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2012 | 10 | 5 | 1506-1515
Tytuł artykułu

Methyl- and methoxysalicylatocopper complexes with 2-pyridylmethanol: Synthesis, spectral properties, structure and EPR characterization in solid-state and in solution

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The syntheses and characterizations of salicylatocopper(II) complexes of the formula Cu(X-sal)2(2-pyme)2 (X = 3-MeO (1), 4-MeO (2), 3-Me (3), 4-Me (4) and 5-Me (5), where 3-MeOsal− = 3-methoxysalicylate, 4-MeOsal− = 4-methoxysalicylate, 3-Mesal− = 3-methylsalicylate, 4-Mesal− = 4-methylsalicylate, 5-Mesal− = 5-methylsalicylate anion, and 2-pyme = 2-pyridylmethanol) are reported. The composition was determined by elemental analysis, and ligand coordination modes have been determined by spectroscopic methods (IR, UV-VIS). The crystal structure determination of [Cu(3-MeOsal)2(2-pyme)2] (1) and [Cu(5-Mesal)2(2-pyme)2] (5) have confirmed conclusions originally based on spectral data. EPR measurements of frozen water/methanol solutions containing different copper(II): 2-pyme molar ratios have indicated presence of complexes with only two nitrogen donor atoms bonded to each central atom. [...]
Wydawca

Czasopismo
Rocznik
Tom
10
Numer
5
Strony
1506-1515
Opis fizyczny
Daty
wydano
2012-10-01
online
2012-07-21
Twórcy
  • Department of Inorganic Chemistry, Slovak University of Technology, SK-812 37, Bratislava, Slovakia
  • Department of Physical Chemistry, Slovak University of Technology, SK-812 37, Bratislava, Slovakia
autor
  • Department of Inorganic Chemistry, Slovak University of Technology, SK-812 37, Bratislava, Slovakia
  • Department of Inorganic Chemistry, Slovak University of Technology, SK-812 37, Bratislava, Slovakia
autor
  • Department of Physical Chemistry, Slovak University of Technology, SK-812 37, Bratislava, Slovakia
  • Department of Inorganic Chemistry, Slovak University of Technology, SK-812 37, Bratislava, Slovakia
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-012-0065-7
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