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2013 | 11 | 10 | 1674-1681
Tytuł artykułu

Voltammetric behavior of rutin at a boron-doped diamond electrode. Its electroanalytical determination in a pharmaceutical formulation

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
This paper examined for the first time, the possibilities of the usage of a boron-doped diamond electrode for the redox behavior of rutin using cyclic and adsorptive stripping voltammetry. The cyclic voltammograms showed a pair of redox peaks at lower potentials followed by an irreversible oxidation peak at higher positive potential. Using square-wave adsorptive stripping voltammetry, the compound yielded a well-defined voltammetric response in Britton-Robinson buffer, pH 4.0 at +0.48 V (vs. Ag/AgCl) (after 60 s accumulations at a fixed potential of 0.2 V). The calibration curve was linear in the concentration range from 0.01 µg mL−1 to 0.1 µg mL−1 (1.64×10−8 M − 1.64×10−7 M). A detection limit of 0.0017 µg mL−1 (2.78×10−9 M) was observed without any chemical modifications and electrochemical surface pretreatments. As an example, the practical applicability of boron-doped diamond electrode was tested with the measurement of rutin in dietary supplement products. [...]
Wydawca

Czasopismo
Rocznik
Tom
11
Numer
10
Strony
1674-1681
Opis fizyczny
Daty
wydano
2013-10-01
online
2013-07-19
Twórcy
  • Faculty of Science, Department of Analytical Chemistry, Yüzüncü Yıl University, 65080, Van, Turkey
  • Faculty of Pharmacy, Department of Analytical Chemistry, Yüzüncü Yıl University, 65080, Van, Turkey, yavuzyardim2002@yahoo.com
  • Faculty of Science, Department of Analytical Chemistry, Yüzüncü Yıl University, 65080, Van, Turkey
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-013-0292-6
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