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2016 | Vol. 28, no. 1 | 129--143
Tytuł artykułu

Simultaneous determination of four major constituents in Citri Grandis Exocarpium by HPLC-DAD

Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Citri Grandis Exocarpium (CGE) is a traditional Chinese medicine with a variety of biological activities. For efficient quality control of CGE, a simple, rapid, and accurate high-performance liquid chromatographic (HPLC) method was developed for simultaneous determination of four main compounds (naringin, rhoifolin, meranzin hydrate, and isoimperatorin) in this herb. These four compounds were separated on a C18 column by gradient elution with methanol and water. The flow rate was 1.0 mL•min−1, and the detection wavelength was 324 nm. The recoveries of the method ranged from 96.32% to 103.71%, and good linear relationships (r2 > 0.9998) over relative wide concentration ranges were obtained. Then this validated method was successfully applied to the analysis of nine batches of CGE samples.
Słowa kluczowe
Wydawca

Rocznik
Strony
129--143
Opis fizyczny
Bibliogr. 16 poz., rys., tab.
Twórcy
autor
  • School of Pharmaceutical Sciences, Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
  • Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China
autor
  • School of Pharmaceutical Sciences, Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
  • Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China
autor
  • School of Pharmaceutical Sciences, Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
  • Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China
autor
  • School of Pharmaceutical Sciences, Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
  • Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China
autor
  • School of Pharmaceutical Sciences, Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
  • Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China
autor
  • School of Pharmaceutical Sciences, Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China, xxj2702@sina.com
  • Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China
Bibliografia
  • [1] China Pharmacopoeia Committee, Pharmacopoeia of the People's Republic of China, First Division (2010 edition), China Chemical Industry Press, Beijing, China, 2009, p. 69
  • [2] S.X. Wu, J. Guangdong Med. College, 2, 54 (1988)
  • [3] C. Ma and M.S. Jiang, Sci. Tech. Review, 13, 200 (2009)
  • [4] P.B. Li, Y. Ma, H.L. Yang, Q. Jia, Y.G. Wang, and W.W. Su, Chin. Tradit. Herb. Drugs, 37, 251 (2006)
  • [5] P.B. Li, Y. Ma, Y.G. Wang, and W.W. Su, China J. Chin. Mat. Med., 31, 1350 (2006)
  • [6] X.L., Mo, Y.W. Cai, and Q.Q. Zeng, Food Drug, 9, 39 (2007)
  • [7] J. Li, J. Clin. Med. Pract., 13, 74 (2009)
  • [8] W.Q. Xiao, C.H. Zhang, L.S. Xie, H.F. Dai, B.X. Huang, and X.R. Wang, Food Sci., 30, 320 (2009)
  • [9] C.H. Zhang, W.Q. Xiao, P. Zhao, L.S. Xie, H.F. Dai, B.X. Huang, and H. Zhang, J. Huazhong. Agric. Univ., 28, 48 (2009)
  • [10] L.Z. Huang, Z.H. Liang, L. Lin, D.X. Gao, and J.F. Ou, Tradit. Chin. Drug Res. Clin. Pharmacol., 16, 59 (2005)
  • [11] M.J. Martin, E. Marhuenda, C. Perez-Guerrero, and J.M. Franco, Pharmacol., 49, 144 (1994)
  • [12] C.H. Lee, T.S. Jeong, Y.K. Choi, B.H. Hyun, G.T. Oh, E.H. Kim, J.R. Kim, J.I. Han, and S.H. Bok, Biochem. Biophys. Res. Commun., 284, 681 (2001)
  • [13] Q. Lv, Y. Yang, Y. Zhao, D. Gu, D. He, A. Yili, Q. Ma, Z. Cheng, Y. Gao, H.A. Aisa, and Y. Ito, J. Liq. Chromatogr. Relat. Technol., 32, 2879 (2009)
  • [14] M. Mokbel and T. Suganuma, Eur. Food Res. Technol., 224, 39 (2006)
  • [15] M. Mokbel, Y. Watanabe, F. Hashinaga, and T. Suganuma, Pak. J. Bio. Sci., 9, 145 (2006)
  • [16] Y.R. Pokharel, E.H. Han, J.Y. Kim, S.J. Oh, S.K. Kim, E.R. Woo, H.G. Jeong, and K.W. Kang, Carcinogenesis, 27, 2483 (2006)
Uwagi
PL
Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.
Typ dokumentu
Bibliografia
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Identyfikator YADDA
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