Characterisation of Ni-C films obtained in PVD/CVD process

• Autorzy: Justyna Kęczkowska
• Języki publikacji: EN

Abstrakty

EN

The work presents the results of the scanning electron microscopy (SEM) and Raman spectrometry studies of carbonaceous nanostructures containing nickel nanocrystallites. The films were obtained using a two-step method. In the first phase the Physical Vapour Deposition (PVD) method was applied, whereas in the second Chemical Vapour Deposition (CVD) method was used. The paper presents results for samples with various Ni content obtained with different parameters of the two-phase technological process. The research confirms that the thin films obtained by PVD method contain Ni nanocrystallites distributed in a carbonaceous matrix. The matrix is composed of various carbon allotropes (amorphous carbon, graphite, fullerene). The thin films made by CVD method make a matrix when multiwalled, carbonaceous nanotubes are obtained. Depending on the technological process parameters of each phase, we obtain multiwall nanotubes with a various degree of defects.

Słowa kluczowe

EN

PVD method; CVD method; Ni-C films; Raman spectroscopy; carbon nanotubes

• Czasopismo: Open Physics
• Rocznik: 2011
• Tom: 9
• Numer: 2
• Strony: 330-337

Daty

wydano

2011-04-01

online

2011-02-20

Twórcy

autor

Justyna Kęczkowska

• Kielce University of Technolog, al. 1000-lecia P.P. 7, 25-314, Kielce, Poland,

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Identyfikatory

DOI

10.2478/s11534-010-0090-0