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2011 | 9 | 6 | 972-981
Tytuł artykułu

Use of multivariate statistical techniques to optimize the separation of isoflavones by liquid chromatography

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The aim of this paper is to optimize and validate a high performance liquid chromatography (HPLC) method for separation and quantification of five isoflavones. A statistical central composite design was used to separate all peaks. These multivariate procedures were efficient in determining the optimal separation condition using resolution, capacity factor, asymmetry and number of theoretical plates. [...] The effective separation of the examined compounds was applied on a Develosil RP Aqueous AR 5 RP-30 column with a gradient mobile phase system and a DAD detector. The isolation and preconcentration of the isoflavones from urine and plasma samples were conducted by means of the solid-phase extraction (SPE). For optimize SPE conditions various sorbents were tested. Furthermore, high recoveries and good relative standard deviations were obtained when the samples were passed through the Oasis HLB column. The developed method was validated and successfully applied for determination of isoflavones in urine and plasma.
Wydawca

Czasopismo
Rocznik
Tom
9
Numer
6
Strony
972-981
Opis fizyczny
Daty
wydano
2011-12-01
online
2011-09-27
Twórcy
  • Department of Analytical Chemistry, Chemical Faculty, Silesian University of Technology, 44-100, Gliwice, Poland, irena.baranowska@polsl.pl
  • Department of Analytical Chemistry, Chemical Faculty, Silesian University of Technology, 44-100, Gliwice, Poland
  • Department of Clinical Physiology, University Hospital, SE-581 85, Linköping, Sweden
Bibliografia
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-011-0093-8
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