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2015 | 13 | 1 |
Tytuł artykułu

Liquid chromatographic determination of glyphosate and aminomethylphosphonic acid residues in rapeseed with MS/MS detection or derivatization/fluorescence detection

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Języki publikacji
EN
Abstrakty
EN
Glyphosate and AMPA determinations in rapeseed extracts by (a) liquid chromatography with triple quadrupole MS detection (LC-MS/MS), or (b) liquid chromatography with post-column OPA derivatization and fluorescence detection (LC-FLD) were developed. Mean recoveries for glyphosate and AMPA were (a) 88.8–95.0% and 82.1–86.1%, and (b) 70.8–74.1% and 62.4–72.6%. RSD were below (a) 11% and (b) 22%. Correlation coefficients were above 0.997 for both methods. LOD were 0.01 mg kg-1 for (a) and 0.05 mg kg-1 for (b). Both methods are simple and efficient for routine analysis of glyphosate and AMPA in a fatty matrix.
EN
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Wydawca

Czasopismo
Rocznik
Tom
13
Numer
1
Opis fizyczny
Daty
otrzymano
2014-12-08
zaakceptowano
2015-04-01
online
2015-06-22
Twórcy
  • Institute of Plant Protection – National Research Institute, Chełmońskiego 22, 15-195 Bialystok, Poland
  • Institute of Plant Protection – National Research Institute, Chełmońskiego 22, 15-195 Bialystok, Poland
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Typ dokumentu
Bibliografia
Identyfikatory
Identyfikator YADDA
bwmeta1.element.-psjd-doi-10_1515_chem-2015-0107
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