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The main objective of the work was to create a layer of carbon nanofibre on the surface of the NiTi shape memory alloy. The coating process was carried out in three stages. First, polyacrylonitrile was deposited by electrospinning. Then it was stabilized at temperatures up to 250°C. The last stage was the carbonization performed below 1000°C. The microstructure of the obtained coatings was observed using a scanning electron microscope. The X-ray diffraction techniques were applied to analyze the coating structure. After the polyacrylonitrile deposition, the fibers had an average diameter of about 280 nm, and the final fibers were almost twice as tiny. The applied steps also changed the phase and crystalline state of the fibers, finally leading to the formation of amorphous-nanocrystalline graphite.
Słowa kluczowe
Wydawca
Czasopismo
Rocznik
Tom
Strony
1109--1114
Opis fizyczny
Bibliogr. 7 poz., fot., rys., wykr.
Twórcy
autor
- University of Silesia in Katowice, Institute of Materials Science, 75 Pułku Piechoty 1A, 41-500 Chorzów, Poland
autor
- AGH University of Science and Technology, Faculty of Materials Science and Ceramics, al. Mickiewicza 30, 30-059 Kraków, Poland
autor
- AGH University of Science and Technology, Faculty of Materials Science and Ceramics, al. Mickiewicza 30, 30-059 Kraków, Poland
autor
- AGH University of Science and Technology, Faculty of Materials Science and Ceramics, al. Mickiewicza 30, 30-059 Kraków, Poland
Bibliografia
- [1] T. Yoneyama, S. Miyazaki, Shape memory alloys for biomedical applications, Woodhead Publishing Limited, Cambridge (2009).
- [2] T. Goryczka, Z. Lekston, J. Lelątko, T. Szponder, J. Paluch, Eng. Biomater. 138, 72 (2016).
- [3] S. Keshavarz, O.V. Okoro, M. Hamidi, H. Derakhshankhah, M. Azizi, S.M. Nabavi, S. Gholizadeh, S.M. Amini, A. Shavandi, R. Luque, H. Samadian, Coord. Chem. Rev. 472, 214770 (2022).
- [4] D. Yadav, F. Amini, A. Ehrmannl, Eur. Polym. J. 138, 109963 (2020).
- [5] K.B.K. Teo, C. Singh, M. Chhowalla, W.I. Milne, Catalytic synthesis of carbon nanotubes and nanofibres, in: H.S. Nalwa (Ed.), Encycl. Nanosci. Nanotechnol., American Scientific Publishers, CA, USA, (2004) pp. 665-686.
- [6] M.S.A. Rahaman, A.F. Ismail, A. Mustafa, A review of heat treatment on polyacrylonitrile fiber, Polym. Degrad. Stab. 92 (8), 1421-1432 (2007).
- [7] L. Laffont et al., An EELS study of the structural and chemical transformation of PAN polymer to solid carbon, Carbon 42 (12-13), 2485-2494 (2004).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-04c53e1c-d0b7-4c28-8bdd-85d2fb3a9f82