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2013 | 11 | 5 | 774-781
Tytuł artykułu

Research on thermal decomposition of trinitrophloroglucinol salts by DSC, TG and DVST

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The thermal decomposition of the four nitrogen-rich salts of ammonia (NH4), aminoguanidine (AG), carbohydrazide (CHZ) and 5-aminotetrazo (ATZ) based on trinitrophloroglucinol (H3TNPG) was investigated using the differential scanning calorimetry (DSC), thermogravity (TG), and dynamic vacuum stability test (DVST). DSC and TG methods research the complete decomposition, while DVST method researches the very early reaction stage. The peak temperatures of DSC curves are consistent with the temperatures of maximum mass loss rates of TG curves. The apparent activation energies of these H3TNPG-based salts obtained by DSC and DVST have the same regularity, i.e., (ATZ)(H2TNPG)·2H2O 2O 4(H2TNPG) 2TNPG). The thermal stability order is (ATZ)(H2TNPG)·2H2O 2O 2TNPG) 4(H2TNPG), which was evaluated by DVST according to the evolved gas amount of thermal decomposition. DVST can monitor the real-time temperature and pressure changes caused by thermal decomposition, dehydration, phase transition and secondary reaction, and also evaluate the thermal stability and kinetics. [...]
Wydawca

Czasopismo
Rocznik
Tom
11
Numer
5
Strony
774-781
Opis fizyczny
Daty
wydano
2013-05-01
online
2013-02-27
Twórcy
autor
  • State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing, 100081, China
  • State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing, 100081, China, ztlbit@bit.edu.cn
autor
  • State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing, 100081, China
autor
  • State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing, 100081, China
autor
  • The 3rd Department, Institute of Chemical Defense, Beijing, 102205, China
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-013-0205-8
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