Microstructure silica leached by NaOH from semi-burned rice husk ash for moisture adsorbent

• Autorzy: A’yuni D.Q. , Subagio A. , Hadiyanto H. , Kumoro A.C. , Djaeni M.

Identyfikatory

DOI

10.5604/01.3001.0015.0248

• Języki publikacji: EN

Abstrakty

EN

Purpose: This work aims to study the water vapor adsorption property of fine silica particles from semi-burned rice husk ash. The semi-burned rice husk ash is selected as the raw material since it contains high silica and is easily found as a by-product of pottery furnace combustion. Design/methodology/approach: The silica adsorbent from semi-burned rice husk ash was prepared through a sol-gel method using various NaOH concentrations. In doing so, the different pH precipitation was also observed. Here, the fine silica powder was obtained by pulverizing dry sol-gel. The product characterizations were conducted based on water adsorption capacity at different air relative humidity. Findings: The results show no significant effects of different treatments in the extraction and gelation process. The fine silica particles exhibit large porous surfaces with agglomerated nano-sized particles that formed pores. This porous structure is related to the distributions of pore size of each sample, which mostly obey the mesoporous characteristics. From sorption isotherm, weak adsorbent-adsorbate bonding was observed and demonstrated multilayer adsorption of mesoporous materials. Research limitations/implications: The study of water adsorption was carried out at room temperature, which can change at any time, even though has no significant effect on the humidity. However, it is needed to study the adsorption in an incubated area to receive a constant temperature. Practical implications: The products namely silica prepared from semi-burned rice husk ash show a high moisture uptake, especially at a high relative humidity region. This property can be comparable with the other silica preparation methods. So, this product can be a highly potential adsorbent for air or gas dehumidification systems. Originality/value: The silica-based semi-burned rice husk ash as a water adsorbent is more sustainable than commercial silica. This is a positive contribution to find a potentially develop water vapor adsorbent with good adsorption capacity. Besides, the synthesis process is a simple and low-cost process.

Słowa kluczowe

EN

microstructure; moisture absorption; silica; rice husk ash

PL

mikrostruktura; absorpcja wilgoci; krzemionka; popiół z łusek ryżu

• Wydawca: International OCSCO World Press
• Czasopismo: Archives of Materials Science and Engineering
• Rocznik: 2021
• Tom: Vol. 108, nr 1
• Strony: 5--15
• Opis fizyczny: Bibliogr. 46 poz.

Twórcy

autor

A’yuni D.Q.

• Department of Chemical Engineering, Faculty of Engineering, Universitas Diponegoro Jl. Prof. Sudharto Tembalang, Semarang, Central Java, Indonesia

autor

Subagio A.

• Department of Physics, Faculty of Science and Mathematics, Universitas Diponegoro Jl. Prof. Sudharto Tembalang, Semarang, Central Java, Indonesia

autor

Hadiyanto H.

• Department of Chemical Engineering, Faculty of Engineering, Universitas Diponegoro Jl. Prof. Sudharto Tembalang, Semarang, Central Java, Indonesia

autor

Kumoro A.C.

• Department of Chemical Engineering, Faculty of Engineering, Universitas Diponegoro Jl. Prof. Sudharto Tembalang, Semarang, Central Java, Indonesia

autor

Djaeni M.

• Department of Chemical Engineering, Faculty of Engineering, Universitas Diponegoro Jl. Prof. Sudharto Tembalang, Semarang, Central Java, Indonesia

• https://orcid.org/0000-0002-8002-6627

Bibliografia

• [1] Y. Artioli, Adsorption, in: Encyclopedia of Ecology, Five-Volume Set, 2008, 60-65.
• [2] H. Hu, K. Xu, Physicochemical technologies for HRPs and risk control, in: H. Ren, X. Zhang (Eds.), High-Risk Pollutants in Wastewater, Elsevier, 2020, 169-207. DOI: https://doi.org/10.1016/B978-0-12-816448- 8.00008-3
• [3] M. Djaeni, P.V. Bartels, J.P.M. Sanders, G. van Straten, A.J.B. van Boxtel, Computational fluid dynamics for multistage adsorption dryer design, Drying Technology 26/4 (2008) 487-502. DOI: https://doi.org/10.1080/07373930801929532
• [4] M. Djaeni, S.B. Sasongko, A. Prasetyaningrum, X. Jin, A.J. van Boxtel, Carrageenan drying with dehumidified air: Drying characteristics and product quality, International Journal of Food Engineering 8/3 (2012) 32. DOI: https://doi.org/10.1515/1556-3758.2682
• [5] P. Aprea, B. de Gennaro, N. Gargiulo, A. Peluso, B. Liguori, F. Iucolano, D. Caputo, Sr-, Zn- and Cd-exchanged zeolitic materials as water vapor adsorbents for thermal energy storage applications, Applied Thermal Engineering 106 (2016) 1217-1224. DOI: https://doi.org/10.1016/j.applthermaleng.2016.06.066
• [6] A. Galarneau, M. Nader, F. Guenneau, F. Di Renzo, A. Gedeon, Understanding the stability in water of mesoporous SBA-15 and M CM-41, Journal of Physical Chemistry C 111/23 (2007) 8268-8277. DOI: https://doi.org/10.1021/jp068526e
• [7] Qiongfen Yu, Huirong Zhao, Hong Zhao, Shengnan Sun, Xu Ji, Ming Li, Yunfeng Wang, Preparation of tobacco-stem activated carbon from using response surface methodology and its application for water vapor adsorption in solar drying system, Solar Energy 177 (2019) 324-336. DOI: https://doi.org/10.1016/j.solener.2018.11.029
• [8] A.J. Fletcher, Y. Uygur, K. Mark Thomas, Role of surface functional groups in the adsorption kinetics of water vapor on microporous activated carbons, Journal of Physical Chemistry C 111/23 (2007) 8349-8359. DOI: https://doi.org/10.1021/jp070815v
• [9] S.K. Wahono, A. Suwanto, D.J. Prasetyo, Hernawan, T.H. Jatmiko, K. Vasilev, Plasma activation on natural mordenite-clinoptilolite zeolite for water vapor adsorption enhancement, Applied Surface Science 483 (2019) 940-946. DOI: https://doi.org/10.1016/j.apsusc.2019.04.033
• [10] S. Saliba, P. Ruch, W. Volksen, T.P. Magbitang, G. Dubois, B. Michel, Combined influence of pore size distribution and surface hydrophilicity on the water adsorption characteristics of micro- and mesoporous silica, Microporous and Mesoporous Materials 226 (2016) 221-228. DOI: https://doi.org/10.1016/j.micromeso.2015.12.029
• [11] E. David, C. Sandru, A. Armeanu, Zeolitization characteristics of fly ash and its use to manufacture porous materials, Archives of Materials Science and Engineering 90/2 (2018) 56-67. DOI: https://doi.org/10.5604/01.3001.0012.0663
• [12] E.T. Wahyuni, R. Roto, F.A. Nissah, Mudasir, N.H. Aprilita, Modified silica adsorbent from volcanic ash for Cr(VI) anionic removal, Indonesian Journal of Chemistry 18/3 (2018) 428-433. DOI: https://doi.org/10.22146/ijc.26905
• [13] A. Sdiri, T. Higashi, S. Bouaziz, M. Benzina, Synthesis and characterization of silica gel from siliceous sands of southern Tunisia, Arabian Journal of Chemistry 7/4 (2014) 486-493. DOI: https://doi.org/10.1016/j.arabjc.2010.11.007
• [14] S. Sun, Q. Yu, M. Li, H. Zhao, C. Wu, Preparation of coffee-shell activated carbon and its application for water vapor adsorption, Renewable Energy 142 (2019) 11-19. DOI: https://doi.org/10.1016/j.renene.2019.04.097
• [15] R. Wang, Y. Amano, M. Machida, Surface properties and water vapor adsorption-desorption characteristics of bamboo-based activated carbon, Journal of Analitycal and Applied Pyrolysis 104 (2013) 667-674. DOI: https://doi.org/10.1016/j.jaap.2013.04.013
• [16] M. Thommes, K. Kaneko, A.V. Neimark, J.P. Olivier, F. Rodriguez-Reinoso, J. Rouquerol, K.S.W. Sing, Physisorption of gases, with special reference to the evaluation of surface area and pore size distribution (IUPAC Technical Report), Pure and Applied Chemistry 87/9-10 (2015) 1051-1069. DOI: https://doi.org/10.1515/pac-2014-1117
• [17] K.M. Kim, H.T. Oh, S.J. Lim, K. Ho, Y. Park, C.H. Lee, Adsorption Equilibria of Water Vapor on Zeolite 3A, Zeolite 13X, and Dealuminated y Zeolite, Journal of Chemical & Engineering Data 61/4 (2016) 1547- 1554. DOI: https://doi.org/10.1021/acs.jced.5b00927
• [18] A. Centineo, H.G.T. Nguyen, L. Espinal, J.C. Horn, S. Brandani, An experimental and modelling study of water vapour adsorption on SBA-15, Microporous and Mesoporous Materials 282 (2019) 53-72. DOI: https://doi.org/10.1016/j.micromeso.2019.03.018
• [19] M. Djaeni, P. Bartels, J. Sanders, G. van Straten, A.J. B. van Boxtel, Process integration for food drying with air dehumidified by zeolites, Drying Technology 25/1 (2007) 225-239. DOI: https://doi.org/10.1080/07373930601161096
• [20] M. Djaeni, A.M. Perdanianti, The study explores the effect of onion (allium cepa l.) drying using hot air dehumidified by activated carbon, silica gel and zeolite, Journal of Physics: Conference Series 1295 (2019) 012025. DOI: https://doi.org/10.1088/1742- 6596/1295/1/012025
• [21] L. Xin, L. Huiling, H. Siqi, L. Zhong, Dynamics and isotherms of water vapor sorption on mesoporous silica gels modified by different salts, Kinetics and Catalysis 51/5 (2010) 754-761. DOI: https://doi.org/10.1134/S0023158410050186
• [22] H. Negishi, A. Miyamoto, A. Endo, Preparation of thick mesoporous silica coating by electrophoretic deposition with binder addition and its water vapor adsorption-desorption properties, Microporous and Mesoporous Materials 180 (2013) 250-256. DOI: https://doi.org/10.1016/j.micromeso.2013.06.040
• [23] P. Velmurugan, J. Shim, K.-J. Lee, M. Cho, S.-S. Lim, S.-K. Seo, K.-M. Cho, K.-S. Bang, B.-T. Oh, Extraction, characterization, and catalytic potential of amorphous silica from corn cobs by sol-gel method, Journal of Industrial and Engineering Chemistry 29 (2015) 298-303. DOI: https://doi.org/10.1016/j.jiec.2015.04.009
• [24] R.A. Bakar, R. Yahya, S.N. Gan, Production of High Purity Amorphous Silica from Rice Husk, Procedia Chemistry 19 (2016) 189-195. DOI: https://doi.org/10.1016/j.proche.2016.03.092
• [25] T.H. Liou, C.C. Yang, Synthesis and surface characteristics of nanosilica produced from alkali-extracted rice husk ash, Materials Science and Engineering: B 176/7 (2011) 521-529. DOI: https://doi.org/10.1016/j.mseb.2011.01.007
• [26] A. Mahmud, P.S.M. Megat-Yusoff, F. Ahmad, A.A. Farezzuan, Acid leaching as efficient chemical treatment for rice husk in production of amorphous silica nanoparticles, ARPN Journal of Engineering and Applied Sciences 11/22 (2016) 13384-13388.
• [27] H.X. Nguyen, N.T.T. Dao, H.T.T. Nguyen, A.Q.T. Le, Nanosilica synthesis from rice husk and application for soaking seeds, IOP Conference Series: Earth and Environmental Science 266/1 (2019) 012007. DOI: https://doi.org/10.1088/1755-1315/266/1/012007
• [28] S. Shekar, M. Sander, R.C. Riehl, A.J. Smith, A. Braumann, M. Kraft, Modelling the flame synthesis of silica nanoparticles from tetraethoxysilane, Chemical Engineering Science 70 (2012) 54-66. DOI: https://doi.org/10.1016/j.ces.2011.06.010
• [29] H. Yoo, J. Pak, Synthesis of highly fluorescent silica nanoparticles in a reverse microemulsion through double-layered doping of organic fluorophores, Journal of Nanoparticle Research 15/5 (2013) 1609. DOI: https://doi.org/10.1007/s11051-013-1609-2
• [30] S. Azat, A.V. Korobeinyk, K. Moustakas, V.J. Inglezakis, Sustainable production of pure silica from rice husk waste in Kazakhstan, Journal of Cleaner Production 217 (2019) 352-359. DOI: https://doi.org/10.1016/j.jclepro.2019.01.142
• [31] K.V. Selvakumar, A. Umesh, P. Ezhilkumar, S. Gayatri, P. Vinith, V. Vignesh, Extraction of silica from burnt paddy husk, International Journal of ChemTech Research 6/9 (2014) 4455-4459.
• [32] R.R. Zaky, M.M. Hessien, A.A. El-midany, M.H. Khedr, Preparation of silica nanoparticles from semi-burned rice straw ash, Powder Technology 185 (2008) 31-35. DOI: https://doi.org/10.1016/j.powtec.2007.09.012 [33] P.M. Doran, Introduction to Engineering Calculations, in: Bioprocess Engineering Principles, Second Edition, Academic Press, Oxford, 2013, 13-44.
• [34] C. Bourgault, P. Lessard, C. Remington, C.C. Dorea, Experimental Determination of Moisture Sorption Isotherm of Fecal Sludge, Water 11/2 (2019) 303. DOI: https://doi.org/10.3390/w11020303
• [35] L. Greenspan, Humidity fixed points of binary saturated aqueous solutions, Journal of Research of the National Bureau of Standards ‒ A. Physics and Chemistry 81/1 (1977) 89-96.
• [36] S.B. Daffalla, H. Mukhtar, M.S. Shaharun, Characte-rization of adsorbent developed from rice husk: Effect of surface functional group on phenol adsorption, Journal of Applied Science 10/12 (2010) 1060-1067. DOI: https://doi.org/10.3923/jas.2010.1060.1067
• [37] M.M. Saravanan, M. Sivaraja, Mechanical behavior of concrete modified by replacement of cement by rice husk ash, Brazilian Archives of Biology and Technology 59/S2 (2016) 1-11. DOI: http://dx.doi.org/10.1590/1678-4324-2016161072
• [38] I.M. Joni, L. Nulhakim, M. Vanitha, C. Panatarani, Characteristics of crystalline silica (SiO2) particles prepared by simple solution method using sodium silicate (Na2SiO3) precursor, Journal of Physics: Conference Series 1080 (2018) 012006. DOI: https://doi.org/10.1088/1742-6596/1080/1/012006
• [39] I.C. Medeiros-Costa, C. Laroche, J. Pérez-Pellitero, B. Coasne, Characterization of hierarchical zeolites: Combining adsorption/intrusion, electron microscopy, diffraction and spectroscopic techniques, Microporous and Mesoporous Materials 287 (2019) 167-176. DOI: https://doi.org/10.1016/j.micromeso.2019.05.057
• [40] J. Zecevic, C.J. Gommes, H. Friedrich, P.E. de Jongh, K.P. de Jong, Mesoporosity of Zeolite Y: Quantitative Three-Dimensional Study by Image Analysis of Electron Tomograms, Angewandte Chemie International Edition 51/17 (2012) 4213-4217. DOI: https://doi.org/10.1002/anie.201200317
• [41] K.S.W. Sing, R.T. Williams, Physisorption hysteresis loops and the characterization of nanoporous materials, Adsorption Science and Technology 22/10 (2004) 773- 782. DOI: https://doi.org/10.1260/0263617053499032
• [42] Y. Liu, Y. Guo, Y. Zhu, D. An, W. Gao, Z. Wang, Y. Ma, Z. Wang, A sustainable route for the preparation of activated carbon and silica from rice husk ash, Journal of Hazardous Materials 186/2-3 (2011) 1314-1319. DOI: https://doi.org/10.1016/j.jhazmat.2010.12.007
• [43] Musyarofah, S. Soontaranon, W. Limphirat, Triwikantoro, S. Pratapa, XRD, WAXS, FTIR, and XANES studies of silica-zirconia systems, Ceramics International 45/12 (2019) 15660-15670. DOI: https://doi.org/10.1016/j.ceramint.2019.05.078
• [44] P. Lu, Y. Hsieh, Highly pure amorphous silica nano-disks from rice straw, Powder Technology 225 (2012) 149-155. DOI: https://doi.org/10.1016/j.powtec.2012.04.002
• [45] T. Liou, Preparation and characterization of nano-structured silica from rice husk, Materials Science and Engineering: A 364/1-2 (2004) 313-323. DOI: https://doi.org/10.1016/j.msea.2003.08.045
• [46] H. Zhang, W. Gu, M.J. Li, Z.Y. Li, Z.J. Hu, W.Q. Tao, Experimental study on the kinetics of water vapor sorption on the inner surface of silica nano-porous materials, International Journal of Heat and Mass Transfer 78 (2014) 947-959. DOI: https://doi.org/10.1016/j.ijheatmasstransfer.2014.07.047