Preparation and characterization of cobalt and copper oxide nanocrystals

• Autorzy: Moharram A. H.

Identyfikatory

DOI

10.2478/msp-2019-0048

• Języki publikacji: EN

Abstrakty

EN

Copper oxide and cobalt oxide (Co₃O₄, CuO) nanocrystals (NCs) have been successfully prepared using microwave irradiation. The obtained powders of the nanocrystals (NCs) were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric (TGA) analysis and Fourier-transform infrared spectroscopy. The obtained results confirm the presence of both nanooxides which have been produced during chemical precipitation using microwave irradiation. TEM micrographs have shown that the obtained nanocrystals are characterized by high dispersion and narrow size distribution. The results of X-ray diffraction confirmed those obtained from the transmission electron microscope. Optical absorption analysis indicated the direct band gap for both kinds of the nanocrystals.

Słowa kluczowe

EN

nanoparticles synthesis; metal oxides; microwave ovens; TEM micrographs; X-ray diffraction

• Wydawca: De Gruyter
• Czasopismo: Materials Science Poland
• Rocznik: 2019
• Tom: Vol. 37, No. 3
• Strony: 347--352
• Opis fizyczny: Bibliogr. 20 poz., rys.

Twórcy

autor

Moharram A. H.

• Physics Dept., College of Science & Arts, King Abdulaziz Univ., Jeddah, Saudi Arabia

Bibliografia

• [1] HENGLEIN A., Chem. Rev., 89 (1989), 1861.
• [2] KAMPMEIER J., RASHAD M., WOGGON U., RUTH M., MEIER C., SCHIKORA D., LISCHKA K., PAWLIS A., Phys. Rev. B, 85 (2012), 155405.
• [3] RASHAD M., PALUGA M., PAWLIS A., LISCHKA K., SCHIKORA D., ARTEMYEV M. V., WOGGON U., Phys. Stat. Sol. C, (2010), 1.
• [4] IJAZ F., SHAHID S., KHAN S.A., AHMAD W., ZAMAN S., Tropical J. Pharmac. Res., 16 (2017), 743.
• [5] POIZOT P., LARUELLE S., GRUGEON S., DUPONT L., Nature, 407 (2000), 496.
• [6] SASKIA A.G., Chem. Soc. Rev., 269 (1997), 233.
• [7] JADHAV S., GAIKWAD S., NIMSE M., RAJBHOJ A., J. Clust. Sci., 22 (2011), 121.
• [8] SANKAR R., MANIKANDAN P., MALARVIZHI V., FATHIMA T., SHIVASHANGARI K.S., RAVIKUMAR V., Spectrochim. Acta Mol. Biomol. Spectrosc., 121 (2014) 746.
• [9] YAO W.T., YU S.H., ZHOU Y., JIANG J., WU Q.S., ZHANG L., JIANG J., J. Phys. Chem. B, 109 (2005), 14016.
• [10] KLUG H., ALEXANDER L., X-ray Diffraction Procedures, Wiley, New York, 1962, p. 125.
• [11] DAS SK, KHAN MMR, GUHAB AK, NASKAR N., Green Chem., 15 (2013), 2548.
• [12] SAIF S., TAHIR A., ASIM T., CHEN Y., Nanoma., 6 (2016), 1.
• [13] MOTE V.D., PURUSHOTHAM Y., DOLE B.N., J. Theor. Appl. Phys., 6 (2012).
• [14] MANIMARAN R., PALANIRADJA K., ALAGUMURTHI N., SENDHILNATHAN S., HUSSAIN J., Appl. Nanosci., 4 (2014), 163.
• [15] SOCRATES G., Group Frequencies – Tables and Charts, 2nd ed., John Wiley and Sons, England, 1994.
• [16] PANKOVE J.I., Optical processes in semiconductors. Englewood Cliffs, Prentice-Hall, New York, 1971.
• [17] SANTRA K., SARKAR C.K., MUKHERJEE M. K., COSH B., Thin Solid Films, (1992) 213.
• [18] ZHU J.W., CHEN H.Q., LIU H.B., YANG X.J., LU L.D., WANG X., Mater Sci. Eng. A, 384 (2004), 172.
• [19] DRASOVEAN R., J. Non-Cryst. Solids, 352 (2006), 1479.
• [20] GU F., KI C., HU Y., ZHANG L., J. Cryst. Growth, 304 (2007), 369.

Uwagi

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).