Alternative, Direct Synthesis Method of the Ceramic Solid Solutions Based on BaTiO3 Through a High Energy Ball Milling

• Autorzy: Bąk W. , Dulian P. , Garbarz-Glos B. , Czekaj D. , Lisińska-Czekaj A.

Identyfikatory

DOI

10.24425/amm.2020.132824

• Języki publikacji: EN

Abstrakty

EN

Polycrystalline samples BaTiO₃ and the solid solutions Ba_0.9 Sr_0.1 TiO₃, _0.9 Sr_0.1 Ti_0.9 Sn_0.1 O₃, Ba_0.9 Sr_0.1 Ti_0.8 Sn_0.2 O₃ were obtained by means of a mechanochemical treatment based on the high-energy ball milling technique and next a high temperature solid state reaction method. The influence of synthesis condition on microstructural, dielectric and ferroelectric properties of obtained solid solutions were investigated. The structure and morphology of the investigated samples were characterized by an X-ray diffraction (XRD) and scanning electron microscopy (SEM). The characterization of electrical properties of the ceramics within the temperature range from –130°C to 250°C were performed by means of a dielectric spectroscopy method at the frequency ranging from 0.1 Hz to10 MHz. The diffusion of the paraelectric – ferroelectric phase transition and dielectric relaxation for ceramic samples are described.

Słowa kluczowe

EN

ceramics; mechanochemical synthesis; dielectric properties; phase transitions; ferroelectrics

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2020
• Tom: Vol. 65, iss. 2
• Strony: 805--810
• Opis fizyczny: Bibliogr. 26 poz., fot., rys.

Twórcy

autor

Bąk W.

• Pedagogical University, Institute of Technology, 2 Podchorążych Str., 30-084 Kraków, Poland

autor

Dulian P.

• Cracow University of Technology, Faculty of Chemical Engineering and Technology, 24 Warszawska Str., 31-155 Kraków, Poland

autor

Garbarz-Glos B.

• Pedagogical University, Institute of Technology, 2 Podchorążych Str., 30-084 Kraków, Poland

autor

Czekaj D.

• Gdańsk University of Technology, Department of Materials Engineering and Welding, Faculty of Mechanical Engineering, 11/12 G.Narutowicza Str., 80-233, Gdańsk, Poland

autor

Lisińska-Czekaj A.

• Gdańsk University of Technology, Department of Materials Engineering and Welding, Faculty of Mechanical Engineering, 11/12 G.Narutowicza Str., 80-233, Gdańsk, Poland

Bibliografia

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Uwagi

PL

Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2020).