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2010 | 8 | 1 | 28-33
Tytuł artykułu

Hydrate of 2,3:4,5-di-O-isopropylidene-β-D-arabino-hexos-2-ulo-2,6-pyranose as new crystalline reagent in the preparation of Amadori derived peptides

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
We established, that crystalline hydrate of 2,3:4,5-di-O-isopropylidene-β-D-arabino-hexos-2-ulo-2,6-pyranose is a new, convenient and stable reagent for solid phase synthesis of peptide derived Amadori products. The structure of the title compound was studied by X-ray analysis, NMR spectroscopy, and high resolution ESI-MS. The crystal structure indicated the existence of two symmetry-independent molecules that were not connected with hydrogen bonds. A comparison with previously reported 2,3:4,5-di-O-isopropylidene-β-D-fructopyranose revealed, that these two compounds are isostructural. [...]
Wydawca

Czasopismo
Rocznik
Tom
8
Numer
1
Strony
28-33
Opis fizyczny
Daty
wydano
2010-02-01
online
2010-02-16
Twórcy
  • Faculty of Chemistry, University of Wrocław, 50-383, Wrocław, Poland, stp@wchuwr.pl
  • Faculty of Chemistry, University of Wrocław, 50-383, Wrocław, Poland
  • Faculty of Chemistry, University of Wrocław, 50-383, Wrocław, Poland
  • Faculty of Chemistry, University of Wrocław, 50-383, Wrocław, Poland
  • Faculty of Chemistry, University of Wrocław, 50-383, Wrocław, Poland
autor
  • Faculty of Chemistry, University of Wrocław, 50-383, Wrocław, Poland
Bibliografia
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-009-0123-y
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