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2013 | 11 | 3 | 341-347
Tytuł artykułu

A silica gel-bound macrocycle system for the selective separation of toxic cadmium from metal-affluent aqueous matrix

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Abstract Selective separation of cadmium(II) on a macrocycle immobilized solid phase extraction (SPE) system namely AnaLig Cd-01, and commonly known as molecular recognition technology (MRT) gel, have been examined. The MRT-SPE able to retain the cadmium from the metal-affluent aqueous matrix at the pH range of 2 to 8, and the captured species can be recovered via elution with 1 and 6 M HNO3. Besides the effects of solution pH and eluent concentration, the impacts of sample loading flow rates and coexisting matrix ions were also investigated and optimized. The Cd(II) retention capacity of the MRT-SPE was 0.26 mmol g-1, and it can be reused for more than 100 loading and elution cycles. The Cd(II) recovery attained from the metal-spiked natural waters was satisfactory (95.3–98.1%). However, the Cd(II) retention ability of the MRT-SPE was significantly decreased when excess of chelant remain in the aqueous waste matrix. Graphical abstract [...]
Wydawca
Czasopismo
Rocznik
Tom
11
Numer
3
Strony
341-347
Opis fizyczny
Daty
wydano
2013-03-01
online
2012-12-28
Twórcy
autor
  • Graduate School of Natural Science and Technology, Kanazawa University, Kakuma, Kanazawa, 920-1192, Japan
  • Graduate School of Natural Science and Technology, Kanazawa University, Kakuma, Kanazawa, 920-1192, Japan
autor
  • Institute of Science and Engineering, Kanazawa University, Kakuma, Kanazawa, 920-1192, Japan
  • GL Sciences, Inc., Nishishinjuku 6-22-1, Shinjuku, Tokyo, 163-1130, Japan
  • Graduate School of Engineering, Osaka City University, Sugimoto 3-3-138, Sumiyoshi-Ku, Osaka, 558-8585, Japan
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-012-0176-1
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