PL EN


Preferencje help
Widoczny [Schowaj] Abstrakt
Liczba wyników
Tytuł artykułu

Evaluation of ammonium citrate tribasic as a leaching reagent for lead-bearing ore

Treść / Zawartość
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
In this study, the leaching process of a lead-bearing ore, consisting mainly of cerussite, in an ammonium citrate tribasic medium was investigated. The parameters including temperature, reagent concentration, particle size, and stirring speed were examined. During leaching process, the lead conversion rate increased with an increase in reagent concentration, reaction temperature, and stirring speed, and a decrease in particle size. The results show that about 95% of lead content was extracted from the samples with particle size range of +75-96 μm after 21 min leaching in 1.25 mol/L ammonium citrate tribasic solution at 800 r/min and 40°C. It was found that the leaching reaction followed the shrinking core model. The results indicated that ammonium citrate tribasic could be used as an effective leaching reagent for extracting lead from lead oxide ore.
Słowa kluczowe
Rocznik
Strony
689--700
Opis fizyczny
Bibliogr. 33 poz., rys. kolor.
Twórcy
autor
  • Kunming University of Science and Technology
autor
  • Kunming University of Science and Technology
autor
  • University of Toronto, 5 King's College Road, M5S 3G8 Toronto, Canada
  • Kunming University of Science and Technology
  • Kunming University of Science and Technology
  • Zhengzhou University of Aeronautics
autor
  • Kunming University of Science and Technology
autor
  • Kunming University of Science and Technology
Bibliografia
  • BADA NOIU , G., BUZATU , T., BUZATU, M., BUTU, M., 2013. Study concerning PbO solubility in NaOH solution for the treatment of sulfate oxide pastes obtained from dismantling used lead acid batteries, Revista de Chimie., 64(9), 1004-1010.
  • BINGOL, D., C ANBAZOGLU, M., A YDOGAN, S., 2005. Dissolution kinetics of malachite in ammonia/ammonium carbonate leaching, Hydrometallurgy., 76(1), 55 62.
  • DENG, J., W EN, S. S., Y IN, Q. Q., W U, D., S UN, Q., 2017. Leaching of malachite using 5 sulfosalicylic acid, Journal of the Taiwan Institute of Chemical Engineers., 71, 20 27.
  • QICHENG F., W EN S., WANG Y., ZHAO, W., DENG, J., 2015. Investigation of leaching kinetics of cerussite in sodium hydroxide solutions , Physicochemical Problems of Mineral Processing , 51 2 ), 491 500 0204060801001200.00.20.40.60.81.0 y=0.02285+0.01244x1-3(1-x)2/3+2(1-x)0(C)0.92 (P)0.42(r)0.73exp(-E/RT) t
  • JUNWEI,, H.,H., LLIANG, C.IANG, C., L, LIU, W., IU, W., QQIN, W., IN, W., JJIAO, F.,IAO, F., LLI, W.,I, W., 2017. Pretreatment of tin anode slime using alkaline pressure Pretreatment of tin anode slime using alkaline pressure oxidativeoxidative leaching, Separation and Purification Technology., 174, 389leaching, Separation and Purification Technology., 174, 389-395.
  • H JUNWEI.,H., LLIU, W., QIN, W.IU, W., QIN, W., P, PENGENG,, B.,B., YANG, K.,YANG, K., ZHENG, Y.,ZHENG, Y., 2015.. Recovery of zinc and iron from high iron-bearing zinc calcine by selective reduction roasting, Journal of Industrial and Engineering Chemistry., 22, 272--279.
  • HIROYOSHIHI, N., , N., KISHIMOTOKISHIMOTO, , N., N., TSUNEKAWATSUNEKAWA, , M., M., HIRAJIMAHIRAJIMA T., T., MISHIMAMISHIMA, H.,, H., 2004. "Recovery of metals from Recovery of metals from melting furnace fly ash by ammonia/chloride leaching melting furnace fly ash by ammonia/chloride leaching. " Proceedings of the 29th Spring Annual Meet of The Mining and and Materials Processing Institute of Japan: 31-32
  • HUA, Y.2004. An Introduction to Metallurgical Process Kinetics, Metallurgy Industry Press, Beijing.
  • KUNKUL, A., A., GULEZGIN,GULEZGIN, A.A., DEMIRKIRAN,, DEMIRKIRAN, N.N.,, 2013. Investigation of the use of ammonium acetate as an alternative Investigation of the use of ammonium acetate as an alternative lixiviant in the leaching of malachite orelixiviant in the leaching of malachite ore,,. Chemical Industry and Chemical Engineering Quarterly/CICEQ, 19(1): 25.
  • LEVENSPIEL, O., , O., Chemical Reaction Engineering Chemical Reaction Engineering, John Wiley, New York, ,1972.
  • Li,, S., LiS., Li,, H., ChenH., Chen,, W., W., 2018. Ammonia Leaching of Zinc from Low Ammonia Leaching of Zinc from Low-grade Oxide Zinc Ores Using the Enhancement of the grade Oxide Zinc Ores Using the Enhancement of the Microwave Irradiation, International Journal of Chemical Reactor Engineering., 16(3), 1-9.
  • LIU, Z., , ZHOULAN, Y.ZHOULAN, Y., , HU., H., CHEN, Q.,HU., H., CHEN, Q., 2012. Leaching kinetics of low Leaching kinetics of low-grade copper ore with high grade copper ore with high-lkality gangues alkality gangues in ammoniain ammonia-ammonium sulphate solution, Journal of Central South University., 19(1), 77ammonium sulphate solution, Journal of Central South University., 19(1), 77-84.
  • YINGBO, M., DENG, J., WEN, S., , FANG, J.,FANG, J., YIN, Q., YIN, Q., 2016. Recovering copper from volcanic Recovering copper from volcanic ashash by NH3• H2Oby NH3• H2O-NH2COONH4, Russian Journal of NonNH2COONH4, Russian Journal of Non-Ferrous Metals., 57(6), 533Ferrous Metals., 57(6), 533-543.
  • MIKHLIN, Y., , Y., KUKLINSKYI,, A.,A., MIKHLINAMIKHLINA, , E., KARGIN, V.,E., KARGIN, V., ASANOV, I.,ASANOV, I., 2004. Electrochemical behaviour of galena Electrochemical behaviour of galena (PbS) in aqueous nitric acid and perchloric acid solutions, Jour(PbS) in aqueous nitric acid and perchloric acid solutions, Journal of applied electrochemistry., 34(1), 37-46.
  • MENG, X, X.., HAN, K.N., , HAN, K.N., 1996. "The principles and applications of ammonia leaching of metalsThe principles and applications of ammonia leaching of metals - a review. Mineral Processing and Extractive Metullargy Review 16(1): 23-61.
  • MORADI, S., S., MONHEMIUS, A.,, MONHEMIUS, A., 2011. Mixed sulphide-oxide lead and zinc ores: Problems and solutions, Minerals oxide lead and zinc ores: Problems and solutions, Minerals engineering., 24(10), 1062-1076.
  • NAGIB, S., S.,, INOUE, K.,INOUE, K., 2000. Recovery of lead and zinc from fly ash generated from municipal incineration plants by means Recovery of lead and zinc from fly ash generated from municipal incineration plants by means of acid and/or alkaline leaching, of acid and/or alkaline leaching, Hydrometallurgy., 56(3), 269-292.
  • NIKOLIĆ, P., , P., MIHAJLOVIĆ, P.,MIHAJLOVIĆ, P., TODOROVIĆ, D.,TODOROVIĆ, D., 1996.. Far infrared and infrared properties of single crystal anglesite, Far infrared and infrared properties of single crystal anglesite, Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy., 52(2), 131-137.
  • NOWAK, P., P., LAAJALEHTO, K., , LAAJALEHTO, K., 2007. On the interpretation of the XPS spectra of adsorbed layers of flotation collectors. On the interpretation of the XPS spectra of adsorbed layers of flotation collectors-ethyl xanthate on metallic lead, Physicochemical Problems of Mineral Processing., 41, 107-116.
  • OKADA, T.,, T., TOYOTOYO, , Y., TANAKA, N., Y., TANAKA, N., MMATSUTO, T. ,ATSUTO, T., 2007. "Recovery of zinc and lead from fly ash from ash-melting and gasification-melting processes of MSW–Comparison and applicability of chemical leaching methods." Waste management 27(1): 69-80.
  • PROSSER, A. P., A. P., , 1996. "Review of uncertainty in the collection and Review of uncertainty in the collection and interpretation of leaching data interpretation of leaching data." Hydrometallurgy 41(2-3): 1193): 119-153.
  • QIN, W., L, LII, , W., LAN, Z., QIU, G., W., LAN, Z., QIU, G., 2007. Simulated small-scale pilot plant heap leaching of low scale pilot plant heap leaching of low-grade oxide zinc ore with grade oxide zinc ore with integrated selective extraction of zinc, Minerals Engineering., 20(7), 694(7), 694-700.
  • SCHRODER-WOLTHROOM, A.,WOLTHROOM, A., KKUITERTUITERT,, S., S., DDIJKMAN, H., IJKMAN, H., HHUISMAN, J.L., 2UISMAN, J.L., 2008. Application of sulfate reduction for the biological conversion of anglesite (PbSO 4) to galena (PbS), Hydrometallurgy., 94(1), 105-109.
  • SHENG, T., T., , 2013 Study on Study on Enhancement Sulfide Flotation Technology of Lead Oxide. Jiangxi University of Science and Enhancement Sulfide Flotation Technology of Lead Oxide. Jiangxi University of Science and Technology.22-33.
  • SUN, Y., SHEN, X.-Y., ZHAI, Y.Y., ZHAI, Y.-C., C., 2015. Thermodynamics and Kinetics of Extracting Zinc from Zinc Oxide Ore by the Ammonium Sulfate Roasting Method,International Journal of Minerals, Metallurgy, and Materials 22,467–475.
  • SZEKELY, J., J., , 1976. Gas-solid reactions, Academic Presss , New York.
  • TAKAOKA, , MM., ., KAWAI, T., TAKEDA, N., OSHITA, K., KAWAI, T., TAKEDA, N., OSHITA, K., 2002. ""Recovery of heavy metals in fly ash from ash melting Recovery of heavy metals in fly ash from ash melting furnace by solvent extraction by solvent extraction." Environmental Engineering Research 39: 403-412.
  • WANG, R., , TANG, M.TANG, M., , YANG, S.,YANG, S., ZHANG, W.ZHANG, W., , TANG, C.TANG, C., , HE, J.,HE, J., YANG, J., YANG, J., 2008. Leaching kinetics of low grade zinc Leaching kinetics of low grade zinc oxide ore in NH 3oxide ore in NH 3-NH 4 ClNH 4 Cl-H 2 O system,H 2 O system, Journal of Central South University of Technology., 15(5), 679Journal of Central South University of Technology., 15(5), 679-683.
  • WU, D., CUI, C.CUI, C., , WEN, S.,WEN, S., DENG, J.,DENG, J., 2016. Kinetics of Cerussite Leaching in Sulfamic Acid Solution, Journal of Chemical Kinetics of Cerussite Leaching in Sulfamic Acid Solution, Journal of Chemical Engineering of Japan., 49(5), 445-451.
  • WU, D., WEN, S., DENG, J., 2015. Leaching kinetics of cerussite using a new complexation reaction reagent, New Journal Leaching kinetics of cerussite using a new complexation reaction reagent, New Journal of Chemistry.,39(3), 1922-1929.
  • WU, Z.,, DREISINGER, D.B.,DREISINGER, D.B., URCH, H.,URCH, H., FASSBENDER, S.,FASSBENDER, S., 2014.2014. Fundamental study of lead recovery from cerussite Fundamental study of lead recovery from cerussite concentrate with methane sulfonic acid (MSA), Hydrometallurgy., 142, 23-35.
  • YUAN, W., LI, J., ZHANG, W., SAITO, F., 2012. Mechanochemical sulfidization of lead oxides by grinding with sulfur, Powder technology., 230, 63ogy., 230, 63-66.
  • ZHAO, Y., STANFORTH, R., 2000 Production of Zn powder by alkaline treatment of smithsonite Zn-Pb ores, Hydrometallurgy., 56(2), 237-249.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-178f52f5-b515-4d69-bbf3-d7e0ccee06fb
JavaScript jest wyłączony w Twojej przeglądarce internetowej. Włącz go, a następnie odśwież stronę, aby móc w pełni z niej korzystać.