Nowa wersja platformy jest już dostępna.
Przejdź na


Preferencje help
Widoczny [Schowaj] Abstrakt
Liczba wyników
2014 | 2 | 1 |
Tytuł artykułu

Design of experiment in the development of spme method for the determination of pesticide residues in fruits and vegetables

Treść / Zawartość
Warianty tytułu
Języki publikacji
The various microextraction techniques have been developed in order to reduce sample preparation time, improve sensitivity and selectivity as well as to corroborate the recent advances in the development of highly sensitive and efficient analytical instrumentation. The current trend is aimed at the simplification and miniaturization of extraction steps, which has led to the combination of multi-step extraction and analytical analysis into single uninterrupted step. The method development involves the screening and subsequent optimization of both gas chromatography-mass spectrometry (GC-MS) and solid phase microextraction (SPME) parameters using multivariate experimental design, which has been shown to be efficient and effective with little experimental runs. The use of microextraction has been very effective in the analysis of contaminants in food, water and the environments to ensure they are safe and does not pose any health risk to human.
Słowa kluczowe

Opis fizyczny
  • Department of
    Chemical, Geological and Physical Sciences, College of Pure and
    Applied Sciences, Kwara State University, Malete, P.M.B. 1530, Ilorin,
    Kwara State
  • Department of Chemistry,
    Faculty of Science, University of Malaya, 50603, Pantai Valley, Kuala
    Lumpur, Malaysia
  • Department of Chemistry,
    Faculty of Science, University of Malaya, 50603, Pantai Valley, Kuala
    Lumpur, Malaysia
  • [1] Kataoka, H., Recent developments and applications of microextractiontechniques in drug analysis, Anal. Bioanal. Chem.,2010, 396, 339-364.
  • [2] Spietelun, A., Kloskowski, A., Chrzanowski, W., Namiesnik,J., Understanding solid-phase microextraction: Key factorsinfluencing the extraction process and trends in improving thetechnique, Chem. Rev., 2013, 113, 1667-1685.
  • [3] Abdulra’uf, L.B., Chai, M.K., Tan, G.H., Applications ofsolid-phase microextraction for the analysis of pesticideresidues in fruits and vegetables: A review, J. AOAC Int., 2012,95, 1272-1290.
  • [4] Nerín, C., Salafranca, J., Aznar, M., Batlle, R., Critical review onrecent developments in solventless techniques for extraction ofanalytes, Anal. Bioanal. Chem., 2009, 393, 809-833.
  • [5] Tan, G.H., Abdulra’uf, L.B., Recent developments andapplications of microextraction techniques for the analysis ofpesticide residues in fruits and vegetables, in Soundararajan,R.P. (Ed.), Pesticides - recent trends in pesticide residue assay,InTech: Rijeka, 2012, 171-190.
  • [6] Abdulra’uf, L.B., Sirhan, A.Y., Tan, G.H., Recent developmentsand applications of liquid phase microextraction in fruits andvegetables analysis, J. Sep. Sci., 2012, 35, 3540-3553.
  • [7] Jain, A., Verma, K.K., Recent advances in applications ofsingle-drop microextraction: A review, Anal. Chim. Acta, 2011,706, 37-65.
  • [8] Beltran, J., Lopez, F.J., Hernandez, F., Solid-phase microextractionin pesticide residue analysis, J. Chromatogr. A, 2000,885, 389-404.
  • [9] Abdulra’uf, L.B., Hammed, W.A., Tan, G.H., Spme fibers forthe analysis of pesticide residues in fruits and vegetables: Areview, Crit. Rev. Anal. Chem., 2012, 42, 152-161.
  • [10] Kataoka, H., Lord, H.L., Pawliszyn, J., Applications ofsolid-phase microextraction in food analysis, J. Chromatogr. A,2000, 880, 35–62.
  • [11] Lord, H., Strategies for interfacing solid-phase microextractionwith liquid chromatography, J. Chromatogr. A, 2007, 1152, 2-13.
  • [12] Aulakh, J.S., Malik, A.K., Kaur, V., Schmitt-Kopplin, P., A reviewon solid phase micro extraction-high performance liquidchromatography (spme-hplc) analysis of pesticides, Crit. Rev.Anal. Chem., 2005, 35, 71–85.
  • [13] Lambropoulou, D.A., Konstantinou, I.K., Albanis, T.A., Recentdevelopments in headspace microextraction techniques for theanalysis of environmental contaminants in different matrices, J.Chromatogr. A, 2007, 1152 70–96.
  • [14] Kumar, A., Gaurav, Malik, A.K., Tewary, D.K., Singh, B., A reviewon development of solid phase microextraction fibers by sol-gelmethods and their applications, Anal. Chim. Acta, 2008, 610,1-14.
  • [15] De Fátima Alpendurada, M., Solid-phase microextraction: Apromising technique for sample preparation in environmentalanalysis, J. Chromatogr. A., 2000, 889, 3-14.
  • [16] Spietelun, A., Marcinkowski, T., de la Guardia, M., Namieśnik,J., Recent developments and future trends in solid phasemicroextraction techniques towards green analytical chemistry,Journal of Chromatography A, 2013, 1321, 1-13.
  • [17] Lord, H., Bojko, B., Drug analysis by spme, in Pawliszyn, J.(Ed.), Handbook of solid phase microextraction, Elsevier:Waltham, USA, 2012, 335-382.
  • [18] Kataoka, H., Recent developments and applications of microextractiontechniques in drug analysis, Anal. Bioanal. Chem.,2010, 396, 339-364.
  • [19] IUPAC, A vision for chemistry for 2050, in ChemistryInternational, 2012, IUPAC, Boston, USA.
  • [20] Araoud, M., Douki, W., Rhim, A., Najjar, M.F., Gazzah, N.,Multiresidue analysis of pesticides in fruits and vegetables bygas chromatography-mass spectrometry, J. Environ. Sci. Heal.B, 2007, 42, 179-187.
  • [21] Cabras, P., Pesticides: Toxicology and residues in food, inD’Mello, J.P.F. (Ed.), Food safety: Contaminants and toxins, CABIPublishing: Cambridge, MA, USA, 2003, 91-124.
  • [22] Chai, M.K., Tan, G.H., Asha, I., Optimization of headspacesolid-phase microextraction for the determination of pesticideresidues in tomatoes, Anal. Sci., 2008, 24, 273-276.
  • [23] Maharaj, R., Use of insecticides for malaria control and needsfor reversion of resistance, Indian J. Med. Res., 2010, 132,248-250.
  • [24] Sharma, D., Nagpal, A., Pakade, Y.B., Katnoria, J.K., Analyticalmethods for estimation of organophosphorus pesticideresidues in fruits and vegetables: A review, Talanta, 2010, 82,1077-1089.
  • [25] Garrido Frenich, A., Del Mar Martín Fernández, M., DíazMoreno, L., Martínez Vidal, J.L., López-Gutiérrez, N.,Multiresidue pesticide analysis of tuber and root commoditiesby quechers extraction and ultra-performance liquid chromatographycoupled to tandem mass spectrometry, J. AOAC Int.,2012, 95, 1319-1330.
  • [26] Guo, X., Zhang, X., Cai, Q., Shen, T., Zhu, S., Developing a novelsensitive visual screening card for rapid detection of pesticideresidues in food, Food Control, 2013, 30, 15-23.[Crossref]
  • [27] Lambropoulou, D.A., Albanis, T.A., Liquid-phase microextractiontechniques in pesticide residue analysis, J. Biochem.Biophys. Meth., 2007, 70, 195-228.
  • [28] Lambropoulou, D.A., Albanis, T.A., Methods of samplepreparation for determination of pesticide residues in foodmatrices by chromatography–mass spectrometry-basedtechniques: A review, Anal. Bioanal. Chem., 2007, 389,1663-1683.
  • [29] Arthur, C.L., Killam, L.M., Buchholz, K.D., Pawliszyn, J., Berg,J.R., Automation and optimization of solid-phase microextraction,Anal. Chem., 1992, 64, 1960-1966.
  • [30] Shirey, R.E., Spme commercial devices and fiber coatings, inPawliszyn, J. (Ed.), Handbook of solid phase microextraction,Elsevier: Waltham, USA, 2012, 97-133.
  • [31] Arthur, C.L., Pawliszyn, J., Solid phase microextraction withthermal desorption using fused silica optical fibers, Anal.Chem., 1990, 62, 2145-2148.
  • [32] Lord, H., Pawliszyn, J., Evolution of solid-phase microextractiontechnology, J. Chromatogr. A, 2000, 885, 153-193.
  • [33] Pawliszyn, J., Pawliszyn, B., Pawliszyn, M., Solid phasemicroextraction (spme), The Chem. Educ., 1997, 2, 1-7.[Crossref]
  • [34] Risticevic, S., Niri, V.H., Vuckovic, D., Pawliszyn, J., Recentdevelopments in solid-phase microextraction, Anal. Bioanal.Chem., 2009, 393, 781–795.
  • [35] Pawliszyn, J., Quantitative aspect of solid phase microextraction,in Pawliszyn, J. (Ed.), Applications of solid phasemicroextraction, Royal Society of Chemistry: Cambridge, 1999,3-21.
  • [36] Risticevic, S., Lord, H., Górecki, T., Arthur, C.L., Pawliszyn, J.,Protocol for solid-phase microextraction method development,Nat. Protoc., 2010, 5, 122 - 139.
  • [37] Pawliszyn, J., New directions in sample preparation for analysisof organic compounds, TrAC - Trends Anal. Chem., 1995, 14,113-122.
  • [38] Zhang, Z., Pawliszyn, J., Headspace solid-phase microextraction,Anal. Chem., 1993, 65, 1843-1852.
  • [39] Ai, J., Solid-phase microextraction in headspace analysis.Dynamics in non- steady-state mass transfer, Anal. Chem.,1998, 70, 4822-4826.
  • [40] Ai, J., Headspace solid phase microextraction. Dynamics andquantitative analysis before reaching a partition equilibrium,Anal. Chem., 1997, 69, 3260-3266.
  • [41] Pawliszyn, J., Solid phase picroextraction: Theory and practice.VCH, New York, 1997.
  • [42] Ai, J., Solid phase microextraction for quantitative analysis innonequilibrium situations, Anal. Chem., 1997, 69, 1230-1236.
  • [43] Pawliszyn, J., Pawliszyn, B., Pawliszyn, M., Solid phasemicroextarction (spme), The Chem. Educ., 1997, 2, 1-7.[Crossref]
  • [44] Pawliszyn, J., Theory of solid-phase microextraction, inPawliszyn, J. (Ed.), Handbook of solid phase microextraction,Elsevier: Waltham, USA, 2012, 13-59.
  • [45] Wardencki, W., Michulec, M., Curyło, J., A review of theoreticaland practical aspects of solid-phase microextraction in foodanalysis, Int. J. Food Sci. Technol., 2004, 39, 703–717.
  • [46] Kudlejova, L., Risticevic, S., Vuckovic, D., Solid-phase microextractionmethod development, in Pawliszyn, J. (Ed.), Handbookof solid phase microextraction, Elsevier: Waltham, USA, 2012.
  • [47] Zhang, Z., Yang, M.J., Pawliszyn, J., Solid-phase microextraction,Anal. Chem., 1994, 66, 844A-853A.
  • [48] Abdulra’uf, L.B., Hammed, W.A., Tan, G.H., Spme fibers forthe analysis of pesticide residues in fruits and vegetables: Areview, Crit. Rev. Anal. Chem., 2012, 42, 152-161.
  • [49] Sarafraz-Yazdi, A., Amiri, A., Liquid-phase microextraction,TrAC, Trends Anal. Chem., 2010, 29, 1-14.
  • [50] Zeng, J., Chen, J., Lin, Z., Chen, W., Chen, X., Wang, X.,Development of polymethylphenylsiloxane-coated fiber forsolid-phase microextraction and its analytical applicationof qualitative and semi-quantitative of organochlorine andpyrethroid pesticides in vegetables, Anal. Chim. Acta, 2008,619, 59-66.
  • [51] Eisert, R., Pawliszyn, J., Design of automated solid-phasemicroextraction for trace analysis of organic compounds inaqueous samples, J. Chromatogr. A, 1997, 776, 293-303.
  • [52] Ouyang, G., Pawliszyn, J., A critical review in calibrationmethods for solid-phase microextraction, Anal. Chim. Acta,2008, 627, 184-197.
  • [53] Ebrahimi-Najafabadi, H., Leardi, R., Jalali-Heravi, M.,Experimental design in analytical chemistry-part i: Theory, J.AOAC Int., 2014, 97, 3-11.
  • [54] Miller, J.N., Miller, J.C., Statistics and chemometrics foranalytical chemisry, 6th ed. Pearson, Essex, England, 2010.
  • [55] Massart, D.L., Vandaginste, B.G.M., Buydens, L.M.C., De Jong,S., Lewi, P.J., Smeyers-Verbeke, J., Handbook of chemometricsand qualimetrics: Part a. Elsevier, Amsterderm, TheNetherlands, 1997.
  • [56] Stalikas, C., Fiamegos, Y., Sakkas, V., Albanis, T., Developmentson chemometric approaches to optimize and evaluate microextraction,J. Chromatogr. A, 2009, 1216, 175-189.
  • [57] Montgomery, D.C., Design and analysis of experiments. JohnWiley and Sons, New Jersey, 2009.
  • [58] Winer, B.J., Statistical principles in experimental design, 3rded. McGraw-Hill, New York, 1991.
  • [59] Minitab software for quality improvement; Available
  • [60] López, R., Goñi, F., Etxandia, A., Millán, E., Determination oforganochlorine pesticides and polychlorinated biphenyls inhuman serum using headspace solid-phase microextractionand gas chromatography-electron capture detection, J.Chromatogr. B., 2007, 846, 298-305.
  • [61] Abdulra’uf, L.B., Tan, G.H., Chemometric approach to theoptimization of hs-spme/gc–ms for the determination ofmulticlass pesticide residues in fruits and vegetables, FoodChem., 2015, 177, 267-273.
  • [62] Abdulra’uf, L.B., Tan, G.H., Multivariate study of parameters inthe determination of pesticide residues in apple by headspacesolid phase microextraction coupled to gas chromatography–mass spectrometry using experimental factorial design, FoodChemistry, 2013, 141, 4344-4348.
Typ dokumentu
Identyfikator YADDA
JavaScript jest wyłączony w Twojej przeglądarce internetowej. Włącz go, a następnie odśwież stronę, aby móc w pełni z niej korzystać.