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2003 | 1 | 3 | 201-221
Tytuł artykułu

On the possibilities of ICP-AES for analysis of archaeological bones

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The possibility of using inductively coupled plasma atomic emission spectrometry (ICP-AES) to determine the elemental composition of archaeological bones elements was evaluated and discussed. The interferences of the major elements (Ca, P, K, Na, Al and Fe) on the microelements (Ba, Cd, Co, Cr, Cu, Mn, Ni, Pb, Sr, Zn) were investigated and the appropriate analytical lines were selected. The role of different nebulizers (cross-flow, Babington and Meinhard) on detection limits were investigated. The applicability of the proposed procedure was demonstrated analyzing IAEA-SRM-H-5 (Animal bone); and authentic bone sample dating back to the 4th century BC. These results were compared to ETAAS and ICP-MS.
Wydawca

Czasopismo
Rocznik
Tom
1
Numer
3
Strony
201-221
Opis fizyczny
Daty
wydano
2003-09-01
online
2003-09-01
Twórcy
autor
autor
  • Faculty of Chemistry, University of Sofia, 1, James Bouchier Ave, Sofia, Bulgaria
autor
  • Faculty of Chemistry, University of Sofia, 1, James Bouchier Ave, Sofia, Bulgaria
Bibliografia
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  • [5] J.H. Burton and T.D. Price: “The Use and Abuse of Trace-Elements for Paleodietary Inferences”, In: S.H. Ambrose and M.A. Katzenberg, Eds.: Biochemical Approaches to Paleodietary Analysis, Kluwer Academic/Plenum Publishers, Berlin, 2000, pp. 159–171.
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  • [8] N. Piguitore, G. Cruz-Jemenez, T.D. Price: “Incorporation of Trace Elements in Ancient and Modern, Human Bones: A X-ray Absorption Spectroscopy Study”, Trans. AGU, Vol. 82 (47), Abstr. No. B22A-0136, (2001).
  • [9] Y.C. Yoo, S.K. Lee, J.Y. Yang, S.W. In, K.W. Kim, K.H. Chung, M.G. Chung, S.Y. Choung: “Organ Distribution of Heavy Metals in Autopsy Material from North Corea”, Journal of Health Science, Vol. 48, (2002), pp. 186–193. http://dx.doi.org/10.1248/jhs.48.186[Crossref]
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  • [17] R.G.V. Hancock, M.D. Grynpas, K.P. Pritzker: “The Abuse of Bone Mineral Analysis for Archaeological Dietary Studies”, Archaeometry, Vol. 31, (1989), pp. 169–179. [Crossref]
  • [18] R.G.V. Hancock, M.D. Grynpas, K. Akesson, K. Obrant, J. Trunquist, M. Kessler: “Baselines and Variabilites of Major and Trace Elements in Bone”, In: J. Lambert and G. Grupe, Eds.: Prehistoric Human Bone. Archaeology at the Molecular Level, Springer-Verlag, Berlin, 1993, pp. 189–201.
  • [19] S. Safont, A. Malgosa, M.E. Subira, J. Gibert: “Placing the Orce Homind into the Trophic Chain. Trace Element Analysis by ICP-MS in the Venta Micena Site (Orce, Granada, Spain)”, In: Pros. XIII Intern. Congr. Prehistoric and Protohistoric Science, Forli, (Italy), 1996, Forli, 1996, Vol. 1, pp. 297–303.
  • [20] M.E. Subira and A. Malgosa: “Alkaline Earth Metal Content of Human Bones at the Site “S’Illot des Porros” (Iron Age, Mallorca, Spain)”, International Journal of Osteoarchaeology, Vol. 6, (1991), pp. 225–231.
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  • [24] J. Lee: “Calcium Matrix Effects in Multi-Element Analysis of Animal Bone by Inductively-Coupled Plasma Atomic-Emission Spectrometry”, Analytica Chimica Acta, Vol. 152, (1983), pp. 141–147. http://dx.doi.org/10.1016/S0003-2670(00)84904-1[Crossref]
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  • [29] I. Kuleff, R. Djingova, B. Zlateva: “Archaeometric Investigations of Bones from Thrace”, Archaeologia Bulgarica, Vol. 3, (2000), pp. 7–12.
  • [30] B. Zlateva, R. Djingova, I. Kuleff: “Multi-element Analysis of Bones for Dietary Reconstruction of the Inhabitants of Thracia at Hellenistic Times (Bulgaria)”, Berliner Beiträger zur Archaeometrie, Vol. 20, (2003), in press.
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  • [32] B. Zlateva and I. Kuleff: “Reconstruction of paleodiet by the chemical analysis of bones”, Archaeologia Bulgarica, Vol. VII (2), (2003), (in press).
Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_2478_BF02476224
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