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2013 | 11 | 5 | 736-741
Tytuł artykułu

Sensitive and fast determination of papaverine by adsorptive stripping voltammetry on renewable mercury film electrode

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The renewable mercury film electrode, applied for the determination of papaverine traces using differential pulse adsorptive stripping voltammetry (DP AdSV) is presented. The calibration graph obtained for papaverine is linear from 1.25 nM (0.42 µg L−1) to 95 nM (32.2 µg L−1) for a preconcentration time of 60 s, with correlation coefficient of 0.998. For the renewable mercury electrode (Hg(Ag)FE) with a surface area of 9.1 mm2 the detection limit for a preconcentration time of 60 s is 0.7 nM (0.24 µg L−1). The repeatability of the method at a concentration level of the analyte as low as 17 µg L−1, expressed as RSD is 3.3% (n=5). The proposed method was successfully applied and validated by studying the recovery of papaverine from drugs, urine and synthetic solution. [...]
Wydawca

Czasopismo
Rocznik
Tom
11
Numer
5
Strony
736-741
Opis fizyczny
Daty
wydano
2013-05-01
online
2013-02-27
Twórcy
autor
  • Faculty of Materials Science and Ceramics, AGH University of Science and Technology, 30-059, Kraków, Poland, rpiech@agh.edu.pl
  • Faculty of Materials Science and Ceramics, AGH University of Science and Technology, 30-059, Kraków, Poland
Bibliografia
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-013-0208-5
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