Effect of Ultrasonic-Assisted Preparation of Powders on Synthesis of Rare Earth Zirconates

• Autorzy: Niemiec D. , Mikuśkiewicz M.

Identyfikatory

DOI

10.24425/amm.2020.131744

• Języki publikacji: EN

Abstrakty

EN

The aim of the research was to determine the effect of sonochemical treatments on homogenization of powders as well as phase composition and thermal stability of sinters. The compounds were prepared from Eu₂O₃ and ZrO₂ powders, weighed in the mass ratio 1:1. Initially ultrasound treatment was applied. 750-Watt ultrasonic processor VCX-750 equipped with sealed converter VC-334 and horn 630-0219 with the diameter of 13 mm (Sonics & Materials, Inc.) was used as a source of ultrasound. Applied ultrasound frequency was 20 kHz, power density was controlled in the range from 75 W/cm² to 340 W/cm². Investigated compounds were synthesized via solid-state reaction (SSR). The Differential Scanning Calorimetry (DSC) was used in order to investigate the effect of sonochemical treatment on the synthesis of prepared mixtures the powders particle size distribution was analyzed. Ultrasound treatment what wasn’t never been reported before.

Słowa kluczowe

EN

pyrochlore; ultrasonic; TBC

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2020
• Tom: Vol. 65, iss. 1
• Strony: 417--422
• Opis fizyczny: Bibliogr. 19 poz., fot., rys.

Twórcy

autor

Niemiec D.

• Silesian University of Technology, 8 Krasińskiego Str., 40-019 Katowice, Poland

autor

Mikuśkiewicz M.

• Silesian University of Technology, 8 Krasińskiego Str., 40-019 Katowice, Poland

Bibliografia

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Uwagi

EN

1. We gratefully acknowledge the financial support of the National Science Centre, Poland under grant number 2016/21/D/ST8/01687.

PL

2. Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2020).