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2013 | 11 | 12 | 2066-2075
Tytuł artykułu

Copper complexes formed by 3,5-bis(2,2′-bipyridin-4-ylethynyl)benzoic acid and its methyl and ethyl esters as studied by electrospray ionization mass spectrometry

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Electrospray ionization mass spectrometry was used to study the complexes of ligands containing two bipyridine units, namely 3,5-bis(2,2-bipyridin-4-ylethynyl)benzoic acid (1) and its methyl and ethyl esters (2, 3), with copper cation, with CuCl2 as a source of copper. It was found that the type of complexes formed strongly depends on CuCl2 concentration. At lower CuCl2 concentration, the detected complexes were rather simple and some of them were formed upon electrospray ionization conditions e.g. ions [22+Cu2]2+ and [32+Cu2]2+ (complexes ligand-Cu(I) of stoichiometry 2:2) which are analogical to the well known, for quaterpyridine, helical complexes. At higher CuCl2 concentration, the detected complexes were more complicated, and most of them contained copper cations bridged by chlorides. The largest ions were [L2+Cu4Cl6]2+. The CID MS/MS spectra of these ions allowed determination of their mass spectrometric fragmentation pathways and as a consequence their structure elucidation. [...]
Wydawca

Czasopismo
Rocznik
Tom
11
Numer
12
Strony
2066-2075
Opis fizyczny
Daty
wydano
2013-12-01
online
2013-09-26
Twórcy
  • Faculty of Chemistry, Adam Mickiewicz University, 61-614, Poznań, Poland, franski@amu.edu.pl
  • Faculty of Chemistry, Adam Mickiewicz University, 61-614, Poznań, Poland
  • Faculty of Chemistry, Adam Mickiewicz University, 61-614, Poznań, Poland
autor
  • Faculty of Chemistry, Adam Mickiewicz University, 61-614, Poznań, Poland
  • Faculty of Chemistry, Adam Mickiewicz University, 61-614, Poznań, Poland
  • Faculty of Chemistry, Adam Mickiewicz University, 61-614, Poznań, Poland
  • Faculty of Chemistry, Adam Mickiewicz University, 61-614, Poznań, Poland
Bibliografia
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-013-0324-2
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