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Purpose: The article presents the results of research on titanium dioxide synthesized by a sol-gel method that is an easy process enabling the control of the shape and size of particles The purpose of this article is to examine titanium dioxide nanoparticles and thin films deposited by an atomization method. Design/methodology/approach: Titanium dioxide sol was synthesized by using titanium isopropoxide as a precursor. Optical properties were measured by a UV-Vis spectrometer. Structural studies were performed by Raman spectroscopy. Qualitative analysis was performed by the EDS. Surface morphology of nanoparticles and thin films was performed by the SEM technique. Findings: The sol-gel method allows the formation of uniform nanoparticles and thin films of titanium dioxide. The atomization method is a successful method for the deposition of sol to the surface of substrates. Research limitations/implications: The next step in the research will be to investigate the obtained thin films in dye-sensitized solar cells as a semiconductive layer. Practical implications: Unique properties of produced titanium dioxide nanostructural materials have caused the interest in them in such fields as optoelectronics, photovoltaics, medicine and decorative coatings. Originality/value: Titanium dioxide thin films and nanoparticles were synthesized using the sol-gel method and then deposited by the atomization method.
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Rocznik
Tom
Strony
34--41
Opis fizyczny
Bibliogr. 16 poz.
Twórcy
autor
- Graduate of the Silesian University of Technology, ul. Konarskiego 18a, Gliwice, Poland
autor
- Department of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, Gliwice, Poland
autor
- Department of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, Gliwice, Poland
autor
- Department of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, Gliwice, Poland
autor
- Department of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, Gliwice, Poland
Bibliografia
- [1] A. Haider, Z. Jameel, I. Al-Hussaini, Review on: Titanium Dioxide Applications, Energy Procedia 157 (2019) 17-29, DOI: https://doi.org/10.1016/j.egypro.2018.11.159.
- [2] K. Harshakumar, K.C. Nair, N.G. Paulose, V.V. Nair, V. Prasanth, A. Krishnan, Titanium Dioxide as an Osteoconductive Material: An Animal Study, The Journal of Indian Prosthodontic Society 13/2 (2013) 95-100, DOI: https://doi.org/10.1007/s13191-012-0145-6.
- [3] B. O'Regan, M. Grätzel, A low-cost, high-efficiency solar cell based on dye-sensitized colloidal TiO2 films, Nature 353 (1991) 737-740, DOI: https://doi.org/10.1038/353737a0.
- [4] A. Kojima, K. Teshima, Y. Shirai, T. Miyasaka, Organometal Halide Perovskites as Visible-Light Sensitizers for Photovoltaic Cells, Journal of the American Chemical Society 131/17 (2009) 6050- 6051, DOI: https://doi.org/10.1021/ja809598r.
- [5] J. Im, C. Lee, J. Lee, S. Park, N. Park, 6.5% efficient perovskite quantum-dot-sensitized solar cell, Nanoscale 3/10 (2011) 4088-4093, DOI: https://doi.org/10.1039/C1NR10867K.
- [6] Y. Li, J. Hagen, W. Schaffrath, P. Otschik, D. Haarer, Titanium dioxide films for photovoltaic cells derived from a sol–gel process, Solar Energy Materials and Solar Cells 56/2 (1999) 167-174, DOI: https://doi.org/10.1016/S0927-0248(98)00157-3.
- [7] P. Falaras, K. Chryssou, T. Stergiopoulos, I. Arabatzis, G. Katsaros, V. Catalano, R. Kurtaran, A. Hugot-Le Goff, M. Bernard, Dye-sensitization of titanium dioxide thin films by Ru(II)-bpp-bpy complexes, Proceedings of SPIE 4801, Organic Photovoltaics III, 2003, DOI: https://doi.org/10.1117/12.452446.
- [8] Y. Ohya, H. Saiki, T. Tanaka, Y. Takahashi, Microstructure of TiO2 and ZnO Films Fabricated by the Sol-Gel Method, Journal of the American Ceramic Society 79/4 (1996) 825-830, DOI: https://doi.org/10.1111/j.1151-2916.1996.tb08512.x.
- [9] H. Cui, H. Shen, Y. Gao, K. Dwight, A. Wold, Photocatalytic properties of titanium (IV) oxide thin films prepared by spin coating and spray pyrolysis, Materials Research Bulletin 28/3 (1993) 195-201, DOI: https://doi.org/10.1016/0025-5408(93)90152-4.
- [10] K. Ravichandran, G. Muruganantham, K. Saravanakumar, S. Karnan, B. Kannan, R. Chandramohan, B. Sakthivel, Doubly doped tin oxide films from cost effective spray method using perfume atomiser, Surface Engineering 25/1 (2009) 82-87, DOI: https://doi.org/10.1179/026708408X370230.
- [11] B. Reguig, A. Khelil, L. Cattin, M. Morsli, J. Bernede, Properties of NiO thin films deposited by intermittent spray pyrolysis process, Applied Surface Science 253/9 (2007) 4330-4334, DOI: https://doi.org/10.1016/j.apsusc.2006.09.046.
- [12] H. Yanagi, Y. Ohoka, T. Hishiki, K. Ajito, A. Fujishima, Characterization of dye-doped TiO2 films prepared by spray-pyrolysis, Applied Surface Science 113-114 (1997) 426-431, DOI: https://doi.org/10.1016/S0169-4332(96)00946-4.
- [13] K. Choy, B. Su, Titanium dioxide anatase thin films produced by electrostatic spray assisted vapor deposition (ESAVD) technique, Journal of Materials Science Letters 18/12 (1999) 943-945, DOI: https://doi.org/10.1023/A:1006682217672.
- [14] X. Hou, K. Choy, Photocatalytic activity of nanocrystalline TiO2-based films produced by ESAVD method, Materials Science and Engineering: C 25/5-8 (2005) 669-674, DOI: https://doi.org/10.1016/j.msec.2005.06.008.
- [15] M. Rincón, O. Gómez-Daza, C. Corripio, A. Orihuela, Sensitization of screen-printed and spray-painted TiO2 coatings by chemically deposited CdSe thin films, Thin Solid Films 389/1-2 (2001) 91-98, DOI: https://doi.org/10.1016/S0040-6090(01)00900-2.
- [16] R. Kumar, N. Sharma, N. Arora, Study of spray deposited titanium dioxide films, Advances in Applied Science Research 7/3 (2016) 142-147.
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Bibliografia
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