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Purification And Separation Of Rare Earth Elements From CCFL With Extraction Chromatography

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Treść / Zawartość
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Warianty tytułu
PL
Oczyszczanie i separacja metali ziem rzadkich z lamp fluorescencyjnych z zimną katodą (CCFL) przy użyciu chromatografii ekstrakcji
Języki publikacji
EN
Abstrakty
EN
In this study, Amberite XAD-7HP was used as the solvent-impregnated resin to separate each REE from the standard solution, which was mixed with the REEs (e.g., La Eu, Tb, Y and Ba). About 100 ppm of each of the REEs was separated from DI water using extraction chromatography. REEs were separated by extraction chromatography using Amberite XAD-7HP resin, the changes in the pH values of the HCl and HClO4 were between 0.2 N and 5 N, and the extraction rate of the solution was between 0.5 and 3 ml/min. The La solution with the separated REEs was leached. The solid-state REEs were annealed between 1083K. The extraction result was analyzed with ICP-AES and an X-ray diffractometer. Each REE was successfully separated with HCl and HClO4 with pH values between 0.1 N and 3 N and with extraction rate between 1.0 m/min and 3.0 m/min.
Twórcy
autor
  • Incheon National University, Incheon, Korea
Bibliografia
  • [1] http://www.ucoreraremetals.com
  • [2] Rare Earth Elements-End Use and Recyclability, Scientific Investigations Report 2011, USGS, 5094 (2011).
  • [3] China’s Rare-Earth Industry, Open-File Report 2011, USGS, 1042 (2011).
  • [4] http://www.kores.net
  • [5] D. F. Peppard, J. P. Faris, P. R. Gray, G. W. Mason, J. Phys. Chem. 57, 294 (1953).
  • [6] D. F. Peppard, G. W. Mason, J. Laier, W. J. Driscoll, J. Inorg. Nucl. Chem. 4, 334 (1957).
  • [7] D. F. Peppard, G. W. Mason, J. I. Hucher, J. Inorg. Nucl. Chem. 18, 245 (1961).
  • [8] P. Miranda Jr., M. F. Ma’duar, G. Vicentini, Le’a B. Zinner, J. Alloys. Compd. 344, 46 (2002).
  • [9] L. Deqian, W. Xiong, L. Daozhi, X. Yanfeng, L. Suxian, W. Zhonghuai, L. Han, J. Enyui, Solvent Extraction 3, International Solvent Conference, Lie‘ge (1980).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-106a09ca-037a-4ade-952e-804ac4f26d4f
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