PL EN


Preferencje help
Widoczny [Schowaj] Abstrakt
Liczba wyników
Tytuł artykułu

Multiphase extraction of ephedrine from Pinellia ternata using bionic liquid-modified polymer

Treść / Zawartość
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Multiphase extraction (MPE) was applied as a developed, convenient and efficient method in separation of ephedrine from Pinellia ternata. Firstly, in order to increase the adsorption efficiency, bionic liquid-modified polymer was created. Comparing the effects of all sorbents under variables conditions, the highest amount of 5.8 mg/g can be adsorbed on dual imidazole ionic liquid modified polymer (Im-Im-Poly) in methanol/water (70:30, v/v) solution at 25°C within 30.0 min. Then the Im-Im-Poly was applied in MPE, after 7 times repetition of extraction, around 1.0 mg/g of ephedrine from Pinellia ternata was detected. After washing by water, ethanol and methanol, and elution by methanol/acetic acid (99.0:1.0, v/v), ephedrine was successfully separated.
Rocznik
Strony
13--19
Opis fizyczny
Bibliogr. 23 poz., rys., tab.
Twórcy
autor
  • Yangtze University, College of Chemistry and Environmental Engineering, Jingzhou, Hubei, 434023 China
autor
  • Yangtze University, College of Chemistry and Environmental Engineering, Jingzhou, Hubei, 434023 China
autor
  • Yangtze University, College of Chemistry and Environmental Engineering, Jingzhou, Hubei, 434023 China
autor
  • Inha University, Department of Chemistry and Chemical Engineering, Incheon 402751, Korea
Bibliografia
  • 1. Buyel, J.F. (2018). Plants as sources of natural and recombinant anti-cancer agents. Biotechnol. Adv. 36, 506–520. DOI: org/10.1016/j.biotechadv.2018. 02.002.
  • 2. Ložienė, K., Švedienė, J., Paškevičius, A., Raudonienė, V., Sytar, O. & Kosyan, A. (2018). Infl uence of plant origin natural α-pinene with different enantiomeric composition on bacteria, yeasts and fungi. Fitoterapia 127, 20–24. DOI: org/10.1016/ j.fi tote.2018.04.013
  • 3. Unuofin, J.O., Otunola, G.A. & Afolayan, A.J. (2018). Evaluation of acute and subacute toxicity of whole-plant aqueous extract of Vernonia mespilifolia Less. in Wistar rats. J. Integr. Med. 16, 335–341 DOI: org/10.1016/j.joim.2018.07.003.
  • 4. Dubey, N.K., Dwivedy, A.K., Chaudhari, A.K. & Das, S. (2018). Chapter 13-common toxic plants and their forensic signifi cance, in: Natural Products and Drug Discovery, Elsevier Ltd., Amsterdam, pp. 349–374. DOI: org/10.1016/B978-0-08-102081-4.00013-7.
  • 5. Ng, A.W.T., Poon, S.L., Huang, M.N., Lim, J.Q., Boot, A., Yu, W., Suzuki, Y., Thangaraju, S., Ng, C.C.Y., Tan, P., Pang, S., Huang, H., Yu, M., Lee, P., Hsieh, S., Chang, A.Y., Teh, B.T. & Rozen, S.G. (2017). Aristolochic acids and their derivatives are widely implicated in liver cancers in Taiwan and throughout Asia. Sci. Transl. Med. 9, eaan6446. DOI: 10.1126/scitranslmed.aan6446.
  • 6. Alsufyani, H.A. & Docherty, J.R. (2018). Direct and indirect effects of ephedrine on heart rate and blood pressure in vehicle-treated and sympathectomised male rats. Eur. J. Pharmacol. 825, 34–38. DOI: org/10.1016/j.ejphar.2018.02.021.
  • 7. Zhang, X.C., Pharm, N.F., Haronian, T. & Hack, J. (2017). Postoperative anticholinergic poisoning: concealed complications of a commonly used medication. J. Emerg. Med. 53, 520–523. DOI: org/10.1016/j.jemermed.2017.05.003.
  • 8. Georgescu, B.E., Branger, C., Iordache T, Iovu, H., Vitrik, O.B., Dyshlyuk, A.V., Sarbu, A. & Brisset, H. (2018). Application of unusual on/off electrochemical properties of a molecularly imprinted polymer based on an EDOT-thiophene precursor for the detection of ephedrine. Electrochem. Commun. 94, 45–48. DOI: org/10.1016/j.elecom.2018.08.004.
  • 9. Taghvimi, A. & Hamishehkar, H. (2017). Carbon coated magnetic nanoparticles as a novel magnetic solid phase extraction adsorbent for simultaneous extraction of methamphetamine and ephedrine from urine samples. J. Chromatogr. B 1041-1042, 113–119. DOI: org/10.1016/j.jchromb.2016.11.039.
  • 10. Zhong, S., Kong, Y., Zhou, L., Zhou, C., Zhang, X & Wang, Y. (2014). Effi cient conversion of myricetin from Ampelopsis grossedentata extracts and its purification by MIPSPE. J. Chromatogr. B 945–946, 39–45. DOI: org/10.1016/j.jchromb.2013.11.036.
  • 11. Deng, D.L., Zhang, J.Y., Chen, C., Hou, X.L., Su, Y.Y. & Wu, L. (2012). Monolithic molecular imprinted polymer fiber for recognition and solid phase microextraction of ephedrine and pseudoephedrine in biological samples prior to capillary electrophoresis analysis. J. Chromatogr. A 1219, 195–200. DOI: org/10.1016/j.chroma.2011.11.016.
  • 12. Wang, L., Yan, H., Yang, C., Li, Z. & Qiao, F. (2016). Synthesis of mimic molecularly imprinted ordered mesoporous silica adsorbent by thermally reversible semicovalent approach for pipette-tip solid-phase extraction-liquid chromatography fluorescence determination of estradiol in milk. J. Chromatogr. A 1456, 58–67. DOI: org/10.1016/j.chroma.2016.06.010.
  • 13. Han, Y., Yang, C., Zhou, Y., Han, D. & Yan, H. (2017). Ionic liquid-hybrid molecularly imprinted material-filter solid-phase extraction coupled with HPLC for determination of 6-benzyladenine and 4-chlorophenoxyacetic acid in bean sprouts. J. Agr. Food Chem. 65, 1750–1757. DOI: 10.1021/acs.jafc.6b03922.
  • 14. Zhang, H., Yuan, Y., Sun, Y., Niu, C., Qiao, F. & Yan, H. (2018). An ionic liquid-magnetic graphene composite for magnet dispersive solid-phase extraction of triazine herbicides in surface water followed by high performance liquid chromatography. Analyst 143, 175–181. DOI: 10.1039/c7an01290j.
  • 15. Huang, D., Zheng, H., Liu, Z., Bao, A. & Li, B. (2018). Extraction of rubidium and cesium from brine solutions using a room temperature ionic liquid system containing 18-crown-6. Pol. J. Chem. Technol. 20, 40–46. DOI: org/10.2478/pjct-2018-0021.
  • 16. Chen, H., Yuan, Y., Xiang, C., Yan, H., Han, Y. & Qiao, F. (2016). Graphene/multi-walled carbon nanotubes functionalized with an amine-terminated ionic liquid for determination of (Z)-3-(chloromethylene)-6-fluorothiochroman-4-one in urine. J. Chromatogr. A 1474, 23–31. DOI.org/10.1016/j.chroma.2016.10.076.
  • 17. Wang, X., Lin, L., Xie, J., Yan, X., Xiao, W. & Tian, M. (2018). Adsorption efficiency of pentafl uorobenzene on ionic liquids-based silicas. Pol. J. Chem. Technol. 20, 47–52. DOI: 10.2478/pjct-2018-0037.
  • 18. Fang, L., Tian, M., Yan, X. & Xiao, W. (2018). Isolation of aflatoxin B1 from moldy foods by solid-phase extraction combined with bifunctional ionic liquid-based silicas. J. Anal. Methods Chem. 2018, 8427580. DOI: org/10.1155/2018/8427580.
  • 19. Yang, S., Zhang, Q., Hu, Y., Ding, G. & Wang, J. (2019). Synthesis of maleimide modified imidazole derivatives and their application in one-component epoxy resin systems. Mater. Lett. 234, 379–383. DOI: org/10.1016/j.matlet.2018.09.147.
  • 20. Gevaerd, A., Blaskievicz, S.F., Zarbin, A.J.G., Orth, E.S., Bergamini, M.F. & Marcolino-Junior, L.H. (2018). Nonenzymatic electrochemical sensor based on imidazole-functionalized graphene oxide for progesterone detection. Biosensors Bioelectron. 112, 108–113. DOI: 10.1016/j.bios.2018.04.044.
  • 21. Zhang, Y., Zhang, T., Guo, C., Hou, S., Hua, Z., Lv, J., Zhang, Y. & Xu, J. (2018). Development and application of the diffusive gradients in thin fi lms technique for simultaneous measurement of methcathinone and ephedrine in surface river water. Sci. Total Environ. 618, 284–290. DOI: org/10.1016/j.scitotenv.2017.11.068.
  • 22. Tian, S., Guo, Z., Zhang, X. & Wu, X. (2013). Synthesis of molecularly imprinted co-polymers for recognition of ephedrine. Anal. Methods 5, 5179–5187. DOI: 10.1039/C3AY41202D.
  • 23. Dong, X., Wang, W., Ma, S., Sun, H., Li, Y. & Guo, J. (2005). Molecularly imprinted solid-phase extraction of (-)-ephedrine from Chinese Ephedra. J. Chromatogr. A 1070, 125–130. DOI: org/10.1016/j.chroma.2005.03.017.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-0ce1b5af-eeca-47d5-ba58-b4dad9ce4296
JavaScript jest wyłączony w Twojej przeglądarce internetowej. Włącz go, a następnie odśwież stronę, aby móc w pełni z niej korzystać.