Carbon ceramic electrode incorporated with zeolite ZSM-5 for determination of Piroxicam

• Autorzy: Karim Asadpour-Zeynali , Mir Majidi , Mitra Zarifi
• Języki publikacji: EN

Abstrakty

EN

A new chemically modified electrode is constructed based on carbon ceramic electrode incorporated with zeolite ZSM-5. Voltammetric behavior of piroxicam at the carbon ceramic zeolite modified electrode (CCZME) was investigated. The modified electrode exhibited catalytic activity toward the electrooxidation of piroxicam. Experimental parameters such as solution pH, scan rate, concentration of piroxicam and zeolite amount were studied. It has been shown that using the CCZME, piroxicam can be determined by differential pulse voltammetry (DPV) and hydrodynamic amperometry (HA). Under the optimized conditions the calibration plots are linear in the concentration ranges of 0.20–25.00 and 0.20–50.10 μM with limit of detections of 0.65 and 0.29 μM for DPV and HA, respectively. The modified electrode with DPV and HA methods was successfully applied for analysis of piroxicam in pharmaceutical formulations. The results were favorably compared to those obtained by the spiked method. The results of the analysis suggest that the proposed method has promise for the routine determination of piroxicam in the products examined. [...]

Słowa kluczowe

EN

Carbon Ceramic Clectrode; Modified Electrode; Piroxicam; Differential Pulse Voltammetry; Amperometry

• Czasopismo: Open Chemistry
• Rocznik: 2010
• Tom: 8
• Numer: 1
• Strony: 155-162

Daty

wydano

2010-02-01

online

2010-02-16

Twórcy

autor

Karim Asadpour-Zeynali

• Department of Analytical Chemistry, Faculty of Chemistry, University of Tabriz, Tabriz, 51666-16471, Iran,

autor

Mir Majidi

• Department of Analytical Chemistry, Faculty of Chemistry, University of Tabriz, Tabriz, 51666-16471, Iran

autor

Mitra Zarifi

• Department of Analytical Chemistry, Faculty of Chemistry, University of Tabriz, Tabriz, 51666-16471, Iran

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Identyfikatory

DOI

10.2478/s11532-009-0122-z