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2009 | 7 | 1 | 143-147
Tytuł artykułu

Determination of penicillin V potassium in pharmaceuticals and spiked human urine by chemiluminescence

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
A simple and selective method for penicillin V potassium (PVK) determination by chemiluminescence (CL) was developed. Oxidation of PVK by alkaline hydrogen peroxide produces CL, which is greatly enhanced by N, N-dimethyl formamide (DMF) and N-cetyl-N,N,N-trimethylammonium bromide (CTMAB). Optimum conditions were established using luminometry. There is a linear relationship between the chemiluminescent peak height and the amount of PVK within the range 0.5–129.5 mg L−1, with a detection limit of 0.2 mg L−1. The coefficient of variation was 1.2% for 40 mg L−1 PVK solution (n = 7). The method is very simple, has high sensitivity and good selectivity, and is usable for process control. It was successfully utilized for the determination of PVK in pharmaceuticals and spiked human urine. [...]
Wydawca

Czasopismo
Rocznik
Tom
7
Numer
1
Strony
143-147
Opis fizyczny
Daty
wydano
2009-03-01
online
2008-12-23
Twórcy
autor
  • Analytical Chemistry Department, Faculty of Chemistry, University of Tabriz, Tabriz, Iran
  • Analytical Chemistry Department, Faculty of Chemistry, University of Tabriz, Tabriz, Iran
Bibliografia
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-008-0092-6
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