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2015 | 13 | 1 |
Tytuł artykułu

Development and validation of the simple and sensitive spectrophotometric method of sulphanilamides determination with 4-(2-thiazolylazo)-resorcinol in veterinary preparations

Treść / Zawartość
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
New simple, rapid, and accurate spectrophotometric techniques for sulphanilamides assay in combination drugs have been elaborated. The method is based on the formation of coloured products of sulphanilamides diazonium salt azoсoupling with heterocyclic azo reagent 4-(2-thiazolylazo)-resorcinol (TAR) in alkaline medium (pH 9.5) with the following measurement of their absorbance at λmax = 615 nm. Formed products are stable for 1 hour at room temperature. Effective molar absorptivities at absorbance maximum 615 nm for disazo dyes were ~ 104 M-1 cm-1. Linear ranges for sulphanilamides determination were 0.5−30.0 μg mL-1. The developed method was used for the suphanilamides determination in tablets, powder, solutions, suspensions and ointments.
EN
Wydawca

Czasopismo
Rocznik
Tom
13
Numer
1
Opis fizyczny
Daty
otrzymano
2014-09-22
zaakceptowano
2015-04-02
online
2015-10-21
Twórcy
  • Ivan Franko Lviv National University, Chemistry Faculty, Analytical Chemistry Department, Kyrylо & Mefodiy Str., 6, 79005, Lviv, Ukraine
  • State Scientific Research Control Institute of Veterinary Preparations and Fodder Additives, Donetska Str.,11, 79019, Lviv, Ukraine
autor
  • Ivan Franko Lviv National University, Chemistry Faculty, Analytical Chemistry Department, Kyrylо & Mefodiy Str., 6, 79005, Lviv, Ukraine
  • Ivan Franko Lviv National University, Chemistry Faculty, Analytical Chemistry Department, Kyrylо & Mefodiy Str., 6, 79005, Lviv, Ukraine
  • Ivan Franko Lviv National University, Chemistry Faculty, Analytical Chemistry Department, Kyrylо & Mefodiy Str., 6, 79005, Lviv, Ukraine
  • State Scientific Research Control Institute of Veterinary Preparations and Fodder Additives, Donetska Str.,11, 79019, Lviv, Ukraine
Bibliografia
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Typ dokumentu
Bibliografia
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Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_1515_chem-2015-0139
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