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2012 | 10 | 5 | 1617-1623
Tytuł artykułu

Photometric determination of aqueous cobalt (II), nickel (II), copper (II) and iron (III) with 1-nitroso-2-naphthol-3,6-disulfonic acid disodium salt in gelatin films

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Języki publikacji
EN
Abstrakty
EN
Photometric determination of aqueous Co(II), Cu(II), Ni(II) and Fe(III) was performed using indicator films prepared by immobilization of 1-nitroso-2-naphthol-3,6-disulfonic acid disodium salt (NRS) into hardened photographic film. Immobilization was based on electrostatic interaction of reagent and metal complexes with the gelatin. The isoelectric point pH of hardened gelatin (4.46±0.04) was evaluated by viscometry. Co(II), Fe(III), Ni(II) form 1:3 complexes with NRS in gelatin at pH 2 and Cu(II) forms 1:2 complexes. Their log β′ values were: Co-6.7, Fe-8.6, Cu-8.0, and Ni-6.4. The absorption maxima were: 370nm for NRS, and 430nm, 470nm, 495nm and 720nm for complexes of Co(II), Ni(II), Cu(II) and Fe(III). An algorithm for their simultaneous determination using the indicator films was developed. The detection limits were: clim(Co2+) = 0.45×10−5 M, clim(Fe3+) = 0.50×10−5 M, clim(Cu2+) = 0.67×10−5 M, clim(Ni2+) = 0.75×10−5 M,; and their sum clim(ΣMn+) = 0.82×10−5 M. [...]
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Wydawca

Czasopismo
Rocznik
Tom
10
Numer
5
Strony
1617-1623
Opis fizyczny
Daty
wydano
2012-10-01
online
2012-07-21
Twórcy
  • Department of Chemical Metrology, Chemical Faculty, Kharkiv V.N. Karazin National University, Kharkiv, 61022, Ukraine
  • Department of Chemical Metrology, Chemical Faculty, Kharkiv V.N. Karazin National University, Kharkiv, 61022, Ukraine
  • Department of Chemical Metrology, Chemical Faculty, Kharkiv V.N. Karazin National University, Kharkiv, 61022, Ukraine, nikitina@univer.kharkov.ua
Bibliografia
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-012-0081-7
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