Structural and photocatalytic properties of Ni-TiO2 photocatalysts prepared by mechanochemical synthesis assisted with calcination

• Autorzy: Kucio Karolina , Charmas Barbara , Zięzio Magdalena , Pasieczna-Patkowska Sylwia

Identyfikatory

DOI

10.37190/ppmp/150348

• Języki publikacji: EN

Abstrakty

EN

In the study the mechanochemical synthesis in the planetary ball mill was used to prepare photocatalytic materials obtained on the basis of TiO₂ and nickel(II) acetylacetonate as a Ni²⁺ source. Three materials with different contents of Ni²⁺: 5, 10 and 20% wt. were prepared. The obtained materials were calcinated at 800°C for 1 h. Their physicochemical properties were investigated using the N₂ adsorption/desorption, FT-IR/PAS, XRD, UV-Vis/DRS and SEM methods. Additionally, thermal stability of the obtained materials was examined (TGA/DTG/DTA). Photocatalytic activity of the samples was tested in relation to the aqueous solution of Safranin T (initial concentration C0 = 1×10^-5 mol L^-1) at the visible light (Vis). The results indicate that the mechanochemical synthesis is an effective and simple method for preparing materials with photocatalytic properties. All obtained materials were characterized by greater photocatalytic activity compared to the initial TiO₂.

Słowa kluczowe

EN

mechanochemical synthesis; titanium dioxide; photocatalysis; photocatalysts; safranin T

• Wydawca: Oficyna Wydawnicza Politechniki Wrocławskiej
• Czasopismo: Physicochemical Problems of Mineral Processing
• Rocznik: 2022
• Tom: Vol. 58, iss. 4
• Strony: art. no. 150348
• Opis fizyczny: Bibliogr. 58 poz.

Twórcy

autor

Kucio Karolina

• Institute of Chemical Sciences, Faculty of Chemistry, Maria Curie-Sklodowska University, Maria Curie-Sklodowska Sq. 3, 20-031 Lublin, Poland

autor

Charmas Barbara

• Institute of Chemical Sciences, Faculty of Chemistry, Maria Curie-Sklodowska University, Maria Curie-Sklodowska Sq. 3, 20-031 Lublin, Poland

autor

Zięzio Magdalena

• Institute of Chemical Sciences, Faculty of Chemistry, Maria Curie-Sklodowska University, Maria Curie-Sklodowska Sq. 3, 20-031 Lublin, Poland

autor

Pasieczna-Patkowska Sylwia

• Institute of Chemical Sciences, Faculty of Chemistry, Maria Curie-Sklodowska University, Maria Curie-Sklodowska Sq. 3, 20-031 Lublin, Poland

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Uwagi

Opracowanie rekordu ze środków MEiN, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2022-2023).