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2010 | 8 | 6 | 1323-1330
Tytuł artykułu

pH impact on the sol-gel preparation of calcium hydroxyapatite, Ca10(PO4)6(OH)2, using a novel complexing agent, DCTA

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Aqueous sol-gel chemistry routes - based on ammonium hydrogen phosphate as the phosphorus precursor, calcium acetate monohydrate as the source of calcium ions, and 1,2-diaminocyclohexanetetraacetic acid monohydrate (DCTA) as the complexing agent - have been used to prepare calcium hydroxyapatite (HA). The sol-gel process was performed in aqueous solution at different pH values followed by calcination of the dry precursor gels for 5 h at 1000°C. Phase transformations, composition, and structural changes in the polycrystalline samples were studied by thermoanalytical methods (TG/DTA), infrared spectroscopy (IR), X-ray powder diffraction analysis (XRD), and scanning electron microscopy (SEM). It was shown that pH adjustment has significant impact on the apatite formation process and on the morphology and phase purity of the ceramic samples.
Wydawca

Czasopismo
Rocznik
Tom
8
Numer
6
Strony
1323-1330
Opis fizyczny
Daty
wydano
2010-12-01
online
2010-10-08
Twórcy
  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania
  • Laboratory of Inorganic Materials, Tallinn University of Technology, 19086, Tallinn, Estonia
autor
  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania
  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-010-0113-0
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