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EN
A series of Schiff’s bases have been synthesized by fly-ash:p-toluenesulfonic acid (fly-ash:PTS) catalyzed microwave assisted oxidative coupling of arylamines and substituted benzaldehydes under solvent-free condition. The synthesized Schiff’s bases are characterized by their physical constants, analytical and spectroscopic data. The group frequencies of imines such as IR (v, cm–1) and NMR (δ, ppm) spectral data was correlated with Hammett substituent constants, F and R parameters using single and multi-linear regression analysis. The antimicrobial activities of these Schiff’s bases have been studied using Bauer-Kirby method.
EN
Passive Torque Simulator (PTS) is an important ground based hardware tester simulator used for qualification of flight actuation system under aerodynamics torque loading .In this work extra torque disturbance due to actuator motion under test is analyzed and fuzzy Backstepping control with online parameters tuning scheme is proposed. Since extra torque affects both transient and steady state performance of the control loop, high gain adaptive control is investigated to improve the transient response of PTS torque tracking. Finally fuzzy Back stepping control with online parameters tuning scheme is proposed to improve torque tracking performance of load simulator both in transient and steady state. Simulations results show the validity of proposed control.
PL
W artykule przedstawiono analizę wpływu ruchu siłownika w czasie testu, na zakłócenia pomiaru momentu obciążenia na potrzeby symulatora obciążenia aerodynamicznego w systemie siłowników (ang. Passive Torque Simulator). W algorytmie wykorzystano sterowanie oparte na logice rozmytej z krokiem wstecz i parametrami dobieranymi online.
EN
A series of aryl imines have been synthesized by Fly-ash: PTS catalyzed microwave assisted oxidative coupling of amines and aldehydes under solvent-free conditions. The yield of the imines has been found to be more than 90 %. The purity of all imines has been checked using their physical constants and spectral data as published earlier in literature. The UV ?maxC=N(nm), infrared ?C=N(cm-1), NMR ?(ppm) of CH=N and C=N spectral data have been correlated with Hammett substituent constants and F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituents on the above spectral data has been studied. The antimicrobial activities of all imines have been studied using Bauer-Kirby method.
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