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Tytuł artykułu

Development and validation of liquid chromatography–tandem mass spectrometry method for simultaneous determination of zinc pyrithione and pyrithione in shampoos

Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
A simple, rapid, and sensitive liquid chromatography–tandem mass spectrometry (LC–MS/MS) method was developed and validated for the determination of zinc pyrithione (ZnPT) and pyrithione (PT) in shampoos. The method consisted of a liquid–liquid extraction for sample preparation. The mass spectrometer was operated in multiple reaction monitoring (MRM) mode via the positive electrospray ionization interface. A linear regression (weighted 1/x) was used to fit calibration curves over the concentration range of 50–2000 ng/mL for both ZnPT and PT. Excellent linearity (r 2 ≥ 0.9996) was achieved for all. The method was validated and found to be accurate (95.9–108.2% for ZnPT and 94.9–110.4% for PT), precise, and selective. Analytes in shampoos were found to be stable in the autosampler (6 °C for 6 h), in room temperature (for 6 h), and after three freeze–thaw cycles, and recovery of analytes was reproducible (90.8–94.6% for ZnPT and 90.2–96.3% for PT).
Rocznik
Strony
200--205
Opis fizyczny
Bibliogr. 31 poz., rys.
Twórcy
autor
  • Bioresource Regional Innovation Center, Soonchunhyang University, Soonchunhyang-ro 22, Shinchang-myun, Asan, Chungnam 31538, Republic of Korea
autor
  • Department of Pharmacology, College of Medicine, Dankook University, Dandae-ro 119, Dongnam-gu, Cheonan, Chungnam 31116, Republic of Korea
autor
  • Department of Pharmacology, College of Medicine, Dankook University, Dandae-ro 119, Dongnam-gu, Cheonan, Chungnam 31116, Republic of Korea
autor
  • Department of Pharmacology, College of Medicine, Dankook University, Dandae-ro 119, Dongnam-gu, Cheonan, Chungnam 31116, Republic of Korea
autor
  • Department of Pharmacology, College of Medicine, Dankook University, Dandae-ro 119, Dongnam-gu, Cheonan, Chungnam 31116, Republic of Korea
autor
  • Department of Pharmacology, College of Medicine, Dankook University, Dandae-ro 119, Dongnam-gu, Cheonan, Chungnam 31116, Republic of Korea
Bibliografia
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  • [2] Thoma, K. V. J. Chromatogr. A 1999, 833, 105.
  • [3] Bao, V. W. W.; Leung, K. M. Y.; Kwok, K. W. H.; Zhang, A. Q.; Lui, G. C. S. Mar. Pollut. Bull. 2008, 57, 616.
  • [4] Bellas, J.; Granmo, A.; Beiras, R. Mar. Pollut. Bull. 2005, 50, 1382.
  • [5] Goka, K. Environ. Res. 1999, 81, 81.
  • [6] Kobayashi, N.; Okamura, H. Mar. Pollut. Bull. 2002, 44, 748.
  • [7] Koutsaftis, A.; Aoyama, I. Environ. Toxicol. 2006, 21, 432.
  • [8] Mochida, K.; Ito, K.; Harino, H.; Kakuno, A.; Fujii, K. Environ. Toxicol. Chem. 2006, 25, 3058.
  • [9] Mochida, K.; Ito, K.; Harino, H.; Onduka, T.; Kakuno, A.; Fujii, K. Environ. Toxicol. Chem. 2008, 27, 367.
  • [10] Mochida, K.; Ito, K.; Harino, H.; Tanaka, H.; Onduka, T.; Kakuno, A.; Fujii, K. Comp. Biochem. Physiol. C 2009, 149, 624.
  • [11] Mochida, K.; Amano, H.; Onduka, T.; Kakuno, A.; Fujii, K. Chemosphere 2011, 82, 390.
  • [12] Onduka, T.; Mochida, K.; Harino, H.; Ito, K.; Kakuno, A.; Fujii, K. Arch. Environ. Contam. Toxicol. 2010, 58, 991.
  • [13] Okamura, H.; Watanabe, T.; Aoyama, I.; Hasobe, M. Chemosphere 2002, 46, 945.
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  • [17] Sahenk, Z.; Mendell, J. R. Neurology 1977, 27, 393.
  • [18] Scientific Committee on Consumer Safety (SCCS), Opinion on Zinc Pyrithione (Colipa P81) 2014.
  • [19] Howes, D.; Black, J. G. Toxicol. 1975, 5, 209.
  • [20] Gibson, W. B.; Jeffcoat, A. R.; Turan, T. S.; Wendt, R. H.; Hughes, P. F.; Twine, M. E. Toxicol. Appl. Pharmacol. 1982, 62, 237.
  • [21] Kabacoff, B. L.; Fairchild, C. M. J. Soc. Cosmet. Chem. 1975, 26, 453.
  • [22] Voulvoulis, N.; Scrimshaw, M. D.; Lester, J. N. Chemosphere 1999, 38, 3503.
  • [23] Yamaguchi, Y.; Kumakura, A.; Sugasawa, S.; Harino, H.; Yamada, Y.; Shibata, K.; Senda, T. Int. J. Environ. Anal. Chem. 2006, 86, 83.
  • [24] Gu, Y. X.; Wang, Q. H.; Zhou, Z. L.; Lv, Q.; Mai, C. H. J. Cosmet. Sci. 2014, 65, 265.
  • [25] Chen, G.; Miao, M.; Hoptroff, M.; Fei, X.; Collins, L. Z.; Jones, A.; Janssen, H. G. J. Chromatogr. B 2015, 1003, 22.
  • [26] Krivis, A. F.; Gazda, E. S.; Supp, G. R.; Robinson, M. A. Anal. Chem. 1963, 35, 966.
  • [27] Wang, L. H. Electroanalysis 2000, 12, 227.
  • [28] Mackie, D. S.; van den Berg, C. M. G.; Readman, J. W. Anal. Chim. Acta. 2004, 511, 47.
  • [29] Montoya, M. R.; Galvin, R. M.; Mellado, J. M. R. Electroanalysis 1998, 10, 1030.
  • [30] Shih, Y.; Zen, J. M.; Kumar, A. S.; Chen, P. Y. Talanta 2004, 62, 912.
  • [31] Guidance for Industry, Bioanalytical Method Validation, US Department of Health and Human Services, Food and Drug Administration, Center for Drug Evaluation and Research (CDER), Center for Veterinary Medicine (CVM) May 2001.
Uwagi
PL
Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-184e8b01-2fbe-40d7-b006-026cea8afa32
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