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Surface structure and properties of Ti6Al4V alloy laser melted at cryogenic conditions

Wybrane pełne teksty z tego czasopisma
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: The research work has been to determine whether surface melting of the Ti6Al4V bioalloy with the high power laser, when immersed in liquid nitrogen, would result in an appearance of hard and thick surface layer, containing new structural constituents. Design/methodology/approach: The laser melting of the Ti6Al4V alloy has been made by the CO2 laser at different laser beam energy and scan rate. The specimens have been immersed in liquid nitrogen bath during laser treatment. The Vickers microhardness of cross-sections of the surface layer has been measured, and the microscopic examinations have been performed with the SEM. Findings: The laser melting at cryogenic conditions has resulted in creation of the modified surface layer, up to 1.5 mm thick with HAZ, of properties and structures different from those of the base metal. The layer has been well adjacent to base metal, its microhardness being significantly higher. The numerous zones have been observed within the surface layer, with nitrogen-containing martensite and titanium nitride structures. The negative effect has been an initiation of surface cracks. The laser beam energy has influenced the presence of different zones, their thickness, and number of cracks. Research limitations/implications: So far research has shown that proposed technique can create thick and hard surface layer, containing new structural important components. The new research is necessary in order to establish the laser treatment parameters which permit to avoid cracking and determine the phase constituents and crystallinity within the surface layer. Practical implications: The elaborated technique may be useful in order to improve the surface properties of the Ti alloys for biomedical applications. Originality/value: The paper shows original in the world-scale results of laser treatment of the Ti bioalloy at cryogenic conditions.
Rocznik
Strony
423--426
Opis fizyczny
Bibliogr. 15 poz., rys., tab.
Twórcy
  • Department of Materials Science and Engineering, Gdańsk University of Technology, ul. Narutowicza 11/12, 80-952 Gdańsk, Poland
  • Department of Materials Science and Engineering, Gdańsk University of Technology, ul. Narutowicza 11/12, 80-952 Gdańsk, Poland
  • Department of Materials Science, Corrosion and Environment Protection, Ship Design and Research Centre, ul. Wały Piastowskie 1, 80-952 Gdańsk, Poland
  • Department of Materials Science and Engineering, Gdańsk University of Technology, ul. Narutowicza 11/12, 80-952 Gdańsk, Poland
Bibliografia
  • [1] T.M. Yue, T.M. Cheung, H.C. Man, The effects of laser surface treatment on the corrosion properties of Ti-6Al-4V alloy in Hank`s solution, Journal of Materials Science Letters 19 (2000), 205-208.
  • [2] T.M. Yue, J.K. Yu, Z. Mei, H.C. Man, Excimer laser surface treatment of Ti-6Al-4V alloy for corrosion resistance enhancement, Materials Letters 52 (2002), 206-212.
  • [3] F. Guillemot, E. Prima et al., Ultraviolet laser surface treatment fore biomedical applications of E titanium alloys: morphological and structural characterization, Applied Physics A 77 (2003), 899-904.
  • [4] H. Badekas, C. Panagopoulos, S. Economou, Laser surface-treatment of titanium, Journal of Materials Processing Technology 44 (1994) 54-60.
  • [5] M.D. Ball, S. Downem, C.A. Scotchford, E.N. Antonom, V.N. Bagratashvilli, V.K. Popov, W.J. Lo, D.M. Grant, S.M. Howdle S.M., Osteoblast growth on titanium foils coated with hydroxyapatite by pulsed laser ablation, Biomaterials 22 (2001), 337-347.
  • [6] H. Badekas, C. Panagopoulos, S. Economou, Laser surface-treatment of titanium, Journal of Materials and Processing Technology 44 (1994), 54-60.
  • [7] M. Bereznai, I. Pelsöczi, Z. Tóth, K. Turzó, M. Radnai, Z. Bor, A. Fazekas, Surface modification induced by ns and sub-ps excimer laser pulses on titanium implant material, Biomaterials 24 (2003), 4197-4203.
  • [8] S.A. Cho, S.K. Jung, A removal torque of the laser-treated titanium implants in rabbit tibia, Biomaterials 24 (2003), 4859-4863.
  • [9] A. Gaggl, G. Schultes, W.D. Müller, H. Kärcher, Scanning electron microscopical analysis of laser-treated titanium implant surfaces – a comparative study, Biomaterials 21 (2000), 1067-1073.
  • [10] I. Garcia, J.J. De Damborena, Corrosion properties of TiN prepared by laser gas alloying of Ti and Ti6Al4V alloy, Corrosion Science 40 (1998), 1411-1498.
  • [11] V.M. Weerasinghe, D.R.F. West, J. de Damborenea, Laser surface nitriding of titanium and a titanium alloy, Journal of Materials Processing Technology 58 (1996), 79-86.
  • [12] G. Giavaresi, L. Ambrosio, G.A. Battistion, U. Casellato, R. Gerbasi, M. Finia, N.N. L. Aldini Martini., L. Rimondini, R. Giardino, Histomorphometric, ultrastructural and microhardness evaluation of the osseointegration of a nanostructured titanium oxide coating by metal-organic chemical vapour depostion: an in vivo study, Biomaterials 25 (2004), 5583-5591.
  • [13] J.R. Goldberg, J.L, Gilbert, The electrochemical and mechanical behavior of passivated and TiN/AlN-coated CoCrMo and Ti6Al4V alloys, Biomaterials 25 (2004), 851-864.
  • [14] H. Güleryüz, H. Çimenoğlu, Effect of thermal oxidation on corrosion and corrosion-wear behaviour of a Ti-6Al-4V alloy, Biomaterials 25 (2004), 3325-3333.
  • [15] L.H. Li, Y.M. Kong, H.W. Kim, Y.W. Kim, H.E. Kim, S.J. Heo, J.-Y. Koak, Improved biological performance of Ti implants due to surface modification by micro-arc oxidation, Biomaterials 25 (2004), 2867-2875.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-17fff525-99dc-4629-9d7c-af40e705918d
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