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2011 | 9 | 2 | 275-282
Tytuł artykułu

Synthesis and characterization of layered double hydroxides with different cations (Mg, Co, Ni, Al), decomposition and reformation of mixed metal oxides to layered structures

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Three layered double hydroxides (LDH) [Mg1−xAlx(OH)2]x+(Am−)x/m]·nH2O and [MII 1−xMIII x (OH)2]x+(Am−)x/m]·nH2O (MII - Mg, Co, Ni; MIII - Al; A - CO3 2−) were successfully synthesized by the low supersaturation method. The as-synthesized LDH samples were thermally decomposed and the derived mixed metal oxides reformed back to layered structures in water and magnesium nitrate media at different temperatures. All synthesized samples were characterized by X-ray diffraction (XRD) analysis, thermogravimetric (TG) analysis, X-ray fluorescence (XRF) analysis and scanning electron microscopy (SEM). The results of XRD and XRF analyses showed that single-phase layered double hydroxides were formed during synthesis and reformation. It was demonstrated, that a partially substituted by cobalt and nickel LDH samples also show memory effect. The crystallite size of regenerated LDH depends on the regeneration media, temperature and chemical composition. The LDH samples after regeneration consist of large particles with sharp edges along with a large amount of smaller particles
Wydawca

Czasopismo
Rocznik
Tom
9
Numer
2
Strony
275-282
Opis fizyczny
Daty
wydano
2011-04-01
online
2011-02-17
Twórcy
  • Kaunas University of Technology
  • Nature Research Centre
  • Amiagus
  • Vilnius University
Bibliografia
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-011-0007-9
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