Thallium I phenylsuccinic acid coordination polymer as precursor for preparation of thallium (III) oxide nano structures by direct thermal decomposition

• Autorzy: Soltanian M J , Tabaroki S

Identyfikatory

DOI

10.2478/s13536-013-0151-3

• Języki publikacji: EN

Abstrakty

EN

A new thallium (I) coordination polymer [Tl(PsucH)]n (PsucH = phenylsuccinic acid) has been synthesized and characterized by single crystal X-Ray analysis, elemental analysis and IR spectroscopy. The single crystal X-Ray analysis shows that this polymer is 2-D along a axis. Flower-like nanostructure thallium (III) oxide, Tl2O3 has been prepared by direct thermal decomposition of thallium (I) coordination polymer. The nanostructure was characterized by scanning electron microscopy (SEM), X-Ray powder diffraction (XRD) and IR spectroscopy. The thermal stability of the Tl2O3 nanostructure was studied by thermal gravimetric analysis and differential thermal analysis (TGA /DTA) too.

Słowa kluczowe

EN

thallium (I); coordination polymer; nanostructure; thallium (III) oxide

• Wydawca: De Gruyter
• Czasopismo: Materials Science Poland
• Rocznik: 2014
• Tom: Vol. 32, No. 1
• Strony: 23--27
• Opis fizyczny: Bibliogr. 28 poz., rys., tab., wykr.

Twórcy

autor

Soltanian M J

• Departement of Chemistry, Firoozabad Branch, Islamic Azad University, Firoozabad, Fars, Iran P.O. Box 74715-117

autor

Tabaroki S

• Departement of Chemistry, Firoozabad Branch, Islamic Azad University, Firoozabad, Fars, Iran P.O. Box 74715-117

Bibliografia

• [1] STUMPF H.O., OUAHAB L., PEI Y. GRANDJEAN D., KAHN O., Science, 261 (1993), 447.
• [2] GARDNER G.B., VENKATARAMAN D.,. MOORE J. S., LEE S., Nature, 374 (1995), 792.
• [3] BRUCE D.W., Accounts Chem. Res., 33 (2000), 831.
• [4] MOULTON B., LU J., HAJNDL R., HARIHARAN S., ZAWOROTKO M.J., Angew. Chem. Int. Edit., 41 (2002) 2821.
• [5] CLEVERTY A.M., WARD M.D., Accounts Chem. Res., 31 (1998), 842.
• [6] RASHIDI RANJBAR Z., MORSALI A., J. Mol. Struct.,936 (2009) 206.
• [7] MORSALI A., TADJARODI R., MOHAMMADI R., MAHJOUB A.R., Z. Krist.-New Cryst. St., 216 (2001) 379.
• [8] MAHJOUB A.R., MORSALI A., J. Coord. Chem., 56 (2003), 779.
• [9] MORSALI A., PAYHEGHADER M., POORHERAVI M.R., JAMALI F.Z., Z. Anorg. Allg. Chem., 629 (2003), 1627.
• [10] MORSALI A., MAHJOUB A. R., DARZI S. J., SOLTANIAN M. J., Z. Anorg. Allg. Chem., 629 (2003), 2596.
• [11] MORSALI A., KEMPE R., Helv. Chim. Acta, 88 (2005), 2267.
• [12] XIAO H.P., MORSALI A., Helv. Chim. Acta, 88 (2005), 2543.
• [13] MORSALI A., MAHJOUB A.R., Solid State Sci., 7 (2005), 1429.
• [14] MORSALI A., Solid State Sci., 8 (2006), 82.
• [15] BECKMAN U., BROOKER S., Coordin. Chem. Rev., 245 (2003), 17.
• [16] KLINGALE M.H., BROOKER S., Coordin. Chem. Rev., 241 (2003) 119.
• [17] HAASNOOT J.G., Coordin. Chem. Rev., 200 (2000), 131.
• [18] WITHERSBY M.A. et al., Inorg. Chem., 38 (1999), 2259.
• [19] BLAKE A.J., CHAMPNESS N.R., COOKE P.A., NICOLSON J.E.B., WILSON C., J. Chem. Soc. Dalton, (2000), 3811.
• [20] WITHERSBY M.A., BLAKE A.J., CHAMPNESS N.R., HUBBERSTEY P., LI W.S., SCHRODER M., Angew. Chem. Int. Edit., 36 (1997), 2327.
• [21] NOTASH B., SAFARI N., KHAVASI H. R., AMANI V.,ABEDI A., J. Organomet. Chem., 693 (2008), 3553.
• [22] AKHBARI K., MORSALI A., Coordin. Chem. Rev., 254(2010), 1977.
• [23] SHELDRICK G. M. (2008), SADABS V2008/1, Bruker-AXS Inc, Madison, Wisconsin, USA.
• [24] SHELDRICK G. M., Acta Crystallogr. A, 64 (2008) 112.
• [25] Mercury 1.4.1, Copyright Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge, CB2 1EZ, UK, 2001.
• [26] DEMKO Z.P., SHARPLESS K. B., J. Org. Chem., 66 (2001), 7945.
• [27] HAZELL A., MCGINLEY J., TOFTLUND H., Inorg. Chim. Acta., 323 (2001), 113.
• [28] YANG J., LIN C., WANG ZH., LIN J., Inorg. Chem., 45 (2006), 8973.