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2014 | 68 | 1-2 | 107-120
Tytuł artykułu

An Application of Microemulsion Method for Synthesis of Copper-Zinc Materials

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Microemulsion method was used for preparation of copperzinc mixed oxides. Samples were prepared from the solutions containing zinc and copper nitrates. Sodium carbonate was used as a precipitant and hydrazine as reducing agent. Water-in-oil (W/O) microemulsions were formed by the application of cyclohexane, isopropyl alcohol, and hexadecyltrimethylammonium bromide (CTAB) as surfactant. The aim of the studies was determination of the influence of the sequence of synthesis stages on the formation of materials, their surface and structural properties. Thermal decomposition studies of materials were carried out by infrared spectroscopy. The physicochemical properties were characterized by nitrogen adsorption-desorption method, X-ray diffraction (XRD) and temperature-programmed reduction (TPR).
Słowa kluczowe
Wydawca

Rocznik
Tom
68
Numer
1-2
Strony
107-120
Opis fizyczny
Daty
online
2014-10-17
Twórcy
  • Faculty of Chemistry, Department of Chemical Technology, Maria Curie-Sklodowska University 3 M. Curie-Skłodowskiej Square, 20-031 Lublin, Poland, ajustyna.pawlonka@gmail.com
  • Faculty of Chemistry, Department of Chemical Technology, Maria Curie-Sklodowska University 3 M. Curie-Skłodowskiej Square, 20-031 Lublin, Poland, grzesiek.slowik@gmail.com
autor
  • Faculty of Chemistry, Department of Chemical Technology, Maria Curie-Sklodowska University 3 M. Curie-Skłodowskiej Square, 20-031 Lublin, Poland, wojtek.gac@poczta.umcs.lublin.pl
  • Faculty of Chemistry, Department of Chemical Technology, Maria Curie-Sklodowska University 3 M. Curie-Skłodowskiej Square, 20-031 Lublin, Poland, tadeusz.borowiecki@umcs.lublin.pl
Bibliografia
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  • 6. C. Wang, D. Chen and T. Huang, Colloids and Surfaces A:Physicochem. Eng. Aspects, 189, 145, (2001).
  • 7. I. Capek, Emulsion Science and Technology, WILEY-VCH, Weinheim 2009.
  • 8. G. Xiong, L. Luo, C. Li and X. Yang, Energy & Fuels, 23, 1342, (2009).
  • 9. S. Hingorani, V. Pillai, P. Kumar, M. S. Multani and D. O. Shah, Mat. Res. Bull., 28, 1303, (1993).
  • 10. G. Fierro, M. L. Jacono, M. Inversi, P. Porta, F. Cioci and R. Lavecchia, Applied Catalysis: General, 137, 327, (1996).
  • 11. S. H. Taylor, G. J. Hutchings, A. A. Mirzaei, Catalysis Today, 84, 113. (2003).
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_umcschem-2013-0009
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