A simple HPLC-DAD method for analysis of phenolic acids: Addition effect of a hydrophilic deep eutectic solvent to the mobile phase

• Autorzy: Pérez-López Luis Alejandro , Cavazos-Rocha Norma , Delgado-Montemayor Cecilia , Waksman-Minsky Noemí , Hernández-Salazar Marcelo , Portillo-Castillo Omar J.

Identyfikatory

DOI

10.1556/1326.2022.01055

• Języki publikacji: EN

Abstrakty

EN

The analysis of phenolic acids (PAs) is of great importance, because they are frequently present in natural products and their derivatives, and these compounds also have multiple beneficial effects to human health. This work is focusing on the separation of seven PAs (caffeic acid, coumaric acid, gallic acid, ferulic acid, protocatechuic acid, sinapic acid, and syringic acid), in a reversed-phase liquid chromatographic (RP-HPLC) isocratic method using a hydrophilic deep eutectic solvent (DES) as a mobile phase additive. The analysis was carried out with a diode array detector. The used DES was composed by choline chloride and glycerol, and it was characterized by infrared spectroscopy. The combination of choline chloride:glycerol (1:4) added at 0.25% to mobile phase composed of 0.15% formic acid aqueous solution and methanol (80:20), showed the best separation for target analytes. The new proposed method was validated, and results indicated that the proposed method is linear, selective for almost all analytes, provided high sensitivity with limit of detection ranges from 0.009 to 0.023 mg mL⁻¹, and has satisfactory precision and accuracy, with values of relative standard deviation of 0.24–2.65% and recoveries of 97.97–109%, respectively. Additionally, this method was successfully applied to simultaneous determination of phenolic acids in three kinds of samples of powder to prepare lemon flavour drink enriched with black tea extract.

Słowa kluczowe

EN

phenolic acids; deep eutectic solvents; additives; mobile phase; HPLC

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2023
• Tom: Vol. 35, no. 2
• Strony: 204--216
• Opis fizyczny: Bibliogr. 48 poz., tab., wykr.

Twórcy

autor

Pérez-López Luis Alejandro

• Departamento de Química Analítica, Facultad de Medicina, Universidad Autónoma de Nuevo León, Monterrey, Nuevo León, México

autor

Cavazos-Rocha Norma

• Departamento de Química Analítica, Facultad de Medicina, Universidad Autónoma de Nuevo León, Monterrey, Nuevo León, México

autor

Delgado-Montemayor Cecilia

• Departamento de Química Analítica, Facultad de Medicina, Universidad Autónoma de Nuevo León, Monterrey, Nuevo León, México

autor

Waksman-Minsky Noemí

• Departamento de Química Analítica, Facultad de Medicina, Universidad Autónoma de Nuevo León, Monterrey, Nuevo León, México

autor

Hernández-Salazar Marcelo

• Centro de Investigación en Nutrición y Salud Pública, Facultad de Salud Pública y Nutrición, Universidad Autónoma de Nuevo León, Monterrey, Nuevo León, México

autor

Portillo-Castillo Omar J.

• Departamento de Química Analítica, Facultad de Medicina, Universidad Autónoma de Nuevo León, Monterrey, Nuevo León, México

• https://orcid.org/0000-0002-7690-2153

Bibliografia

• 1. Kumar, N.; Goel, N. Biotechnol. Rep. 2019, 24, e00370.
• 2. Shahidi, F.; Ambigaipalan, P. J. Funct. Foods 2015, 18, 820.
• 3. Paśko, P.; Sajewicz, M.; Gorinstein, S.; Zachwieja, Z. Acta Chromatogr. 2008, 4, 661.
• 4. Chocholouš, P.; Vacková, J.; Šrámková, I.; Šatínský, D.; Solich, P. Talanta 2013, 103, 221.
• 5. Peng, L. Q.; Cao, J.; Du, L. J.; Zhang, Q. D.; Shi, Y. T.; Xu, J. J. J. Chromatogr. A. 2017, 1499, 132.
• 6. Hefni, M. E.; Amann, L. S.; Witthöft, C. M. Food Anal. Methods 2019, 12, 2802.
• 7. Canini, A.; Alesiani, D.; D’Arcangelo, G.; Tagliatesta, P. J. Food Compos. Anal. 2007, 20, 584.
• 8. García-Villalba, R.; Pacchiarotta, T.; Carrasco-Pancorbo, A.; Segura-Carretero, A.; Fernández-Gutiérrez, A.; Deelder, A. M.; Mayboroda, O. A. J. Chromatogr. A. 2011, 1218, 959.
• 9. de Souza Campos Junior, F. A.; Petrarca, M. H.; Meinhart, A. D.; Filho, M. de J.; Godoy, H. T. Food Res. Int. 2019, 126, 108685.
• 10. Chen, X.; Mao, J.; Wen, F.; Xu, X. Anal. Lett. 2020, 54, 817.
• 11. Gałuszka, A.; Migaszewski, Z.; Namieśnik, J. TrAC Trends Anal. Chem. 2013, 50, 78.
• 12. Bastos Santos, L.; Santos Assis, R.; Alves Barreto, J.; Almeida Bezerra, M.; Galvão Novaes, C.; Azevedo Lemos, V. TrAC Trends Anal. Chem. 2022, 146, 116478.
• 13. Pacheco-Fernández, I.; Pino, V. Curr. Opin. Green. Sustain. Chem. 2019, 18, 42.
• 14. Hansen, B. B.; Spittle, S.; Chen, B.; Poe, D.; Zhang, Y.; Klein, J. M.; Horton, A.; Adhikari, L.; Zelovich, T.; Doherty, B. W.; Gurkan, B.; Maginn, E. J.; Ragauskas, A.; Dadmun, M.; Zawodzinski, T. A.; Baker, G. A.; Tuckerman, M. E.; Savinell, R. F.; Sangoro, J. R. Chem. Rev. 2021, 121, 1232.
• 15. Ortega-Zamora, C.; González-Sálamo, J.; Hernández-Borges, J. Molecules. 2021, 26, 6846.
• 16. Abbott, A. P.; Capper, G.; Davies, D. L.; Rasheed, R. K.; Tambyrajah, V. Chem. Comm. 2003, 1, 70.
• 17. Safav, A.; Ahmadi, R.; Ramezani, A. M. Microchem. J. 2018, 143, 166.
• 18. Wan, Y.; Wang, M.; Zhang, K.; Fu, Q.; Wang, L.; Gao, M; Xia, Z.; Gao, D. J. Sep. Sci. 2019, 42, 2044.
• 19. Chen, S.; An, Q.; Sun, H.; Mao, M. Acta Chromatogr. 2021, 33, 30.
• 20. Zhao, M.; Zhao, E.; Wu, J.; Li, Y.; Li, B. Acta Chromatogr. 2022, 34, 53.
• 21. Sutton, A. T.; Fraige, K.; Leme, G. M.; da Silva Bolzani, V.; Hilder, E. F.; Cavalheiro, A. J.; Arrua, R. D.; Funari, C. S. Anal. Bioanal. Chem. 2018, 410, 3705.
• 22. Ramezani, A. M.; Absalan, G. J. Pharm. Biomed. Anal. 2020, 186, 113259.
• 23. Li, L.; Liu, Y.; Wang, Z.; Yang, L.; Liu, H. J. Sep. Sci. 2021, 44, 1098.
• 24. Płotka-Wasylkaa, J.; Rutkowska, M.; de la Guardia, M. J. Chromatogr. A. 2021, 1639, 461918.
• 25. Olives, A. I.; Gonzalez-Ruiz, V.; Martín, M. A. ACS Sustain. Chem. Eng. 2017, 5, 5618.
• 26. Cai, T.; Qiu, H. TrAC Trend Anal. Chem. 2019, 120, 115623.
• 27. Li, G.; Zhu, T.; Lei, Y. Korean J. Chem. Eng. 2015, 32, 2103.
• 28. Tan, T.; Zhang, M.; Wan, Y.; Qiu, H. 2. Talanta 2016, 149, 85.
• 29. Gao, F.; Liu, L.; Tang, W.; Ho Row, K.; Zhu, T. Sep. Sci. Technol. 2018, 53, 397.
• 30. Patil, J.; Ghodke, S.; Jain, R.; Dandekar, P. ACS Sustain. Chem. Eng. 2018, 6, 10578.
• 31. Tang, W.; Row, K. H. Polymers 2019, 11, 871.
• 32. Radošević, K.; Bubalo, M. C.; Srček, V. G.; Grgas, D.; Dragičević, T. L.; Redovniković, I. R. Ecotoxicol. Environ. Saf. 2015, 112, 46.
• 33. Ozturk, B.; Parkinson, C.; Gonzalez-Miquel, M. Sep. Purif. Technol. 2018, 206, 1.
• 34. Pigorsch, E. Starch/Stärke. 2009, 61, 129.
• 35. Mulia, K.; Krisanti, E.; Terahadi, F.; Putri, S. Int. J. Technol. 2015, 6, 1211.
• 36. Jurić, T.; Uka, D.; Barta Holló, B.; Jović, B.; Kordić, B.; Popović, B. M. J. Mol. Liq. 2021, 343, 16968.
• 37. Che Zain, M. S.; Yeoh, J. X.; Lee, S. Y.; Shaari, K. Sustainability 2021, 13, 12981.
• 38. Banjare, R. K.; Banjare, M. K.; Behera, K.; Pandey, S.; Ghosh, K. K. ACS Omega 2020, 5, 19350.
• 39. de Souza Dias, F.; Palma Lovillo, M.; Barroso, C. G.; Fagundes Carneiro, A.; David, J. M. Anal. Methods 2017, 9, 643.
• 40. Speranza, S.; Knechtl, R.; Witlaczil, R.; Schönlechner, R. Front. Plant Sci. 2021, 12, 769151.
• 41. Flieger, J.; Czajkowska- _Zelazko, A. Anal. Lett. 2012, 45, 63.
• 42. Barth, H. G. LCGC North America 2019, 37, 824.
• 43. Dolan, J. W. LCGC North America 2012, 30, 564.
• 44. Adel Nasr, Z.; Soliman, M. M.; Mohamed, E. H.; Fouad, F. A. Acta Chromatogr. 2022, 34, 138.
• 45. ICH, Guidelines. Technical requirements for the registration of pharmaceutical for human use, validation of analytical procedures: text and methodologyQ2 (R1); International Conference on Harmonization, Geneva, Switzerland, 2005.
• 46. Dong, M. W.; Wysocki, J. LCGC North America 2019, 37, 750.
• 47. Glaser, T.; Lienau, A.; Zeeb, D.; Krucker, M.; Dachtler, M.; Albert, K. Chromatographia 2003, 57, S19–125.
• 48. de Souza Santos Cheibub, A. M.; Silva Bahiense de Lyra, E.; Jardim Alves, B.; Andrade Donagemma, R.; Pereira Netto, A. D. Food Chem. 2020, 323, 126811.