogr. A, 997, 139 (2003)
• [20] M. Mori, K. Tanaka, M.I.H. Helaleh, Q. Xu, M. Ikedo, Y. Ogura, S. Sato, W. Hu, K. Hasebe, and P.R. Haddad, J. Chromatogr. A, 997, 219 (2003)
• [21] K. Ito, Y. Takayama, M. Ikedo, M. Mori, H. Taoda, Q. Xu, W. Hu, H. Sunahara, T. Hayashi, S. Sato, T. Hirokawa, and K. Tanaka, J. Chromatogr. A, 1039, 141 (2004)
• [22] M. Mori, M. Ikedo, W. Hu, M.I.H. Helaleh, Q. Xu, H. Itabashi, and K. Tanaka, J. Chromatogr. A, 1092, 250 (2005)
• [23] M. Mori, H. Itabashi, M.I.H. Helaleh, K. Kaczmarski, B.K. Głód, T. Kowalska, Q. Xu, M. Ikedo, W. Hu, and K. Tanaka, J. Chromatogr. A, 1118, 41 (2006)
• [24] M. Mori, K. Tanaka, T. Satori, M. Ikedo, W. Hu, and H. Itabashi, J. Chromatogr. A, 1118, 51 (2006)
• [25] M. Mori, T. Iwata, T. Satori, Shin-Ichi Ohira, H. Itabashi, and K. Tanaka, J. Chromatogr. A, 1213, 125 (2008)
• [26] K. Kaczmarski, M. Mori, B. Głód, and T. Kowalska, Modeling of the Organic Acid Retention on a Strongly Acidic Cation-Exchange Resin in the H+-Form and in the Reversed-Phase C-18 System. In: The XXIXth Symposium on Chromatographic Methods of Investigating the Organic Compounds, Book of Abstracts, p. 12, Katowice-Szczyrk, June 8–10, 2005
• [27] M. Asztemborska, K. Kaczmarski, E. Zbaraża, T. Kowalska, and B.K. Głód, Vacant Reversed Phase High Performance Liquid Chromatography (VRP-HPLC). In: The XXIXth Symposium on Chromatographic Methods of Investigating the Organic Compounds, Book of Abstracts, p. 48, Katowice-Szczyrk, June 8–10, 2005
• [28] K. Kaczmarski, W. Zapała, W. Wanat, M. Mori, B.K. Głód, and T. Kowalska, J. Chromatogr. Sci., 45(1), 6 (2007)
• [29] W. Zapała and K. Kaczmarski, Acta Chromatogr., 22(1), 1 (2010)
• [30] W. Zapała and K. Kaczmarski, Acta Chromatogr., 22(3), 337 (2010)
• [31] K. Kaczmarski, F. Gritti, J. Kostka, and G. Guiochon, J. Chromatogr. A, 1216, 6575 (2009)