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2007 | 5 | 1 | 169-176
Tytuł artykułu

Low temperature synthesis and characterization of Mn3O4 nanoparticles

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Heating hydrous manganese (II) hydroxide gel at 85 °C for 12 hours produces Mn3O4 nanoparticles. They were characterized by X-ray powder diffraction (XRD) and infrared spectroscopy (FTIR). The particle size estimated from the SEM and X-ray peak broadening is approximately 32 nm, showing them to be nanocrystalline. EPR measurements confirm a typical Mn2+signal with a highly resolved hyperfine structure. [...]
Słowa kluczowe
EN
Mn3O4   Nanoparticle   XRD   FTIR   EPR  
Wydawca

Czasopismo
Rocznik
Tom
5
Numer
1
Strony
169-176
Opis fizyczny
Daty
wydano
2007-03-01
online
2007-03-01
Twórcy
  • Department of Chemistry, Fatih University, 34500, Buyukcekmec, Istanbul, Turkey, hbaykal@fatih.edu.tr
  • Department of Physics, Fatih University, 34500, Buyukcekmec, Istanbul, Turkey
  • Department of Chemistry, Fatih University, 34500, Buyukcekmec, Istanbul, Turkey
Bibliografia
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  • [15] S.K. Apte, S.D. Naik, R.S. Sonawane, B.B. Kale, N. Pavaskar, A.B. Mandale and B.K. Das: “Nanosize Mn3O4 (Hausmannite) by a Microwave Irradiation Method”, Mater. Res. Bull., Vol. 41, (2006), pp. 647–654. http://dx.doi.org/10.1016/j.materresbull.2005.08.028[Crossref]
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  • [21] Y. Köseođlu, F. Yıldız, J.V. Yakhmi, J. Qin, X. Chen and B. Aktas: “EPR Studies on BEDT-TTF Intercalated MnPS3 Molecular Magnets”, J. Magn. Magn. Mater., Vol. 416, (2003), pp. 258–259. [Crossref]
  • [22] W. Zhang, Z. Yang, Y. Liu, S. Tang, X. Han and M. Chen: “Controlled Synthesis of Mn3O4 Nanocrystallites and MnOOH Nanorods by a Solvothermal Method”, J. Cryst. Growth, Vol. 263, (2004), pp. 394–399. http://dx.doi.org/10.1016/j.jcrysgro.2003.11.099[Crossref]
  • [23] T. B. Demirci, Y. Köseođlu, S. Güner and B. Ülküseven: “Oxovanadium (IV) Complexes of Bromo-and Methoxy-substituted N1,N4-diarylidene-S-methylthiosemicarbazones”, Cent. Eur. J. Chem., Vol. 4(1), (2006), pp. 149–159. http://dx.doi.org/10.1007/s11532-005-0011-z[Crossref]
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_s11532-006-0064-7
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