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2012 | 10 | 1 | 137-145
Tytuł artykułu

In vitro bioactivity of 70 wt.% SiO2 - 30 wt.% CaO sol-gel glass, doped with 1, 3 and 5 wt.% NbF5

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The 70SiO2-30CaO (wt.%) sol-gel glasses doped with 1, 3 and 5 NbF5 (wt.%) were prepared via polystep sol-gel route. The synthesized glasses were characterized by XRD, FTIR and SEM. Changes in 1.5 SBF solutions were measured by ICP-AES. XRD of the glasses stabilized at 700°C for 6 hours proved the presence of niocalite. FTIR was consistent with XRD data. The in vitro bioactivity study of all glasses prepared were carried out by soaking in 1.5 simulated body fluid (1.5 SBF) at 37°C for 6 and 12 days in static conditions. The FTIR reveals the formation of A-type and B-type carbonate containing hydroxyapatite (CO3HA) layer. Changes in 1.5 SBF solutions, after 6 days of soaking, show that the Ca concentration increased significantly, compared to the initial Ca content in the 1.5 SBF solution before in vitro test. After 12 days of immersion, the Ca concentration decreased, i.e., the formation of HA phase consumed Ca from 1.5 SBF solution. For all soaking times, the concentration of P is much lower than that the used 1.5 SBF. Based on these results we suggest that Ca and P play an active role in the future of the glasses. SEM depicts that the different morphology of hydroxyapatite can be formed as a function of soaking time.
Wydawca

Czasopismo
Rocznik
Tom
10
Numer
1
Strony
137-145
Opis fizyczny
Daty
wydano
2012-02-01
online
2011-11-24
Twórcy
  • University of Chemical Technology and Metallurgy, radev@abv.bg
  • University of Chemical Technology and Metallurgy
  • University of Chemical Technology and Metallurgy
  • University of Aveiro
  • University of Aveiro
Bibliografia
  • [1] T. Kokubo, J. Ceram. Soc. Jpn. 99, 965 (1991) http://dx.doi.org/10.2109/jcersj.99.965[Crossref]
  • [2] T. Kokubo, Journal of Non-Crystalline Solids 120, 138 (1990) http://dx.doi.org/10.1016/0022-3093(90)90199-V[Crossref]
  • [3] T. Kokubo, Biomaterials 12, 155 (1991) http://dx.doi.org/10.1016/0142-9612(91)90194-F[Crossref]
  • [4] Y. Abe, T. Kokubo, T. Yamamuro, J. Mater. Sci.: Mater. Med. 1, 233 (1990) http://dx.doi.org/10.1007/BF00701082[Crossref]
  • [5] K. Hata, N. Ozawa, T. Kokubo, T. Nakamura, J. Ceram. Soc. Jpn. 109(5), 461 (2001) http://dx.doi.org/10.2109/jcersj.109.1269_461[Crossref]
  • [6] G. Ramirez, et al., Appl. Surf. Sci. 25, 2555 (2011) http://dx.doi.org/10.1016/j.apsusc.2010.10.021[Crossref]
  • [7] S. Nagarajan, V. Raman, N. Rajendran, Materials Chemistry and Physics 119, 363 (2010) http://dx.doi.org/10.1016/j.matchemphys.2009.10.033[Crossref]
  • [8] A. Sugino, et al., Acta Biomaterialia 5, 298 (2009) http://dx.doi.org/10.1016/j.actbio.2008.07.014[Crossref]
  • [9] D. Lukito, J.M. Xue, J. Wang, Materials Letters 59, 3267 (2005) http://dx.doi.org/10.1016/j.matlet.2005.05.055[Crossref]
  • [10] A. Martínez, I. Izquierdo-Barba, M. Vallet-Regí, Chem. Mater. 12(10), 3080 (2000) http://dx.doi.org/10.1021/cm001107o[Crossref]
  • [11] G.S. Pappas, et al., Journal of Non-Crystalline Solids 354(2–9), 755 (2008) http://dx.doi.org/10.1016/j.jnoncrysol.2007.09.007[Crossref]
  • [12] J. Roman, S. Padilla, M. Vallet-Regi, Chem. Mater. 15, 798 (2003) http://dx.doi.org/10.1021/cm021325c[Crossref]
  • [13] M. Vallet-Regi, et al., Solid State Ionics 172, 441 (2004) http://dx.doi.org/10.1016/j.ssi.2004.04.037[Crossref]
  • [14] A. Ramila, F. Balas, M. Vallet-Regi, Chem. Mater. 14, 542 (2002) http://dx.doi.org/10.1021/cm0110876[Crossref]
  • [15] D. Arcos, D.C. Greenspan, M. Vallet-Regi, Chem. Mater. 14, 1515 (2002) http://dx.doi.org/10.1021/cm011119p[Crossref]
  • [16] M. Vallet-Regi, A. Ramila, Chem. Mater. 12, 961 (2000) http://dx.doi.org/10.1021/cm991110b[Crossref]
  • [17] M. Vallet-Regi, et al., J. Mater. Chem. 15, 1353 (2005) http://dx.doi.org/10.1039/b415134h[Crossref]
  • [18] J. Perez-Pariente, F. Balas, M. Vallet-Regi, Chem. Mater. 12, 750 (2000) http://dx.doi.org/10.1021/cm9911114[Crossref]
  • [19] Y. Ebisawa, T. Kokubo, K. Ohura, T. Yamamuro, J. Mater. Sci.: Mater. Med. 1, 239 (1990) http://dx.doi.org/10.1007/BF00701083[Crossref]
  • [20] E. Fujii, et al., J. Ceram. Soc. Jpn. 111(10), 762 (2003) http://dx.doi.org/10.2109/jcersj.111.762[Crossref]
  • [21] G. Lusvardi, et al., J. Phys. Chem. B 112(40), 12730 (2008) http://dx.doi.org/10.1021/jp803031z[Crossref]
  • [22] G. Lusvardi, et al., J. Phys. Chem. B 113(30), 10331 (2009) http://dx.doi.org/10.1021/jp809805z[Crossref]
  • [23] G. Lusvardi, et al., Acta Biomaterialia 5, 3548 (2009) http://dx.doi.org/10.1016/j.actbio.2009.06.009[Crossref]
  • [24] G. Falini, S. Fermani, B. Palazzo, N. Roveri, J. Biomed. Mater. Res. A. 87(2), 470 (2008)
  • [25] N.J. Coleman, M. Bellantone, J.W. Nicholson, A.P. Mendham, Ceramics-Silikáty 51(1), 1 (2007)
  • [26] L. Petit, et al., Journal of Non-Crystalline Solids 351, 2076 (2005) http://dx.doi.org/10.1016/j.jnoncrysol.2005.04.058[Crossref]
  • [27] P. Ayyub, M.S. Multani, V.R. Palkar, R. Vijayaraghavan, Phys. Rev. B 34(11), 8137 (1986) http://dx.doi.org/10.1103/PhysRevB.34.8137[Crossref]
  • [28] P. Makreski, et al., Vibrational Spectroscopy 44, 162 (2007) http://dx.doi.org/10.1016/j.vibspec.2006.11.003[Crossref]
  • [29] A. Cruz-Ramirez, et al., Journal of Fluorine Chemistry 132, 323 (2011) http://dx.doi.org/10.1016/j.jfluchem.2011.02.019[Crossref]
  • [30] J. Garcıa, et al., Journal of Non-Crystalline Solids 354, 729 (2008) http://dx.doi.org/10.1016/j.jnoncrysol.2007.07.074[Crossref]
  • [31] I. Georgieva, et al., J. Mater. Sci. 31, 3197 (1996) http://dx.doi.org/10.1007/BF00354668[Crossref]
  • [32] I. Georgieva - Mihailova, PhD Thesis (University of Chemical Technology and Metallurgy, Sofia, 1997)
  • [33] A.A. Lipovskii, et al., Journal of Non-Crystalline Solids 354, 1245 (2008) http://dx.doi.org/10.1016/j.jnoncrysol.2006.11.041[Crossref]
  • [34] A. Flambard, et al., Journal of Non-Crystalline Solids 354, 3540 (2008) http://dx.doi.org/10.1016/j.jnoncrysol.2008.03.017[Crossref]
  • [35] L.F. Santos, L. Wondraczek, J. Deubener, R.M. Almeida, Journal of Non-Crystalline Solids 353, 1875 (2007) http://dx.doi.org/10.1016/j.jnoncrysol.2007.02.018[Crossref]
  • [36] Z. Yin, et al., Hydrometallurgy 103, 215 (2010) http://dx.doi.org/10.1016/j.hydromet.2010.03.006[Crossref]
  • [37] K.R. Heier, K.R. Poeppelmeier, J. Solid State Chem. 133, 576 (1997) http://dx.doi.org/10.1006/jssc.1997.7529[Crossref]
  • [38] M. Ziolek, et al., Catalysis Today 70, 169 (2001) http://dx.doi.org/10.1016/S0920-5861(01)00416-3[Crossref]
  • [39] J. Sarkany, J. Mol. Struct. 410–411, 95 (1997) http://dx.doi.org/10.1016/S0022-2860(96)09667-6[Crossref]
  • [40] J. Sarkany, J. Mol. Struct. 410–411, 137 (1997) http://dx.doi.org/10.1016/S0022-2860(96)09686-X[Crossref]
  • [41] J. Sarkany, J. Mol. Struct. 410–411, 145 (1997) http://dx.doi.org/10.1016/S0022-2860(96)09688-3[Crossref]
  • [42] Z. Sobalik, Z. Tvaruzkova, B. Wichterlova, J. Phys. Chem. B 102, 1077 (1998) http://dx.doi.org/10.1021/jp971436c[Crossref]
  • [43] E. Broclawik, J. Datka, B. Gil, P. Kozyra, Phys. Chem. Chem. Phys. 2, 401 (2000) http://dx.doi.org/10.1039/a908832f[Crossref]
  • [44] R.F. Brandão, et al., J. Braz. Chem. Soc. 20(5), 954 (2009) http://dx.doi.org/10.1590/S0103-50532009000500022[Crossref]
  • [45] I.O. Mazali, L.C. Barbosa, O.L. Alves, J. Mater. Sci.:Mater. Med. 39, 1987 (2004)
  • [46] D. Prasetyoko, Z. Ramli, S. Endud, H. Nur, Advances in Materials Science and Engineering 2008, 1 (2008)
  • [47] Z. Ding, Zh. Yin, H. Hu, Q. Chen, Thermochimica Acta 511, 168 (2010) http://dx.doi.org/10.1016/j.tca.2010.08.010[Crossref]
  • [48] A. Olad, A. Rashidzadeh, Iranian Journal of Chemical Enineering 5(2), 45 (2008)
  • [49] H. Tang, J. Yu, X. Zhao, D.H.L. Ng, Cryst. Res. Technol. 43(5), 473 (2008) http://dx.doi.org/10.1002/crat.200711081[Crossref]
  • [50] L. Radev, et al., Processing and Application of Ceramics 4(1), 15 (2010) [Crossref]
  • [51] N. Pleshko, A. Boskey, R. Mendelsohn, Biophys. J. 60, 786 (1991) http://dx.doi.org/10.1016/S0006-3495(91)82113-0[Crossref]
  • [52] M. Markovic, B. Fowler, M.S. Tung, J. Res. Natl. Inst. Stand. Technol. 109, 553 (2004)
  • [53] V. Jokanovic, et al., J. Mater. Sci.: Mater. Med. 17, 539 (2006) http://dx.doi.org/10.1007/s10856-006-8937-z[Crossref]
  • [54] I. Rehman, W. Bonfield, J. Mater. Sci.: Mater. Med. 8, 1 (1997) http://dx.doi.org/10.1023/A:1018570213546[Crossref]
  • [55] C. Rey, M. Shimuzu, B. Collins, M.J. Glimcher, Calcif Tissue Int. 49, 383 (1991) http://dx.doi.org/10.1007/BF02555847[Crossref]
  • [56] S. Koutsopoulos, J. Biomed. Mater. Res. 62, 600 (2002) http://dx.doi.org/10.1002/jbm.10280[Crossref]
  • [57] I. Hofmann, L. Muller, P. Greil, F. Muller, J. Am. Ceram. Soc. 90(3), 821 (2007) http://dx.doi.org/10.1111/j.1551-2916.2007.01500.x[Crossref]
  • [58] O.C. Compton, F.E. Osterloh, J. Phys. Chem. C 113, 479 (2009) http://dx.doi.org/10.1021/jp807839b[Crossref]
  • [59] C. Rey, et al., Calcif. Tiss. Int. 45 157 (1989) http://dx.doi.org/10.1007/BF02556059[Crossref]
  • [60] H. Ivankovic, et al., J. Mater. Sci.: Mater. Med. 20, 1039 (2009) http://dx.doi.org/10.1007/s10856-008-3674-0[Crossref]
  • [61] H. Feki, Ch. Ren, M. Vignoles, Calcif. Tissue Int. 49, 269 (1991) http://dx.doi.org/10.1007/BF02556216[Crossref]
  • [62] M. Fleet, X. Liu, P. King, American Mineralogist 89, 1422 (2004)
  • [63] P. Regnier, et al., American Mineralogost 79, 809 (1994)
  • [64] E. Landi, G. Geloti, G. Logrocino, A. Tampieri, J. Eur. Ceram. Soc. 23, 2931 (2003) http://dx.doi.org/10.1016/S0955-2219(03)00304-2[Crossref]
  • [65] N. Hijon, M. Cabanas, I. Izquierdo-Barba, M. Vallet-Regi, Chem. Mater. 16, 1451 (2004) http://dx.doi.org/10.1021/cm031164s[Crossref]
  • [66] J. Lafon, E. Champion, D. Bernache-Assolant, J. Eur. Ceram. Soc. 28, 139 (2008) http://dx.doi.org/10.1016/j.jeurceramsoc.2007.06.009[Crossref]
  • [67] Y.-P. Guo, et al., Materials Letters, doi:10.1016/j.matlet.2011.04.057 (2011) [Crossref]
  • [68] M. Fleet, X. Liu, Biomaterials 28, 916 (2007) http://dx.doi.org/10.1016/j.biomaterials.2006.11.003[Crossref]
  • [69] I. Khairoun, et al., J. Biomed. Mater. Res. 60(4), 633 (2002) http://dx.doi.org/10.1002/jbm.10132[Crossref]
  • [70] T. Miyazaki, et al., J. Ceram. Soc. Jpn. 109(11), 929 (2001) http://dx.doi.org/10.2109/jcersj.109.1275_929[Crossref]
  • [71] S. Agathopoulos, et al., Biomaterials 27, 1832 (2006) http://dx.doi.org/10.1016/j.biomaterials.2005.10.033[Crossref]
Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-011-0129-0
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