Comparison of the MWCNTs-Rh and MWCNTs-Re Carbon-Metal Nanocomposites Obtained in High-Temperature

• Autorzy: Dobrzańska-Danikiewicz A. D. , Łukowiec D. , Cichocki D. , Wolany W.

Identyfikatory

DOI

10.1515/amm-2015-0348

Warianty tytułu

PL

Porównanie węglowo-metalowych nanokompozytów MWCNTs-Rh i WCNTs-Re otrzymanych metodą wysokotemperaturową

• Języki publikacji: EN

Abstrakty

EN

Carbon-metal nanocomposites consisting of multiwalled carbon nanotubes coated with rhodium or rhenium nanoparticles by the high-temperature method were fabricated during the research undertaken. Multiwalled carbon nanotubes fabricated by Catalytic-Chemical Vapour Deposition (CCVD) were used in the investigations. Multiwalled carbon nanotubes functionalisation in acid or in a mixture of acids was applied to deposit rhodium or rhenium nanoparticles onto the surface of carbon nanotubes, and then the material was placed in a solution being a precursor of metallic nanoparticles. The material prepared was next subjected to high-temperature reduction in the atmosphere of argon and/or hydrogen to deposit rhodium or rhenium nanoparticles onto the surface of multiwalled carbon nanotubes. The investigations performed include, respectively: fabrication of a CNT-NPs (Carbon NanoTube-NanoParticles) nanocomposite material; the characterisation of the material produced including examination of the structure and morphology, and the assessment of rhodium and/or rhenium nanoparticles distribution on the surface of carbon nanotubes. Micro- and spectroscopy techniques were employed to characterise the structure of the nanocomposites obtained.

PL

W ramach wykonanych badań wytworzono węglowo-metalowe nanokompozyty składające się z wielościennych nanorurek węglowych pokrytych nanocząsteczkami rodu lub renu metodą wysokotemperaturową. W badaniach wykorzystano wielościenne nanorurki weglowe wytworzone metodą katalityczno-chemicznego osadzania z fazy gazowej (ang.: Chemical Catalytic Vapor Deposition – CCVD). W celu osadzenia nanocząsteczek rodu lub renu na powierzchni nanorurek węglowych zastosowano funkcjonalizację wielościennych nanorurek węglowych w kwasie lub mieszaninach kwasów, następnie materiał umieszczono w roztworze będącym prekursorem nanocząsteczek metalicznych. Przygotowany materiał poddano następnie redukcji wysokotemperaturowej w atmosferze argonu i/lub wodoru w celu osadzenia nanocząsteczek rodu lub renu na powierzchni wielościennych nanorurek węglowych. Wykonane badania obejmują kolejno: wytworzenie materiału nanokompozytowego typu CNT-NPs (ang.: Carbon NanoTube-NanoParticles), scharakteryzowanie wytworzonego materiału obejmujące badanie jego struktury i morfologii oraz ocenę rozmieszczenia nanocząsteczek rodu i/lub renu na powierzchni nanorurek węglowych. Dla scharakteryzowania struktury otrzymanych nanokompozytów zastosowano techniki mikroi spektroskopowe.

Słowa kluczowe

EN

nancomposites; carbon nanotube; CCVD; metal nanoparticles

PL

nanokompozyty; nanorurki węglowe; CCVD; nanocząstki metali

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2015
• Tom: Vol. 60, iss. 3A
• Strony: 2053--2060
• Opis fizyczny: Bibliogr. 24 poz., diagr., rys., tab., wykr.

Twórcy

autor

Dobrzańska-Danikiewicz A. D.

• Faculty of Mechanical Engineering, Silesian University of Technology, 18a Konarskiego Str., 44-100 Gliwice, Poland

autor

Łukowiec D.

• Faculty of Mechanical Engineering, Silesian University of Technology, 18a Konarskiego Str., 44-100 Gliwice, Poland

autor

Cichocki D.

• Faculty of Mechanical Engineering, Silesian University of Technology, 18a Konarskiego Str., 44-100 Gliwice, Poland

autor

Wolany W.

• Faculty of Mechanical Engineering, Silesian University of Technology, 18a Konarskiego Str., 44-100 Gliwice, Poland

Bibliografia

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• [21] A. D. Dobrzańska-Danikiewicz, D. Łukowiec, W. Wolany, D. Cichocki, Comperative anaysis of the fabrication methods and structure of the selected CNTs-NPs nanocomposites, Paper of FiMPART’15 conference (in print).
• [22] Patent application no. 411443, Polish Patent Office.
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• [24] A. D. Dobrzańska-Danikiewicz, D. Cichocki, D. Łukowiec, The MWCNTs-Rh nanocomposite obtained by the new high-temperature method, Archives of Metallurgy and Materials 60/2, 1057-1063 (2015).

Uwagi

EN

The works have been implemented within the framework of the ELCON ANO project headed by Prof. A. D. Dobrzańska- Danikiewicz, funded by the Polish National Science Centre in the framework of the “OPUS” competitions. The project was awarded a subsidy under the decision DEC-2011/03/B/ST8/06070.DawidCichocki and WeronikaWolany is holder of scholarship from project “Scholarship and Internship Fund for the development of knowledge transfer in the region” cofinanced by the European Union under the European Fund.