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2014 | 12 | 12 | 1239-1245
Tytuł artykułu

Voltammetric behavior and quantitative determination of ambazone concentrations in urine and in a pharmaceutical formulation

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The use of square wave adsorptive stripping voltammetry (SWAdSV) in conjunction with a cyclic renewable silver amalgam film electrode (Hg(Ag)FE) for the analytical determination of ambazone in urine samples and pharmaceutical formulations is described. A single reduction peak in Britton-Robinson buffer at pH 4.0 was detected at about −1.4 V versus Ag/AgCl. Mechanistic studies have shown that the compound can act as an electrocatalyst. The method was validated. The analytical curve was linear in the concentration range from 1.0×10−9 to 1.0×10−7 mol L−1. The detection and quantification limits were found to be 3.0×10−10 mol L−1 and 1.0×10−9 mol L−1, respectively. The proposed method was successfully applied to ambazone determination in real samples.
Wydawca

Czasopismo
Rocznik
Tom
12
Numer
12
Strony
1239-1245
Opis fizyczny
Daty
wydano
2014-12-01
online
2014-06-07
Twórcy
  • University of Lodz
  • University of Lodz
  • University of Lodz
  • University of Lodz
Bibliografia
  • [1] A.M. Ares, J. Bernal, Cent. Eur. J. Chem. 10, 534 (2012) http://dx.doi.org/10.2478/s11532-012-0003-8[Crossref]
  • [2] J. Ronowicz, B. Kupcewicz, J. Mydłowska, E. Budzisz, Cent. Eur. J. Chem. 11, 1091 (2013) http://dx.doi.org/10.2478/s11532-013-0243-2[Crossref]
  • [3] I. Fulga, Ambazona: notiuniacceptate, informatiinoi, posibile perspective, Pharmakon 2006, 56. www.pharmakon.ro/inc/arhiva/200602/Ambazona.pdf
  • [4] G. Lober, K. Geller, H. Hanschmann, L.M. Popa, R. Repanovici, R. Iliescu, W. Romer, B. Janke, V. Kleinwachter, Physiology 26, 305 (1989)
  • [5] G. Lober, H. Hoffmann, Biophys. Chem. 35, 287 (1990) http://dx.doi.org/10.1016/0301-4622(90)80016-Z[Crossref]
  • [6] G. Kuhnke, D. Gockeritz, R. Pohlaudek-Fabini, Pharmazie 31, 820 (1976) [PubMed]
  • [7] V. Mirceski, S. Komorsky-Lovric, M. Lovric, in: F. Scholz (Ed.), Square-wave voltammetry: theory and applications (Springer, Heidelberg, 2007)
  • [8] M. Lovric, in: F. Scholz (Ed.), Square-wave voltammetry, Electroanalytical methods: guide to experiments and applications (Springer-Verlag, Berlin, 2002)
  • [9] A.M. Beltagi, M.A. El-Attar, E. M. Ghoneim, Cent. Eur. J. Chem. 5, 835 (2007) http://dx.doi.org/10.2478/s11532-007-0026-8[Crossref]
  • [10] P. Snevajsova, L. Tison, I. Brozkova, J. Vytrasova, R. Metelka, K. Vytras, Electrochem. Commun. 12, 106 (2010) http://dx.doi.org/10.1016/j.elecom.2009.10.047[Crossref]
  • [11] K. Vytras, I. Svancara, R. Metelka, J. Serb. Chem. Soc. 74, 1021 (2009) http://dx.doi.org/10.2298/JSC0910021V[Crossref]
  • [12] V. Guzsvany, J. Petrovic, J. Krstic, Z. Papp, M. Putek, L. Bjelica, A. Bobrowski, B. Abramovic, J. Electroanal. Chem. 699, 33 (2013) http://dx.doi.org/10.1016/j.jelechem.2013.04.003[Crossref]
  • [13] T. Sarigul, R. Inam, Electrochim. Acta 54, 5376 (2009) http://dx.doi.org/10.1016/j.electacta.2009.04.022[Crossref]
  • [14] A. Nosal-Wiercinska, M. Grochowski, S. Skrzypek, D. Guziejewski, Desalin. and Water Treat. 51, 1700 (2013) http://dx.doi.org/10.1080/19443994.2012.714501[Crossref]
  • [15] M. Lovric, D. Jadresko, S. Komorsky-Lovric, Electrochim. Acta, 90, 226 (2013) http://dx.doi.org/10.1016/j.electacta.2012.11.101[Crossref]
  • [16] D. Jadresko, J. Electroanal. Chem. 693, 56 (2013) http://dx.doi.org/10.1016/j.jelechem.2013.01.029[Crossref]
  • [17] S. Skrzypek, V. Mirceski, S. Smarzewska, D. Guziejewski, W. Ciesielski, Collect. Czech. Chem. Commun. 76, 1699 (2011) http://dx.doi.org/10.1135/cccc2011122[Crossref]
  • [18] F.E.A. Catunda Jr., M.F. de Araujo, A.M. Granero, F.J. Arevalo, M.G. de Carvalho, M.A. Zon, H. Fernandez, Electrochim. Acta 56, 9707 (2011) http://dx.doi.org/10.1016/j.electacta.2011.07.053[Crossref]
  • [19] V. Mirceski, D. Guziejewski, K. Lisichkov, Electrochim. Acta 114, 667 (2013) http://dx.doi.org/10.1016/j.electacta.2013.10.046[Crossref]
  • [20] D. Krulic, N. Fatouros, J. Electroanal. Chem. 652, 26 (2011) http://dx.doi.org/10.1016/j.jelechem.2010.12.009[Crossref]
  • [21] AGH University of Science and Technology, PL Patent No. P-319984, Method of and apparatus for making a thin-layer mercury electrode, 1997
  • [22] B. Baś, Z. Kowalski, Electroanalysis 14, 1067 (2002) http://dx.doi.org/10.1002/1521-4109(200208)14:15/16<1067::AID-ELAN1067>3.0.CO;2-5[Crossref]
  • [23] S. Smarzewska, S. Skrzypek, W. Ciesielski, Electroanalysis 24, 1591 (2012) http://dx.doi.org/10.1002/elan.201200164[Crossref]
  • [24] P. Kapturski, A. Bobrowski, J. Electroanal. Chem. 617, 1 (2008) http://dx.doi.org/10.1016/j.jelechem.2008.01.007[Crossref]
  • [25] R. Piech, B. Baś, W. W. Kubiak, Talanta 76, 295 (2008) http://dx.doi.org/10.1016/j.talanta.2008.02.038[Crossref]
  • [26] O. Mikkelsen, K. H. Schroeder, T. A. Aarhaug, Collect. Czech. Chem. Commun. 66, 465 (2001) http://dx.doi.org/10.1135/cccc20010465[Crossref]
  • [27] O. Mikkelsen, K. H. Schroeder, Anal. Lett. 33, 3253 (2000) http://dx.doi.org/10.1080/00032719.2000.10399499[Crossref]
  • [28] S. Smarzewska, S. Skrzypek, W. Ciesielski, Electroanalysis 24, 1966 (2012) http://dx.doi.org/10.1002/elan.201200312[Crossref]
  • [29] S. Smarzewska, R. Metelka, D. Guziejewski, M. Skowron, S. Skrzypek, M. Brycht, W. Ciesielski, Anal. Methods (2014) (in press), DOI:10.1039/C3AY42038H [Crossref]
  • [30] R. Selesovska-Fadrna, T. Navratil, M. Vlcek, Chem. Anal. (Warsaw) 52, 911 (2007)
  • [31] B. Yosypchuk, L. Novotny, Electroanalysis 14, 1733 (2002) http://dx.doi.org/10.1002/elan.200290018[Crossref]
  • [32] B. Yosypchuk, L. Novotny, Crit. Rev. Anal. Chem. 32, 141 (2002) http://dx.doi.org/10.1080/10408340290765498[Crossref]
  • [33] P. T. Kissinger, W. R. Heinemann, Laboratory Techniques in Electroanalytical Chemistry, 2nd edition (Taylor & Francis, New York, 1996)
  • [34] D.K. Gosser, Cyclic voltammetry (VCH, New York, 1994)
  • [35] V. Mirceski, S. Skrzypek, W. Ciesielski, A. Sokolowski, J. Electroanal. Chem. 585, 97 (2005) http://dx.doi.org/10.1016/j.jelechem.2005.07.017[Crossref]
  • [36] V. Mirceski, R. Gulaboski, J. Solid State Electrochem. 7, 157 (2003)
  • [37] V. Mirceski, R. Gulaboski, Electroanalysis 13, 1326 (2001) http://dx.doi.org/10.1002/1521-4109(200111)13:16<1326::AID-ELAN1326>3.0.CO;2-S[Crossref]
  • [38] J. Wang, Electroanalytical Techniques in Clinical Chemistry and Laboratory Medicine (VCH, New York, 1988)
  • [39] The United States Pharmacopeia, USP-24, NF-19, Asian Edition, (United States Pharmacopoeial Convention, INC, Rockville, MD, 2000) 2149
  • [40] S.A. Ozkan, Electroanalytical methods in pharmaceutical analysis and their validation (HNB Publishing, New York, 2012)
Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-014-0574-7
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