Techniki i metody wyodrębniania, rozdzielania i oznaczania frakcji asfaltenowej w rafineryjnych strumieniach procesowych

• Autorzy: Chruszczyk D. , Boczkaj G.

Warianty tytułu

EN

Techniques and methods of isolation, separation and quantification of asphaltene fraction in refinery process streams

• Języki publikacji: PL

Abstrakty

PL

W pracy przedstawiono metodyki izolacji frakcji asfaltenowej z rafineryjnych strumieni procesowych w tym ropy naftowej, olei i asfaltów w skali analitycznej i preparatywnej. Uwzględniono podstawowe zależności pomiędzy właściwościami otrzymanej frakcji, a ciśnieniem, temperaturą, proporcją oraz rodzajem czynnika precypitującego, a także czasem i temperaturą kontaktu oraz techniką oczyszczania powstałego osadu. Dodatkowo opisano techniki pozwalające na dalsze rozdzielenie wydzielonej frakcji oraz przedstawiono sposoby badania zawartości asfaltenów w surowcu i produktach jego przeróbki.

EN

The paper presents methods of isolation of asphaltene fraction from refinery process streams especially from crude oil, oils and bitumen in analytical and preparative scale. The relationship between the properties of the obtained fraction, pressure, temperature, proportion and type of precipitating agent, time and contact temperature and the solid asphaltenes purification techniques are described in details. Additionally the techniques used for further separation of asphalthenes into subsequent fractions are discussed as well as methods used for quantitative analysis of asphaltenes content in the feedstock and products of its processing.

Słowa kluczowe

PL

asfalteny; precypitacja; rozdzielanie grupowe; wysokosprawna chromatografia cieczowa (HPLC); chromatografia cienkowarstwowa z detektcją płomieniowo-jonizacyjną; TLC-FID

EN

asphaltenes; precipitation, group-type separation; high performance liquid chromatography (HPLC); thin layer chromatography with flame ionization detector; TLC-FID

• Wydawca: Publishing House of Siedlce University of Natural Sciences and Humanities
• Czasopismo: Camera Separatoria
• Rocznik: 2015
• Tom: Vol. 7, No. 1
• Strony: 5--16
• Opis fizyczny: Bibliogr. 68 poz., tab.

Twórcy

autor

Chruszczyk D.

• Politechnika Gdańska, Wydział Chemiczny, Katedra Inżynierii Chemicznej i Procesowej

autor

Boczkaj G.

• Politechnika Gdańska, Wydział Chemiczny, Katedra Inżynierii Chemicznej i Procesowej

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