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2014 | 12 | 6 | 736-746
Tytuł artykułu

Chemometric analysis of volatiles of propolis from different regions using static headspace GC-MS

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Six samples of propolis were analyzed in the paper: a sample from Brazil, Estonia, China and three samples from different locations of Uruguay. Static headspace technique coupled with gas chromatography-mass spectrometry analysis has been applied for the determination of the characteristic volatile profile with the aim to differentiate the propolis from different regions. Monoterpenes (α- and β-pinenes) were predominant in all samples, except the sample from China. This sample separated itself by the alcohols 3-methyl-3-buten-1-ol and 3-methyl-2-buten-1-ol, (40.33% and 11.57%, respectively) and ester 4-penten-1-yl acetate (9.04%). α-Pinene and β-pinene composed 64.59–77.56% of volatiles in Brazilian and Uruguayan propolis, and 29.43% in Estonian propolis. Brazilian propolis was distinguished by a high amount of β-methyl crotonaldehyde (10.11%), one of Uruguayan samples 3- by limonene (15.58%), and the Estonian sample - by eucalyptol (25.95%). Statistical investigation of the samples was made applying principal component, hierarchical cluster and K-Means cluster analyses. Various data pre-processing techniques were proposed and used to study and obtain the important volatile compounds contributed to the differentiation of the propolis samples from different regions to separate clusters.
Wydawca

Czasopismo
Rocznik
Tom
12
Numer
6
Strony
736-746
Opis fizyczny
Daty
wydano
2014-06-01
online
2014-03-13
Twórcy
  • Kaunas University of Technology
  • Vytautas Magnus University
  • Lithuanian University of Health Science
Bibliografia
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-014-0521-7
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