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2009 | 7 | 1 | 66-73
Tytuł artykułu

Synthesis and structural characterization of amino-functionalized polysaccharides

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
A variety of carbohydrates, in particular polysaccharides can be subjected to chemical modification to obtain derivatives with amphiphilic properties, which enable biochemical or biological reactions at the polymer surface. In the present work, a polydisperse maltodextrin mixture of average molecular weight 3000 was coupled with 1,6-hexamethylenediamine (HMD) via reductive amination reaction. Resulting products were characterized by thermal analysis and positive nanoelectrospray quadrupole time-of-flight (Q-TOF) mass spectrometry (MS) and tandem mass spectrometry (MS/MS). Both thermal analysis and MS screening confirmed the formation of the HMD-polysaccharide coupling products. Moreover, HMD-linked polysaccharide chains containing 2 to 26 glucose building blocks were identified by nanoESI Q-TOF MS. MS/MS fragmentation using collision-induced dissociation (CID) at low ion acceleration energies provided strong evidence for HMD-maltodextrin linkage formation and the set of sequence ions diagnostic for the composition and structure of a HMD-linked chain containing 18 glucose residues. [...]
Wydawca

Czasopismo
Rocznik
Tom
7
Numer
1
Strony
66-73
Opis fizyczny
Daty
wydano
2009-03-01
online
2008-12-23
Twórcy
autor
  • Institute of Chemistry, Romanian Academy, RO-300223, Timisoara, Romania
autor
  • Department of Chemical and Biological Sciences, “Aurel Vlaicu” University of Arad, Romania, RO-310130, Arad, Romania
  • Department of Chemical and Biological Sciences, “Aurel Vlaicu” University of Arad, Romania, RO-310130, Arad, Romania
  • Faculty of Industrial Chemistry and Environment Engineering, “Politehnica” University of Timisoara, RO-300030, Timisoara, Romania
autor
Bibliografia
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-008-0090-8
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