PL EN


Preferencje help
Widoczny [Schowaj] Abstrakt
Liczba wyników
Czasopismo
2010 | 8 | 2 | 264-268
Tytuł artykułu

A preliminary study on the effect of mineralization parameters on determination of metals in Viscum album species

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
An increasing interest in determination of various macro- and microelements in medicinal plants has been observed. The majority of studies are carried out using one mineralization method without any optimization. The present study demonstrates that changes in mineralization parameters can significantly affect the recovery of the elements determined. In the study, the dried plant material was mineralized in 12 ways and iron (Fe), copper (Cu), zinc (Zn), nickel (Ni) and manganese (Mn) levels were determined. The samples were mineralized in the dry or open microwave mode as well as 10 closed microwave modes. The influence of acid amounts, irradiation power and time, addition of hydrogen peroxide and perfluoric acid was examined. All parameters were shown to be critical - good efficiency was observed with larger amounts of acid. The determined content varied significantly in the same sample and were in the ranges (ug g−1): 46–136 (Fe), 1.4–11.8 (Cu), 4.0–11.3 (Ni), 15.4–53.8 (Zn) and 9.5–67.6 (Mn). Increased irradiation resulted in the loss of copper and zinc and better recovery of nickel. The results demonstrate that such determinations should include the mineralization optimization step. [...]
Wydawca

Czasopismo
Rocznik
Tom
8
Numer
2
Strony
264-268
Opis fizyczny
Daty
wydano
2010-04-01
online
2010-03-23
Twórcy
  • Department of Analytical Chemistry, Medical University of Lublin, 20-081, Lublin, Poland
  • Department of Analytical Chemistry, Medical University of Lublin, 20-081, Lublin, Poland
  • Department of Medicinal Chemistry, Medical University of Lublin, 20-090, Lublin, Poland
autor
  • Department of Analytical Chemistry, Medical University of Lublin, 20-081, Lublin, Poland
Bibliografia
  • [1] E.D. Caldas, L.L. Machado, Food Chem. Toxicol. 42, 599 (2003) [Crossref]
  • [2] E. Ernst, Eur. J. Clin. Pharmacol. 62, 1 (2006) http://dx.doi.org/10.1007/s00228-005-0070-2[Crossref]
  • [3] E. Ernst, Pharmacoepid. Drug Safety 13, 767 (2004) http://dx.doi.org/10.1002/pds.1014[Crossref]
  • [4] E. Ernst, Tr. Pharm. Sci. 23, 136 (2002) http://dx.doi.org/10.1016/S0165-6147(00)01972-6[Crossref]
  • [5] S.C. Smolinske, J. Pharm. Pract. 18, 188 (2002) http://dx.doi.org/10.1177/0897190005277217[Crossref]
  • [6] S. Latinca, S. Biljana, N. Miljević, Environ. Chem. Lett. 2, 105 (2004) http://dx.doi.org/10.1007/s10311-004-0073-8[Crossref]
  • [7] C. Bin, W. Xiaouru, F.S.C. Lee, Anal. Chim. Acta 447, 161 (2001) http://dx.doi.org/10.1016/S0003-2670(01)01218-1[Crossref]
  • [8] K. Szentmihályi, M. Hajdú, J. Fodor, L. Kótai, A. Blázovics, A. Somogyi, M. Then, Biol. Trace Elem. Res. 114, 143 (2006) http://dx.doi.org/10.1385/BTER:114:1:143[Crossref]
  • [9] Z. Lamari, S. Landsberger, J. Braisted, H. Neggache, R. Larbi, J. Radioanal. Nucl. Chem. 276, 95 (2008) http://dx.doi.org/10.1007/s10967-007-0415-7[Crossref]
  • [10] R. Chizzola, B. Lukas, Water, Air, Soil Pollut. 170, 331 (2006) http://dx.doi.org/10.1007/s11270-005-9004-y[Crossref]
  • [11] R. Chizzola, H. Michitsch, C. Franz, Eur. Food Res. Technol. 216, 407 (2003)
  • [12] V. Angelova, K. Ivanov, R. Ivanova, J. Herbs, Spices and Medicinal Plants 11, 37 (2006) http://dx.doi.org/10.1300/J044v11n04_05[Crossref]
  • [13] C.Y. Chen, Phytochem. Anal. 16, 315 (2005) http://dx.doi.org/10.1002/pca.850[Crossref]
  • [14] J.Y. Wang et al., Zhongguo Zhongyao Zazhi 29, 758 (2004) (in Chinese)
  • [15] M.K. Wong, P. Tan, Y.C. Wee, Biol. Trace Elem. Res. 36, 135 (1993) http://dx.doi.org/10.1007/BF02783172[Crossref]
  • [16] J. Wu, Y. Zou, X. Zhan, S. Chen, G. Lu, F. Lai, Bull. Environ. Contam. Toxicol. 81, 571, (2008) http://dx.doi.org/10.1007/s00128-007-9170-2[Crossref]
  • [17] Y. Wu, Z. Zhou, Y. Xiong, Y. Wang, J. Sun, Zhongguo Zhongyao Zazhi 24, 84 (1999) (in Chinese)
  • [18] M.F. Ali, Y.H. Lee, W. Ratnam, J. Nais, R. Ripin, Fresenius Environ. Bull. 15, 1316 (2006)
  • [19] E.I. Obiajunwa, A.C. Adebajo, O.R. Omobuwajo, J. Radioanal. Nucl. Chem. 252, 473 (2002) http://dx.doi.org/10.1023/A:1015838300859[Crossref]
  • [20] I. Baranowska, K. Srogi, A. Włochowicz, K. Szczepanik, Pol. J. Environ. Stud. 11, 467 (2002)
  • [21] P. Kalny, Z. Fijałek, A. Daszczuk, P. Ostapczuk, Sci. Total Environ. 381, 99 (2007) http://dx.doi.org/10.1016/j.scitotenv.2007.03.026[Crossref]
  • [22] M. Wesołowski, P. Konieczyński, Chem. Anal. (Warsaw) 41, 377 (1996)
  • [23] S. Razic, S. Dogo, L. Slavkovic, J. Natural Med. 62, 340 (2008) http://dx.doi.org/10.1007/s11418-008-0240-5[Crossref]
  • [24] S. Basgel, S.B. Erdemoglu, Sci. Total Environ. 359 82, (2006) http://dx.doi.org/10.1016/j.scitotenv.2005.04.016[Crossref]
  • [25] N. Sekeroglu, F. Ozkutlu, S.M. Kara, M. Ozguven, J. Sci. Food Agr. 88, 86 (2008) http://dx.doi.org/10.1002/jsfa.3048[Crossref]
  • [26] J. Kalembkiewicz, E. Sitarz-Palczak, Atomic Spectr. 22, 433 (2001)
  • [27] J. Rejnek, Chem. Listy 96, 1010 (2002)
  • [28] M.T. Vidal, M.C. Pascual-Marti, A. Salvador, C. Llabata, Microchem. Journal 72, 221 (2002) http://dx.doi.org/10.1016/S0026-265X(02)00037-1[Crossref]
Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-009-0133-9
JavaScript jest wyłączony w Twojej przeglądarce internetowej. Włącz go, a następnie odśwież stronę, aby móc w pełni z niej korzystać.